铜镍钴硅合金带箔材编制说明

《铜镍钴硅合金带箔材》行业标准编制说明（讨论稿）一、任务来源根据工信厅科函〔2022〕94号《工业和信息化部办公厅关于印发2022年第一批行业标准制修订和外文版项目计划的通知》，其中行业标准（项目编号“2022-0045T-YS”）《铜镍钴硅合金带箔材》由宁波兴业盛泰集团有限公司，宁波兴业鑫泰新型电子材料有限公司，有研工程技术研究院有限公司起草，完成年限为2024年。二、工作简况1、立项目的和意义高强高导铜合金带材具有高的强度、优良的导电和导热性能，是载人航天与探月工程、卫星导航系统等国家重点工程、重点领域和新一代3C产品所必须和急需的关键基础材料。铜镍钴硅合金是上述领域相关部件所必须的接插件、电力转换等元器件的核心材料。据统计，2021年我国高性能铜镍钴硅铜合金带材国内需求量达到约10万吨，产值150亿元以上，年增长率20%以上，但该高端合金板带材完全被日本、美国和德国的铜加工企业垄断，完全依赖进口，严重受制于人，不利于国家经济的发展和国防安全。加快铜镍钴硅合金标准建立，契合国家和地方科技发展规划的要求，属于国家重点领域发展的重大战略需求，可显著提高企业整体技术装备水平及提升国内外市场竞争力的发展战略，是满足国家重大工程、加快企业转型升级和提升产品国际竞争力之急需。2、项目编制组成员根据任务落实会会议精神，本项目的编制组由宁波兴业盛泰集团有限公司负责起草,并且由相关单位参加起草，组织相关单位组建了《铜镍钴硅合金带箔材》行业标准修订起草小组。3、主编单位的技术基础本标准的负责起草单位宁波兴业盛泰集团有限公司是中国铜板带材十强企业（第一），拥有国家认定企业技术中心、国家级博士后科研工作站、浙江省工程研究中心等。先后承担国家“十三五”重点研发计划、国家NQI重点研发计划、火炬计划等项目，迄今已获得41项发明专利，主持、参与我国国家、行业标准制修订工作30余项，引领我国有色合金新材料行业持续发展。宁波兴业盛泰集团有限公司致力于有色合金新材料的研发和生产,服务于超大规模集成电路、5G/6G通讯、航空航天、高铁、船舶、新能源汽车等30多个行业，打破了多项国外企业对高端合金领域的垄断，解决了新材料“卡脖子”问题，助推我国产业升级。公司在有色合金新材料领域多种新材料的成功研发及产业化，为起草本行业标准提供了有力的技术支撑，具备了起草本行业标准的技术基础。4主要工作过程接到标准起草任务后，宁波兴业盛泰集团有限公司立即成立了标准编制小组，首先整理收集本企业曾经生产的产品的技术要求及产品使用现状，为本标准全面、系统、有效的制定奠定了良好的基础；同时编制小组会同市场开发和营销人员对铜镍钴硅合金带箔材市场进一步调研，多角度了解市场商不同客户的需求以及产品未来发展趋势，同时收集了主要生产厂商的生产水平和现状，经综合研究、分析、整合调查的资料，对铜镍钴硅合金带箔材的产品分类、技术要求、试验方法、检验规则等进行了反复试验、检测、验证和确定。开始了本标准的起草工作，经过编制小组多次内部讨论及广泛征求意见，于2022年11月7日形成了本标准的《讨论稿》。三、标准编制原则本标准起草单位自接受起草任务后，成立了本标准编制工作组负责收集生产统计、检验数据、市场需求及客户要求等信息。确定了《铜镍钴硅合金带箔材》标准起草所遵循的基本原则和编制依据：1）查阅相关标准和国内外客户的相关技术要求；2）根据国内铜镍钴硅合金带箔材生产企业具体情况，力求做到标准的合理性与实用性；3）根据技术发展水平及测试数据确定技术指标取值范围；4）完全按照GB/T1.1和有色加工产品标准和国家标准编写示例的要求进行格式和结构编写。四、确定标准主要内容的论据1标准题目与适用范围本文件立项名称为《铜镍钴硅合金带箔材》。此标准名称一方面规定了产品是铜合金箔带材，另一方面也体现了产品主要合金元素为镍钴硅。2要求2.1产品分类产品分类是对铜镍钴硅合金带箔材的牌号、代号、状态、规格应符合的规定，同时规定了产品标记方法。相关情况分别说明如下：（1）本标准根据我国铜镍钴硅合金带箔材应用的实际，参考了相关国家标准中的1个牌号：C70350。（2）状态的确定，铜镍钴硅合金带箔材标准对产品状态标示参照GB/T29094-2012标准，确定硬（TM04)、特硬（TM06）、弹性（TM08）三种状态。（3）规格范围：本标准根据铜镍钴硅合金带箔材的要求，及实际生产控制水平和目前客户的使用要求，规定公称尺寸为厚度（0.08~0.5）*宽度（8~600）mm，都能满足目前用户的使用要求。（4）产品标记方法：按照GB/T1.1-2009的规定，标准中分别给出了产品的典型标记示例。2.2化学成分本标准中的牌号都是来自GB/T5231中的牌号，化学成分应符合GB/T5231的规定。2.3尺寸及尺寸允许偏差对每一批产品，企业都要在出厂前对产品的外形尺寸进行严格的抽样检测。本标准尺寸及尺寸允许偏差根据铜镍钴硅合金带箔材的要求制定。2.3.1厚度带箔材的厚度尺寸及其允许偏差见表1。表1带箔材的厚度及允许偏差 单位为毫米厚度厚度允许偏差普通级较高级0.05-0.15±0.003±0.0025≥0.15-0.2±0.005±0.004≥0.2-0.3±0.006±0.005≥0.3-0.4±0.008±0.0075≥0.4-0.6±0.0125±0.010≥0.6-0.8±0.015±0.0125≥0.8-1.0±0.020±0.0152.3.2宽度带箔材的宽度应符合表2的规定。表2带箔材的宽度及允许偏差单位为毫米宽度宽度及允许偏差5-8080-120120-400400-6100.05-0.50±0.05±0.075±0.1±0.15≥0.50-1.0±0.08±0.1±0.15±0.22.3.3侧边弯曲度带箔材的侧边弯曲度应符合表3的规定。表3带材的侧边弯曲度单位为毫米宽度/mm侧边弯曲度允许偏差（mm/m）普通级高级厚度≥0.05-0.60厚度≥0.60-3.0厚度≥0.05-0.60厚度≥0.60-1.07.5-95634＞9-133.54.023＞13-253.03.51.52.5＞25-502.53.01.52＞50-1002.53.01.52＞100-600231.51.52.3.4毛刺本标准根据铜镍钴硅合金带箔材的要求制定。表4带箔材的毛刺要求单位为毫米厚度边缘毛刺≤0.500.01＞0.50-1.00.022.3力学性能本标准根据铜镍钴硅合金带箔材的要求制定。表5带箔材的力学性能牌号状态抗拉强度Rm/MPa断后伸长率A50mm％维氏硬度HVBSi2-0.8TM04770-900≥4220-280TM06840-970≥1240-300TM08≥900≥1≥2702.4弯曲性能本标准根据铜镍钴硅合金带箔材的要求制定。表6带箔材90°弯曲试验条件合金牌号状态最大弯曲内侧半径a厚度b：0.1mm~1mm垂直于轧制方向（GW）平行于轧制方向（BW）BSi2-0.8TM041×t1×tTM062×t2×tTM083.5×t4×t注1：t表示带材厚度a0×t表示弯曲内侧半径≤0.1mm。b厚度大于1mm的带材，弯曲试验条件由供需双方商定2.5抗应力松弛应力松弛率是恒量材料在常温或高温下，随着时间的变化，保持应力恒定的定量指标。随着端子连接器等电子元器件向着微型化、薄型化、高密度和高度集成化发展，在长时间使用中产生的热效应不断增加，部分元器件还可能在更高的温度下长时间使用，为了保持端子连接器弹片的嵌合力，这就要求材料具有优良的抗应力松弛性能。应力松弛性能已成为未来高端端子连接器材料的重要性能指标，目前部分下游企业已对材料提出了应力松弛性能的要求。因此本标准中创新性的引入弯曲应力松弛试验，符合未来高端连接器材料的使用需求，也体现出本标准的先进性及前瞻性。目前生产企业通常采用弯曲应力松弛试验方法测量材料的应力松弛率，但企业及下游客户对弯曲应力松弛性能的检测方法、试验装置以及评价指标均没有一个统一的标准，因此本标准提出当客户有需求时，弯曲应力松弛性能指标以及试验方法由供需双方协商决定。表7抗应力松弛性能合金牌号状态抗应力松弛率%BSi2-0.8TM0470TM0670TM08552.6电性能当需方要求带箔材电性能时，电性能应由供需双方协商决定，带箔材电性能的测试方法按YS/T478以及GB/T3930的规定进行。表8电性能合金牌号20℃时导电率/%IACSBSi2-0.8≥402.7表面质量本标准根据端子连接器用铜及铜合金带箔材的要求制定。规定带箔材的表面应光滑、清洁，不允许有任何影响使用的缺陷。标准水平分析本标准合金牌号1个，等同采用ASTM牌号、国家标准1个；等同采用日标的牌号1个。本标准是依据目前我国铜及铜合金加工的实际生产和使用情况制定的，基本与国外先进标准保持一致，本标准达到国际先进水平。四、标准主要内容的确定依据4.1合金成分实测情况BSi2-0.8合金实测成分见下表。表9BSi2-0.8合金实测的成分统计数据表元素NiCoSiMnFeZnPbMg标准值1.0～2.51.0～2.00.5～1.2≤0.20≤0.20≤1.0≤0.05≤0.15实际值范围1.41～1.90.95～1.530.5～0.70.01～0.190.007～0.1290.003～0.0820.0002～0.00390.001～0.071统计数（个）291291291291291291291291合格率（%）10097.261001001001001001004.2外形尺寸实测情况BSi2-0.8外形尺寸实测数据见附录。4.3力学性能实测情况表10BSi2-0.8（TM04)合金抗拉强度数据表合金牌号状态样品数量（个）抗拉强度检测结果范围（MPa）BSi2-0.8TM04148770-876图1BSi2-0.8（TM04)合金抗拉强度分布图表11BSi2-0.8（TM06)合金抗拉强度数据表合金牌号状态样品数量（个）抗拉强度检测结果范围（MPa）BSi2-0.8TM06135840-901图2BSi2-0.8（TM06)合金抗拉强度分布图表12BSi2-0.8（TM04)合金断后伸长率数据表合金牌号状态样品数量（个）断后伸长率检测结果范围（%）BSi2-0.8TM041483.5~9图3BSi2-0.8（TM04)合金断后伸长率分布图表13BSi2-0.8（TM06)合金断后伸长率数据表合金牌号状态样品数量（个）断后伸长率检测结果范围（%）BSi2-0.8TM061351~12图4BSi2-0.8（TM06)合金断后伸长率分布图表14BSi2-0.8（TM04)合金维氏硬度数据表合金牌号状态样品数量（个）维氏硬度检测结果范围（HV）BSi2-0.8TM04148220~269图5BSi2-0.8（TM04)合金维氏硬度分布图表15BSi2-0.8（TM06)合金维氏硬度数据表合金牌号状态样品数量（个）维氏硬度检测结果范围（HV）BSi2-0.8TM06135243~280图6BSi2-0.8（TM06)合金维氏硬度分布图表16BSi2-0.8(TM08)合金实测的力学性能统计数据表状态抗拉强度断后伸长率维氏硬度范围/MPa数量合格率范围/%数量合格率范围/%HV数量合格率TM02921~9278100%1.5~3.08100%275~2848100%4.3电性能实测情况表17BSi2-0.8合金导电率数据表合金牌号状态样品数量（个）导电率检测结果范围（%IACS）BSi2-0.8TM04+TM064+TM0829144-53图7BSi2-0.8合金导电率分布图4.4其他指标实测情况表面质量均合格，弯曲性能和抗应力松弛数据待补充。五、与现行相关法律、法规、规章及相关标准，特别是强制性标准的协调性与现行相关法律、法规、规章及相关强制推荐的标准没有冲突。六、重大分歧意见的处理经过和依据无。七、标准作为强制性或推荐性国家（或行业）标准的建议本标准建议不作为强制性标准，建议作为推荐性标准。八、贯彻标准的要求和措施建议本标准是以我国铜镍钴硅合金带箔材的实际生产现状为基础，结合国内、外订货合同要求，建议相关单位组织专项标准宣贯会进行系统学习。本标准发布后，各企业应积极宣传和贯彻，并立即采用新标准订货，以保证产品质量，满足国内、外市场及用户的需要。九、废止现行有关标准的建议无。十、其它应予说明的事项本标准根据目前国内铜镍钴硅合金带箔材的实际生产现状和订货合同情况确定合金的牌号及成分、性能以及其它的要求。考虑随着新材料的开发使用和生产装备的更新，如果以后生产或订货合同中有其它合金或状态需求可在下一版中进行补充修订。十一、预期效果通过标准的贯彻实施，将提高我国铜镍钴硅合金带箔材规范并提高该类产品的生产控制水平。本标准结合我国国情，在国内生产企业及国内外用户需求的基础上，参照国内外相关产品标准规范制定的，技术指标先进，具有普遍性、广泛性、适用性、科学性和先进性。本标准发布后，将规范我国铜镍钴硅合金带箔材的性能和技术要求，提高产品在国内、外市场上的竞争力，给生产企业带来较大的经济效益。《铜镍钴硅合金带箔材》行业标准编制组2022年11月7日附录序号状态厚度宽度抗拉延伸硬度屈服强度导电率%厚度公差宽度公差表面质量1TM040.12286844425380046.70.0010.025合格2TM040.255258185.5258759530.0050.03合格3TM040.255158187.5258759530.0050.045合格4TM040.25787754.523075051.20.0050.025合格5TM040.2550781724175448.90.00250.03合格6TM040.3585777623174545.90.0050.05合格7TM040.255828153.5235789510.0050.035合格8TM040.25300771522075048.40.0050.025合格9TM040.25307724.524072251.10.0040.025合格10TM040.25317724.524072251.10.0040.03合格11TM040.25567771522075048.40.0050.05合格12TM040.33057925.524074745.80.0050.025合格13TM040.254307735.522973047.30.0050.04合格14TM040.25300778623275145.30.00050.025合格15TM040.2300800424476045.90.00350.025合格16TM040.2230810423479145.20.0010.0035合格17TM040.2200804424077146.80.0010.0035合格18TM040.25290781423876146.50.0020.0035合格19TM040.2300770623874245.20.00150.0035合格20TM040.2300770623874245.20.00150.0035合格21TM040.3326788623876345.70.0020.0035合格22TM040.23007914.524177445.60.0010合格23TM040.1515775423775047.50.0020.025合格24TM040.15300783424275247.50.0020.02合格25TM040.25280773424175545.80.00150合格26TM040.219.37914.524177445.60.0020.025合格27TM040.25240822524880244.20.00150合格28TM040.2300794424077145.20.0010合格29TM040.23380788524176746.70.0020.0035合格30TM040.825808622977648.80.0030.03合格31TM040.8200808622977648.80.0020合格32TM040.2300815424875845.20.0020.02合格33TM040.25300796623575546.40.00050.02合格34TM040.25300840425578546.60.0010.02合格35TM040.2523.5840425578546.60.0020.025合格36TM040.861812923876345.50.00150.015合格37TM040.3343822426079046.50.0010.03合格38TM040.25202836725977148.70.00050.02合格39TM040.22708324.525876344.40.0010.02合格40TM040.252808354.525977747.90.0010.02合格41TM040.2300783524175550.30.0010.03合格42TM040.251808395.525978745.60.00150.02合格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