赣榆海州湾生物科技园产业发展规划环境影响评价环境现状监测检测报告

检测报告TESTREPORT编号：连智检（2021）第164号项目名称：

赣榆海州湾生物科技园产业发展规划环境影响评价环境现状监测委托单位： 江苏智盛环境科技有限公司检测类别： 委托检测报告日期： 2021年05月28日学院科技南楼层连云港智清环境科技有限公司 地址连云港市海州区晨光路2号连云港职业技学院科技南楼层4

电话测报告说明一、本报告无检测检验专用章、骑缝章、无审核签发者签字无效。二、对检测结果如有异议者，请于收到报告之日起十日内向连云港智清环境科技有限公司提出。逾期不提出，视为认可检测报告。三、本报告部分复制、私自冒用、涂改或以其它任何形式篡改均属无效。经同意复制的复制件，应由连云港智清环境科技有限公司加盖公章确认。四、委托单位对样品的代表性和真实性负责，检测报告只对所检样品检测项目的检测结果负责，委托检测结果及其对结果的判定结论只代表检测时污染物排放状况，排放标准由客户提供。五、由委托单位自行采集的样品，本检验部门仅对送检样品检验数据负责，不对样品来源负责。六、除客户特别申明并支付样品管理费，所有超过标准规定时效期的样品均不再做留样。七、本单位保证工作的客观公正性，对委托单位的商业信息、技术文件等商业秘密履行保密义务。“*”检测项目带“☆”的，为本实验室无相应资质认定许可技术能力分包项目。单位名称：连云港智清环境科技有限公司联系地址：连云港海州区晨光路2号连云港职业技术学院科技南楼4层联系电话政编码：222000连云港智清环境科技有限公司 连智检（2021）第164号检测报告委托单位江苏智盛环境科技有限公司受检单位/受检单位地址/联系人孙万钊联系电样日期2021.05.06~05.12、05.21、05.23分析日期样品来源采样任务流转卡号JC21153采样人员样品类别地表水、地下水、海水、环境空气、噪声、土壤、底泥、包气带检测目的赣榆海州湾生物科技园产业发展规划环境影响评价环境现状监测检测内容海 水化学需氧量氨氮硝酸盐氮亚硝酸盐氮活性磷酸盐六价铬石油类、铅☆、铬、铜☆、锌☆、镍☆地下水：pH值、钾、钠、钙、镁、碳酸根、重碳酸根、氯化物、硫酸盐、氨氮、硝环境空气：氨、硫化氢、臭气浓度、氯化氢、氟化物、铅、苯乙烯、甲苯、间二甲苯、对二甲苯、邻二甲苯、硫酸雾、甲醇、乙醇、非甲烷总烃土 壤值汞砷铜铅镍镉六价铬氧化还原电位阳离子交换量、容重、挥发性有机物、半挥发性有机物底 泥：铜、锌、镍、铬、镉、铅、汞、砷噪 声：等效连续A声级检测依据详见第19~24页检测结果详见第2~13页备注1、ND为未检出；2、检测项目中带“”项目分包苏州环优检测有限公司，报告编号HY210556、HY210511057、HY210524023(CMA171012050352）。编制： 审核： 签发： 签发日期检测机构检验章年 月日第1页共27页连智检（2021）第连智检（2021）第164号连云港智清环境科技有限公司第第16页共27页表（1）地表水检测结果采样地点采样日期采样时间检测项目化学需氧量氟化物氨氮总磷石油类铅六价铬锌mg/Lmg/Lmg/Lmg/Lmg/Lμg/Lmg/Lmg/L1#兴庄河闸2021.05.1009:31260.581.040.230.0320.3ND0.0215:30280.611.390.260.0432.9ND0.023#官庄河老204国道交汇处10:02380.771.360.280.0337.8ND0.0616:01340.781.680.290.0443.1ND0.054#官庄河闸10:28330.721.440.320.0545.9ND0.0616:26370.721.720.330.0447.6ND0.08采样地点采样日期采样时间铜甲苯间二甲苯对二甲苯邻二甲苯苯乙烯镍☆样品性状μg/Lμg/Lμg/Lμg/Lμg/Lμg/Lmg/L/1#兴庄河闸2021.05.1009:3114.3NDNDNDNDND2.10×10-3淡黄微浊、微弱15:3017.7NDNDNDNDND2.28×10-3淡黄微浊、微弱3#官庄河老204国道交汇处10:0248.4NDNDNDNDND5.09×10-3淡黄微浊、微弱16:0146.9NDNDNDNDND5.37×10-3淡黄微浊、微弱4#官庄河闸10:2885.9NDNDNDNDND5.22×10-3淡黄微浊、微弱16:2695.2NDNDNDNDND0.0113淡黄微浊、微弱表（1）地表水检测结果（续）采样地点采样日期采样时间检测项目化学需氧量氟化物氨氮总磷石油类铅六价铬锌mg/Lmg/Lmg/Lmg/Lmg/Lμg/Lmg/Lmg/L1#兴庄河闸2021.05.1109:30240.561.180.300.0421.3ND0.0215:27250.581.130.290.0520.3ND0.043#官庄河老204国道交汇处10:00300.711.400.270.0635.6ND0.0716:00400.741.440.250.0534.1ND0.074#官庄河闸10:27360.631.410.340.0748.6ND0.0916:27340.641.460.330.0648.6ND0.10采样地点采样日期采样时间铜甲苯间二甲苯对二甲苯邻二甲苯苯乙烯镍☆样品性状μg/Lμg/Lμg/Lμg/Lμg/Lμg/Lmg/L/1#兴庄河闸2021.05.1109:3019.0NDNDNDNDND3.77×10-3淡黄微浊、微弱15:2719.3NDNDNDNDND3.62×10-3淡黄微浊、微弱3#官庄河老204国道交汇处10:0045.6NDNDNDNDND0.0141淡黄微浊、微弱16:0045.1NDNDNDNDND0.0123淡黄微浊、微弱4#官庄河闸10:2778.1NDNDNDNDND0.0127淡黄微浊、微弱16:2796.6NDNDNDNDND0.0109淡黄微浊、微弱表（1）地表水检测结果（续）采样地点采样日期采样时间检测项目化学需氧量氟化物氨氮总磷石油类铅六价铬锌mg/Lmg/Lmg/Lmg/Lmg/Lμg/Lmg/Lmg/L1#兴庄河闸2021.05.1209:33290.551.190.250.0419.3ND0.0215:26270.621.210.270.0433.6ND0.043#官庄河老204国道交汇处10:06350.761.480.330.0434.1ND0.0815:59340.751.480.310.0541.4ND0.084#官庄河闸10:32360.671.580.280.0642.6ND0.0916:25350.611.560.290.0646.6ND0.09采样地点采样日期采样时间铜甲苯间二甲苯对二甲苯邻二甲苯苯乙烯镍☆样品性状μg/Lμg/Lμg/Lμg/Lμg/Lμg/Lmg/L/1#兴庄河闸2021.05.1209:3312.4NDNDNDNDND2.48×10-3淡黄微浊、微弱15:2619.5NDNDNDNDND2.80×10-3淡黄微浊、微弱3#官庄河老204国道交汇处10:0647.2NDNDNDNDND5.31×10-3淡黄微浊、微弱15:5944.8NDNDNDNDND5.95×10-3淡黄微浊、微弱4#官庄河闸10:3278.1NDNDNDNDND0.0135淡黄微浊、微弱16:2597.4NDNDNDNDND0.0129淡黄微浊、微弱表（2）海水检测结果采样地点采样日期采样时间检测项目化学需氧量氨硝酸盐亚硝酸盐活性磷酸盐六价铬石油类mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L2#老兴庄河闸下(G228国道附近)2021.05.0709:102.660.1700.2150.02070.0246ND0.0515:112.340.1530.1310.01530.0235ND0.026#兴庄河闸下近岸海域09:263.950.2180.2840.05900.0333ND0.1415:313.890.2050.2140.03050.0224ND0.035#沙旺河闸下近岸海域09:542.650.2210.2110.09050.0273ND0.0515:552.340.2100.1570.04080.0262ND0.03采样地点采样日期采样时间镍☆铅☆铜☆锌☆铬☆//mg/Lmg/Lmg/Lmg/Lmg/L//2#老兴庄河闸下(G228国道附近)2021.05.0709:104.5×10-32.23×10-30.01240.02937×10-4//15:114.2×10-32.49×10-30.01250.01063.8×10-3//6#兴庄河闸下近岸海域09:264.3×10-34.79×10-30.01220.00853.6×10-3//15:314.2×10-32.09×10-30.01240.00962.8×10-3//5#沙旺河闸下近岸海域09:543.2×10-31.46×10-38.6×10-30.00963.6×10-3//15:554.3×10-32.11×10-30.01270.01062.8×10-3//表（2）海水检测结果（续）采样地点采样日期采样时间检测项目化学需氧量氨硝酸盐亚硝酸盐活性磷酸盐六价铬石油类mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L2#老兴庄河闸下(G228国道附近)2021.05.0809:362.680.1670.3100.02110.0197ND0.0415:362.220.1620.1730.01540.0191ND0.026#兴庄河闸下近岸海域09:593.980.2140.2700.05930.0341ND0.1016:013.960.2350.2050.03080.0338ND0.035#沙旺河闸下近岸海域10:272.940.2180.2350.08900.0278ND0.0516:292.380.2000.2140.04050.0265ND0.03采样地点采样日期采样时间镍☆铅☆铜☆锌☆铬☆//mg/Lmg/Lmg/Lmg/Lmg/L//2#老兴庄河闸下(G228国道附近)2021.05.0809:363.0×10-31.39×10-33.2×10-30.02984×10-4//15:363.3×10-31.90×10-33.7×10-30.01705×10-4//6#兴庄河闸下近岸海域09:593.5×10-31.98×10-33.5×10-30.02985×10-4//16:013.2×10-31.97×10-33.7×10-30.01491.8×10-3//5#沙旺河闸下近岸海域10:275.4×10-31.39×10-33.9×10-30.01542.7×10-3//16:295.1×10-31.90×10-33.6×10-3ND2.6×10-3//表（2）海水检测结果（续）采样地点采样日期采样时间检测项目化学需氧量氨硝酸盐亚硝酸盐活性磷酸盐六价铬石油类mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L2#老兴庄河闸下(G228国道附近)2021.05.0909:422.610.1680.3180.02100.0240ND0.0415:472.170.1620.1780.01530.0221ND0.036#兴庄河闸下近岸海域10:113.980.2180.2360.06000.0300ND0.0916:203.950.2070.2140.03080.0276ND0.035#沙旺河闸下近岸海域10:342.810.2210.1940.08880.0267ND0.0516:492.400.2020.1610.04180.0254ND0.02采样地点采样日期采样时间镍☆铅☆铜☆锌☆铬☆//mg/Lmg/Lmg/Lmg/Lmg/L//2#老兴庄河闸下(G228国道附近)2021.05.0909:429.5×10-31.29×10-33.6×10-30.01177.0×10-4//15:473.1×10-31.19×10-33.1×10-30.02025.0×10-4//6#兴庄河闸下近岸海域10:112.9×10-31.14×10-35.7×10-30.00962.7×10-3//16:203.3×10-31.89×10-33.6×10-30.01121.8×10-3//5#沙旺河闸下近岸海域10:343.3×10-39.9×10-40.01190.00962.7×10-3//16:495.6×10-37.15×10-37.1×10-30.02342.7×10-3//表（3）地下水检测结果表采样地点采样日期采样时间检测项目pH值钾钠钙镁碳酸根重碳酸根氯化物硫酸根无量纲mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/LD12021.05.1216:566.7722.727015431.2ND39051881.2D217:248.5573.32.38×10341898.0562784.21×103618D317:497.862836.96×103827374ND4391.20×1042.09×103D418:167.2725.530118926.9ND430568179D518:507.282567.85×103863355ND4301.35×1042.06×103采样地点采样日期采样时间检测项目耗氧量（CODMn）总硬度（以CaCO3计）溶解性总固体硝酸盐氮（以N计）亚硝酸盐氮（N计）氨氮六价铬铜铅mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lμg/Lμg/LD12021.05.1216:560.826201.95×1031.2ND0.626ND15.421.4D217:2430.61.87×1039.20×1032.11.355.84ND49.436.3D317:493.324.55×1034.60×1040.50.0054.89ND90.962.1D418:164.537101.83×1030.20.0320.679ND17.714.9D518:504.295.25×1034.82×1040.60.0183.15ND80.964.4表（3）地下水检测结果表（续）采样地点采样日期采样时间检测项目地下水检测点位参数及样品性状统计表锌甲苯对二甲苯间二甲苯邻二甲苯镍☆经度纬度样品性状mg/Lμg/Lμg/Lμg/Lμg/Lmg/L///D12021.05.1216:560.07NDNDNDND8.30×10-4119.150759967034.9188860198无色透明、无味D217:240.04NDNDNDND0.0177119.179683170234.9197617750淡黄微浊、弱D317:490.10NDNDNDND5.13×10-3119.182922623234.9074296283淡黄微浊、微弱D418:160.13NDNDNDND3.59×10-3119.168746765734.8982262282淡黄微浊、微弱D518:500.26NDNDNDND8.54×10-3119.193072930234.9094913567淡黄微浊、微弱以下空白第第19页共27页表（4）环境空气检测结果表采样地点采样时间检测项目氨mg/m³硫化氢mg/m³臭气浓度无量纲氯化氢mg/m³氟化物μg/m³硫酸雾mg/m³非甲烷总烃mg/m³苯乙烯mg/m³甲苯mg/m³间二甲苯mg/m³G1匡口村（园区内）2021.05.0602:000.050.003ND0.032ND0.0890.59NDNDND08:000.060.003ND0.027ND0.0880.62NDNDND14:000.080.005ND0.030ND0.0770.61NDNDND20:000.050.006ND0.029ND0.0750.62NDNDNDG2兴庄村02:000.060.004ND0.041ND0.0910.49NDNDND08:000.060.003ND0.041ND0.0670.49NDNDND14:000.080.004ND0.032ND0.0830.53NDNDND20:000.060.006ND0.033ND0.0820.63NDNDNDG3李巷村02:000.060.003ND0.020ND0.0810.50NDNDND08:000.040.004ND0.018ND0.0960.43NDNDND14:000.040.005ND0.031ND0.0760.49NDNDND20:000.050.005ND0.017ND0.0800.47NDNDND表（4）环境空气检测结果表（续）采样地点采样时间检测项目氨mg/m³硫化氢mg/m³臭气浓度无量纲氯化氢mg/m³氟化物μg/m³硫酸雾mg/m³非甲烷总烃mg/m³苯乙烯mg/m³甲苯mg/m³间二甲苯mg/m³G1匡口村（园区内）2021.05.0702:000.050.003ND0.036ND0.0900.52NDNDND08:000.070.003ND0.037ND0.0870.49NDNDND14:000.060.004ND0.029ND0.0790.48NDNDND20:000.040.005ND0.027ND0.0750.48NDNDNDG2兴庄村02:000.030.006ND0.028ND0.0920.43NDNDND08:000.020.004ND0.026ND0.0680.43NDNDND14:000.070.006ND0.029ND0.0820.39NDNDND20:000.070.005ND0.032ND0.0820.46NDNDNDG3李巷村02:000.050.006ND0.029ND0.0790.58NDNDND08:000.050.004ND0.029ND0.1020.53NDNDND14:000.040.006ND0.029ND0.0770.59NDNDND20:000.030.003ND0.039ND0.0800.55NDNDND表（4）环境空气检测结果表（续）采样地点采样时间检测项目氨mg/m³硫化氢mg/m³臭气浓度无量纲氯化氢mg/m³氟化物μg/m³硫酸雾mg/m³非甲烷总烃mg/m³苯乙烯mg/m³甲苯mg/m³间二甲苯mg/m³G1匡口村（园区内）2021.05.0802:000.050.003ND0.030ND0.0100.51NDNDND08:000.070.004ND0.033ND0.0110.35NDNDND14:000.030.005ND0.034ND0.0080.48NDNDND20:000.080.006ND0.032ND0.0080.50NDNDNDG2兴庄村02:000.060.006ND0.032ND0.0100.74NDNDND08:000.060.004ND0.032ND0.0070.56NDNDND14:000.060.006ND0.032ND0.0090.63NDNDND20:000.060.004ND0.033ND0.0090.48NDNDNDG3李巷村02:000.060.003ND0.030ND0.0080.62NDNDND08:000.040.004ND0.034ND0.0100.50NDNDND14:000.070.003ND0.041ND0.0080.50NDNDND20:000.040.003ND0.040ND0.0080.56NDNDND表（4）环境空气检测结果表（续）采样地点采样时间检测项目氨mg/m³硫化氢mg/m³臭气浓度无量纲氯化氢mg/m³氟化物μg/m³硫酸雾mg/m³非甲烷总烃mg/m³苯乙烯mg/m³甲苯mg/m³间二甲苯mg/m³G1匡口村（园区内）2021.05.0902:000.070.005ND0.020ND0.0100.47NDNDND08:000.060.003ND0.022ND0.0100.44NDNDND14:000.050.003ND0.016ND0.0080.45NDNDND20:000.030.004ND0.024ND0.0080.47NDNDNDG2兴庄村02:000.060.004ND0.020ND0.0100.66NDNDND08:000.070.003ND0.022ND0.0070.66NDNDND14:000.040.004ND0.023ND0.0090.66NDNDND20:000.040.004ND0.043ND0.0090.66NDNDNDG3李巷村02:000.110.005ND0.040ND0.0080.42NDNDND08:000.040.005ND0.041ND0.0100.41NDNDND14:000.070.005ND0.019ND0.0070.47NDNDND20:000.060.006ND0.013ND0.0080.43NDNDND表（4）环境空气检测结果表（续）采样地点采样时间检测项目氨mg/m³硫化氢mg/m³臭气浓度无量纲氯化氢mg/m³氟化物μg/m³硫酸雾mg/m³非甲烷总烃mg/m³苯乙烯mg/m³甲苯mg/m³间二甲苯mg/m³G1匡口村（园区内）2021.05.1002:000.050.004ND0.038ND0.0100.29NDNDND08:000.060.004ND0.038ND0.0100.25NDNDND14:000.070.006ND0.033ND0.0080.25NDNDND20:000.030.006ND0.023ND0.0080.27NDNDNDG2兴庄村02:000.050.004ND0.023ND0.0100.34NDNDND08:000.050.006ND0.023ND0.0070.34NDNDND14:000.060.004ND0.041ND0.0090.31NDNDND20:000.090.002ND0.041ND0.0090.33NDNDNDG3李巷村02:000.040.004ND0.042ND0.0080.50NDNDND08:000.030.002ND0.029ND0.0100.44NDNDND14:000.050.004ND0.020ND0.0070.41NDNDND20:000.070.005ND0.019ND0.0080.37NDNDND表（4）环境空气检测结果表（续）采样地点采样时间检测项目氨mg/m³硫化氢mg/m³臭气浓度无量纲氯化氢mg/m³氟化物μg/m³硫酸雾mg/m³非甲烷总烃mg/m³苯乙烯mg/m³甲苯mg/m³间二甲苯mg/m³G1匡口村（园区内）2021.05.1102:000.060.005ND0.020ND0.0100.30NDNDND08:000.050.003ND0.019ND0.0100.30NDNDND14:000.030.004ND0.019ND0.0090.31NDNDND20:000.060.005ND0.021ND0.0050.28NDNDNDG2兴庄村02:000.060.004ND0.021ND0.0090.34NDNDND08:000.050.006ND0.020ND0.0090.39NDNDND14:000.050.005ND0.030ND0.0070.35NDNDND20:000.030.004ND0.028ND0.0090.34NDNDNDG3李巷村02:000.050.005ND0.027ND0.0070.40NDNDND08:000.060.005ND0.041ND0.0100.39NDNDND14:000.040.006ND0.042ND0.0090.35NDNDND20:000.050.006ND0.041ND0.0090.38NDNDND表（4）环境空气检测结果表（续）采样地点采样时间检测项目氨mg/m³硫化氢mg/m³臭气浓度无量纲氯化氢mg/m³氟化物μg/m³硫酸雾mg/m³非甲烷总烃mg/m³苯乙烯mg/m³甲苯mg/m³间二甲苯mg/m³G1匡口村（园区内）2021.05.1202:000.050.005ND0.020ND0.0100.30NDNDND08:000.030.002ND0.019ND0.0100.28NDNDND14:000.050.004ND0.021ND0.0090.30NDNDND20:000.060.003ND0.021ND0.0070.32NDNDNDG2兴庄村02:000.040.003ND0.021ND0.0090.45NDNDND08:000.060.004ND0.022ND0.0090.46NDNDND14:000.060.004NDNDND0.0080.46NDNDND20:000.080.003ND0.020ND0.0090.44NDNDNDG3李巷村02:000.060.004ND0.019ND0.0070.39NDNDND08:000.050.005ND0.019ND0.0090.37NDNDND14:000.090.005ND0.020ND0.0100.43NDNDND20:000.090.005ND0.019ND0.0090.40NDNDND表（4）环境空气检测结果表（续）采样地点采样时间检测项目对二甲苯mg/m³邻二甲苯mg/m³甲醇mg/m³乙醇mg/m³气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.0602:00NDNDNDND15.2100.8西南3.672.6多云08:00NDNDNDND20.9100.7西南3.264.7多云14:00NDNDNDND25.7100.6西南2.946.7多云20:00NDNDNDND22.1100.7西南3.558.6多云G2兴庄村02:00NDNDNDND15.4100.8西南3.672.8多云08:00NDNDNDND20.9100.7西南3.164.3多云14:00NDNDNDND25.5100.6西南2.846.4多云20:00NDNDNDND22.3100.7西南3.358.3多云G3李巷村02:00NDNDNDND15.4100.8西南3.772.9多云08:00NDNDNDND20.9100.7西南3.264.3多云14:00NDNDNDND25.8100.6西南3.046.4多云20:00NDNDNDND22.3100.7西南3.158.5多云表（4）环境空气检测结果表（续）采样地点采样时间检测项目对二甲苯mg/m³邻二甲苯mg/m³甲醇mg/m³乙醇mg/m³气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.0702:00NDNDNDND15.4100.9西3.170.8晴08:00NDNDNDND19.5100.7西2.860.7晴14:00NDNDNDND24.4100.6西2.640.2晴20:00NDNDNDND20.5100.7西2.954.3晴G2兴庄村02:00NDNDNDND15.6100.9西3.370.5晴08:00NDNDNDND19.7100.7西2.760.4晴14:00NDNDNDND24.5100.6西2.640.1晴20:00NDNDNDND20.5100.7西3.054.2晴G3李巷村02:00NDNDNDND15.6100.9西3.270.5晴08:00NDNDNDND19.3100.7西2.960.8晴14:00NDNDNDND24.6100.6西2.739.8晴20:00NDNDNDND20.4100.7西2.954.1晴表（4）环境空气检测结果表（续）采样地点采样时间检测项目对二甲苯mg/m³邻二甲苯mg/m³甲醇mg/m³乙醇mg/m³气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.0802:00NDNDNDND16.5100.6西南3.768.8晴08:00NDNDNDND22.0100.5西南3.462.4晴14:00NDNDNDND28.6100.4西南3.038.7晴20:00NDNDNDND24.6100.5西南3.556.7晴G2兴庄村02:00NDNDNDND16.2100.6西南3.768.7晴08:00NDNDNDND22.2100.5西南3.362.2晴14:00NDNDNDND28.8100.4西南3.138.7晴20:00NDNDNDND24.7100.5西南3.456.5晴G3李巷村02:00NDNDNDND16.3100.6西南3.668.6晴08:00NDNDNDND21.8100.5西南3.362.2晴14:00NDNDNDND28.4100.4西南3.238.9晴20:00NDNDNDND24.6100.5西南3.656.9晴第第25页共27页表（4）环境空气检测结果表（续）采样地点采样时间检测项目对二甲苯mg/m³邻二甲苯mg/m³甲醇mg/m³乙醇mg/m³气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.0902:00NDNDNDND14.5100.7东3.678.9阴08:00NDNDNDND16.8100.6东3.470.6阴14:00NDNDNDND23.6100.5东3.253.6阴20:00NDNDNDND17.4100.6东3.562.3阴G2兴庄村02:00NDNDNDND14.2100.7东3.778.6阴08:00NDNDNDND16.7100.6东3.570.2阴14:00NDNDNDND23.4100.5东3.153.1阴20:00NDNDNDND17.3100.6东3.662.7阴G3李巷村02:00NDNDNDND14.6100.7东3.779.2阴08:00NDNDNDND16.6100.6东3.570.1阴14:00NDNDNDND23.8100.5东3.352.9阴20:00NDNDNDND17.5100.6东3.762.5阴表（4）环境空气检测结果表（续）采样地点采样时间检测项目对二甲苯mg/m³邻二甲苯mg/m³甲醇mg/m³乙醇mg/m³气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.1002:00NDNDNDND12.5100.8东北3.875.6多云08:00NDNDNDND13.9100.7东北3.469.9多云14:00NDNDNDND20.4100.6东北3.245.6多云20:00NDNDNDND14.7100.7东北3.662.8多云G2兴庄村02:00NDNDNDND12.4100.8东北3.774.9多云08:00NDNDNDND13.8100.7东北3.669.5多云14:00NDNDNDND20.4100.6东北3.045.9多云20:00NDNDNDND14.8100.7东北3.862.3多云G3李巷村02:00NDNDNDND12.3100.8东北3.975.8多云08:00NDNDNDND13.7100.7东北3.569.2多云14:00NDNDNDND20.5100.6东北3.245.9多云20:00NDNDNDND14.6100.7东北3.463.2多云表（4）环境空气检测结果表（续）采样地点采样时间检测项目对二甲苯mg/m³邻二甲苯mg/m³甲醇mg/m³乙醇mg/m³气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.1102:00NDNDNDND13.0100.9东北3.681.8阴08:00NDNDNDND13.8100.8东北3.472.3阴14:00NDNDNDND16.8100.7东北3.050.6阴20:00NDNDNDND14.6100.8东北3.564.7阴G2兴庄村02:00NDNDNDND12.8100.9东北3.581.3阴08:00NDNDNDND13.6100.8东北3.272.8阴14:00NDNDNDND17.2100.7东北2.949.8阴20:00NDNDNDND14.4100.8东北3.464.2阴G3李巷村02:00NDNDNDND13.2100.9东北3.481.4阴08:00NDNDNDND13.9100.8东北3.372.9阴14:00NDNDNDND16.6100.7东北3.050.2阴20:00NDNDNDND14.8100.8东北3.464.1阴表（4）环境空气检测结果表（续）采样地点采样时间检测项目对二甲苯mg/m³邻二甲苯mg/m³甲醇mg/m³乙醇mg/m³气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.1202:00NDNDNDND13.4101.0东北2.477.6多云08:00NDNDNDND16.6100.9东北2.370.3多云14:00NDNDNDND20.4100.8东北1.943.7多云20:00NDNDNDND17.0100.9东北2.363.4多云G2兴庄村02:00NDNDNDND13.3101.0东北2.676.8多云08:00NDNDNDND16.8100.9东北2.270.7多云14:00NDNDNDND20.3100.8东北2.043.4多云20:00NDNDNDND16.7100.9东北2.463.8多云G3李巷村02:00NDNDNDND13.2101.0东北2.777.2多云08:00NDNDNDND16.2100.9东北2.470.9多云14:00NDNDNDND20.6100.8东北2.043.2多云20:00NDNDNDND17.2100.9东北2.463.9多云表（4）环境空气检测结果表（续）采样地点采样时间检测项目铅及其化合物气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.06日均值ND21.0100.7西南3.260.7多云G2兴庄村日均值ND21.0100.7西南3.260.5多云G3李巷村日均值ND21.1100.7西南3.360.5多云G1匡口村（园区内）2021.05.07日均值ND20.0100.7西2.956.5晴G2兴庄村日均值ND20.1100.7西2.956.3晴G3李巷村日均值ND20.0100.7西2.956.3晴G1匡口村（园区内）2021.05.08日均值ND22.9100.5西南3.456.7晴G2兴庄村日均值ND23.0100.5西南3.456.5晴G3李巷村日均值ND22.8100.5西南3.456.7晴G1匡口村（园区内）2021.05.09日均值ND18.1100.6东3.466.4阴G2兴庄村日均值ND17.9100.6东3.566.2阴G3李巷村日均值ND18.1100.6东3.666.4阴表（4）环境空气检测结果表（续）采样地点采样时间检测项目铅及其化合物气温℃气压kPa风向风速m/s%RH天气状况G1匡口村（园区内）2021.05.10日均值ND15.4100.7东北3.563.5多云G2兴庄村日均值ND15.4100.7东北3.563.2多云G3李巷村日均值ND15.3100.7东北3.563.5多云G1匡口村（园区内）2021.05.11日均值ND14.6100.8东北3.467.4阴G2兴庄村日均值ND14.5100.8东北3.367.0阴G3李巷村日均值ND14.6100.8东北3.367.2阴G1匡口村（园区内）2021.05.12日均值ND16.9100.9东北2.263.8多云G2兴庄村日均值ND16.8100.9东北2.463.8多云G3李巷村日均值ND16.8100.9东北2.463.8多云以下空白连云港智清环境科技有限公司连智检（2021连云港智清环境科技有限公司连智检（2021）第164号第第29页共27页表（5）土壤检测结果表采样日期采样地点T1园区内(德友精工附近)T4园区内采样深度（cm）0~5000150~150002150~3000030~5000450~150005150~300006检测项目单位测定值2021.05.21pH值无量纲7.87/////阳离子交换量cmol+/kg6.0/////氧化还原电位mv510/////容重g/cm31.59/////汞mg/kg0.0680.0480.0300.0710.1250.063砷mg/kg5.234.403.845.102.582.65铜mg/kg65465124299铅mg/kg19.120.821.014.016.17.2镍mg/kg412633312214镉mg/kg0.350.370.430.500.450.27六价铬mg/kgNDNDNDNDNDND氯甲烷μg/kgNDNDNDNDNDND氯乙烯μg/kgNDNDNDNDNDND1,1-二氯乙烯μg/kgNDNDNDNDNDND二氯甲烷μg/kgNDNDNDNDNDND反式-1,2-二氯乙烯μg/kgNDNDNDNDNDND1,1-二氯乙烷μg/kgNDNDNDNDNDND顺式-1,2-二氯乙烯μg/kgNDNDNDNDNDND氯仿μg/kgNDNDNDNDNDND1,1,1-三氯乙烷μg/kgNDNDNDNDNDND四氯化碳μg/kgNDNDNDNDNDND苯μg/kgNDNDNDNDNDND1,2-二氯乙烷μg/kgNDNDNDNDNDND三氯乙烯μg/kgNDNDNDNDNDND1,2-二氯丙烷μg/kgNDNDNDNDNDND表（5）土壤检测结果表（续）采样日期采样地点T1园区内(德友精工附近)T4园区内采样深度（cm）0~5000150~150002150~3000030~5000450~150005150~300006检测项目单位测定值2021.05.21甲苯μg/kgNDNDNDNDNDND1,1,2-三氯乙烷μg/kgNDNDNDNDNDND四氯乙烯μg/kgNDNDNDNDNDND氯苯μg/kgNDNDNDNDNDND1,1,1,2-四氯乙烷μg/kgNDNDNDNDNDND乙苯μg/kgNDNDNDNDNDND-二甲苯μg/kgNDNDNDNDNDND邻二甲苯μg/kgNDNDNDNDNDND苯乙烯μg/kgNDNDNDNDNDND1,1,2,2-四氯乙烷μg/kgNDNDNDNDNDND1,2,3-三氯丙烷μg/kgNDNDNDNDNDND1,4-二氯苯μg/kgNDNDNDNDNDND1,2-二氯苯μg/kgNDNDNDNDNDND苯胺mg/kgNDNDNDNDNDND2-氯苯酚mg/kgNDNDNDNDNDND硝基苯mg/kgNDNDNDNDNDND萘mg/kgNDNDNDNDNDND苯并(a)蒽mg/kgNDNDNDNDNDND䓛mg/kgNDNDNDNDNDND苯并(b)荧蒽mg/kgNDNDNDNDNDND苯并(k)荧蒽mg/kgNDNDNDNDNDND苯并(a)芘mg/kgNDNDNDNDNDND茚并(1,2,3-cd)芘mg/kgNDNDNDNDNDND二苯并(a,h)蒽mg/kgNDNDNDNDNDND表（5）土壤检测结果表（续）采样日期采样地点T3园区内(云海电源附近)采样深度（cm）0~5000750~150008150~300009检测项目单位测定值2021.05.21汞mg/kg0.0260.0290.138砷mg/kg1.350.945.59铜mg/kg141518铅mg/kg20.019.214.2镍mg/kg221131镉mg/kg0.310.420.36六价铬mg/kgNDNDND氯甲烷μg/kgNDNDND氯乙烯μg/kgNDNDND1,1-二氯乙烯μg/kgNDNDND二氯甲烷μg/kgNDNDND反式-1,2-二氯乙烯μg/kgNDNDND1,1-二氯乙烷μg/kgNDNDND顺式-1,2-二氯乙烯μg/kgNDNDND氯仿μg/kg1.41.5ND1,1,1-三氯乙烷μg/kgNDNDND四氯化碳μg/kgNDNDND苯μg/kgNDNDND1,2-二氯乙烷μg/kgNDNDND三氯乙烯μg/kgNDNDND1,2-二氯丙烷μg/kgNDNDND甲苯μg/kgNDNDND1,1,2-三氯乙烷μg/kgNDNDND表（5）土壤检测结果表（续）采样日期采样地点T3园区内(云海电源附近)采样深度（cm）0~5000750~150008150~300009检测项目单位测定值2021.05.21四氯乙烯μg/kgNDNDND氯苯μg/kgNDNDND1,1,1,2-四氯乙烷μg/kgNDNDND乙苯μg/kgNDNDND-二甲苯μg/kgNDNDND邻二甲苯μg/kgNDNDND苯乙烯μg/kgNDNDND1,1,2,2-四氯乙烷μg/kgNDNDND1,2,3-三氯丙烷μg/kgNDNDND1,4-二氯苯μg/kgNDNDND1,2-二氯苯μg/kgNDNDND苯胺mg/kgNDNDND2-氯苯酚mg/kgNDNDND硝基苯mg/kgNDNDND萘mg/kgNDNDND苯并(a)蒽mg/kgNDNDND䓛mg/kgNDNDND苯并(b)荧蒽mg/kgNDNDND苯并(k)荧蒽mg/kgNDNDND苯并(a)芘mg/kgNDNDND茚并(1,2,3-cd)芘mg/kgNDNDND二苯并(a,h)蒽mg/kgNDNDND第第40页共27页表（6）底泥检测结果表采样日期采样地点D1老新庄河闸底泥D2官庄河闸底泥D3200米检测项目单位测定值2021.05.21pH值无量纲8.228.198.20铜mg/kg564947锌mg/kg174110141镍mg/kg644757铬mg/kg128103122镉mg/kg0.410.380.38铅mg/kg31.633.229.2汞mg/kg0.0940.0550.032砷mg/kg8.756.347.93样品性状/壤土、黄棕色、无异味壤土、黄棕色、微弱壤土、黄棕色、微弱以下空白表（7）包气带检测结果表采样日期采样地点B1(德友精工附近)B2(北港镍业附近)采样深度地面以下10cm010地下水水位以上20cm011地面以下10cm012地下水水位以上20cm013检测项目单位测定值2021.05.23氟化物mg/L0.560.370.410.40铅μg/L79.065.243.114.1铬mg/LNDNDNDND锌mg/L0.020.050.200.08铜μg/L6.19.06.312.4甲苯μg/LNDNDNDND对二甲苯μg/LNDNDNDND间二甲苯μg/LNDNDNDND邻二甲苯μg/LNDNDNDND苯乙烯μg/LNDNDNDND镍☆μg/L0.7720.1501.601.30经度/119°10′38.10″119°10′38.10″119°10′44.56″119°10′44.56″纬度/34°55′3.66″34°55′3.66″34°54′16.32″34°54′16.32″样品性状/无植物根系、潮砂壤土、黄棕色无植物根系、湿壤土、棕色无植物根系、潮砂壤土、黄色无植物根系、湿壤土、棕色以下空白表（7）包气带检测结果表（续）采样日期采样地点B3(云海电源附近)B4赵沙村(背景值点位)采样深度地面以下10cm014地下水水位以上20cm015地面以下10cm016地下水水位以上20cm017检测项目单位测定值2021.05.23氟化物mg/L0.440.310.190.13铅μg/L19966.795.836.0铬mg/LNDNDNDND锌mg/L0.09ND0.120.18铜μg/L11.24.311.424.8甲苯μg/LNDNDNDND对二甲苯μg/LNDNDNDND间二甲苯μg/LNDNDNDND邻二甲苯μg/LNDNDNDND苯乙烯μg/LNDNDNDND镍☆μg/L2.341.963.174.37经度/119°11′14.68″119°11′14.68″119°10′24.98″119°10′24.98″纬度/34°53′22.76″34°53′22.76″34°55′8.40″34°55′8.40″样品性状/无植物根系、潮壤土、黄棕色无植物根系、湿壤土、棕色无植物根系、潮壤土、黄色无植物根系、湿壤土、棕色表（8）噪声测量结果执行标准GB3096-2008《声环境质量标准》测量时间2021年05月10日09:22~12:362021年05月10日22:01~05月11日01:152021年05月11日09:17~12:222021年05月11日22:01~05月12日01:25气象参数测点编号检测日期昼间风速（m/s）昼间风向夜间风速（m/s）夜间风向检测日期昼间风速（m/s）昼间风向夜间风速（m/s）夜间风向N12021.05.10~05.113.8东北3.9东北2021.05.11~05.123.4东北3.6东北N23.7东北3.8东北3.5东北3.7东北N33.7东北3.7东北3.6东北3.6东北N43.7东北3.6东北3.4东北3.7东北N53.6东北3.8东北3.5东北3.7东北N63.6东北3.7东北3.4东北3.6东北N73.6东北3.5东北3.5东北3.5东北N83.5东北3.6东北3.5东北3.7东北N93.6东北3.7东北3.4东北3.6东北N103.5东北3.6东北3.6东北3.5东北以下空白噪声测量结果（续）测点编号检测点位名称主要噪声源等效声级LeqdB（A）2021.05.10~05.112021.05.11~05.12昼间夜间昼间夜间N1N1生活噪声54465548N2N2交通噪声68536854N3N3生活噪声53465446N4N4工业噪声61506252N5N5生活噪声55465747N6N6工业噪声63516252N7N7工业噪声60526353N8N8工业噪声62536353N9N9生活噪声56485848N10N10工业噪声53475747备注检测期间N2点车辆情况：2021.05.10~05.1185辆/h13815辆/h45辆/h；2021.05.11~05.1283辆/h14718辆/h36辆/h。噪声校准表检测日期标准值校准值 dB(A)校准前校准后2021.05.1094.093.893.82021.05.1194.093.893.82021.05.1294.093.893.8以下空白附表：土壤参数表采样地点采样深度（cm）采样日期土壤检测点位参数及样品性状统计表经度纬度样品性状T1园区内(德友精工附近)0~502021.05.21119°10′42.38″34°55′5.75″无植物根系、潮砂壤土、黄棕色50~150119°10′42.38″34°55′5.75″黄棕色150~300119°10′42.38″34°55′5.75″棕色T4园区内0~50119°11′30.46″34°54′7.16″黄棕色50~150119°11′30.46″34°54′7.16″棕色150~300119°11′30.46″34°54′7.16″灰色T3园区内(云海电源附近)0~50119°11′20.52″34°53′22.76″黄棕色50~150119°11′20.52″34°53′22.76″黄棕色150~300119°11′20.52″34°53′22.76″黄棕色地表水质控数据统计表质控措施检测项目加标回收平行值质控样实验室空白数量回收率%数量相对偏差%保证值测得值数量化学需氧量35.1±1.9（mg/L）35.0（mg/L）35.1±1.9（mg/L）36.5（mg/L）35.1±1.9（mg/L）35.8（mg/L）氟化物//氨氮//总磷6.81±0.73（mg/L）7.16（mg/L）6.81±0.73（mg/L）7.20（mg/L）6.81±0.73（mg/L）7.06（mg/L）铅//石油类//铬锌铜镍甲苯对二甲苯间二甲苯邻二甲苯苯乙烯以下空白海水质控数据统计表质控措施检测项目加标回收平行值质控样实验室空白数量回收率%数量相对偏差%保证值测得值数量化学需氧量氨氮硝酸盐氮亚硝酸盐氮活性磷酸盐六价铬石油类以下空白地下水质控数据统计表质控措施检测项目加标回收平行值质控样实验室空白数量回收率%数量相对偏差%保证值测得值数量pH值/7.06±0.057.09/钾/1.54±0.12（mg/L）1.52（mg/L）2钠/0.882±0.045（mg/L）0.887（mg/L）2钙/4.48±0.19（mg/L）4.39（mg/L）2镁/0.118±0.008（mg/L）0.124（mg/L）2总碱度（碳酸根、碳酸氢根）/36.6±2.9（mg/L）37.6（mg/L）2总硬度/1.57±0.23（mmol/L）1.75（mmol/L）2硫酸根/31±1.8（mg/L）32.6（mg/L）2氨氮1//2氯化物/96.4±5.4（mg/L）97.7（mg/L）2耗氧量（CODMn）/13.4±0.8（mg/L）13.8（mg/L）2硝酸盐氮1//2亚硝酸盐氮1//2铅1//2六价铬1//2铜1//2锌1//2甲苯//2对二甲苯//2间二甲苯//2邻二甲苯以下空白土壤质控数据统计表质控措施检测项目加标回收平行值质控样实验室空白数量回收率%数量相对偏差%保证值测得值数量pH值//5.130±0.1905.16/汞//0.116±0.012（mg/kg）0.110（mg/kg）4砷//13.3±1.1（mg/kg）13.9（mg/kg）4铜//54±2（mg/kg）55（mg/kg）4铅//41±2（mg/kg）40.2（mg/kg）4镍//43±2（mg/kg）43（mg/kg）4镉//0.59±0.04（mg/kg）0.59（mg/kg）4六价铬//9.91±0.96（mg/kg）9.78（mg/kg）2阳离子交换量//12.5±1.1（cmol+/kg）13.0（cmol+/kg）2氯甲烷2//1氯乙烯2//11,1-二氯乙烯2//1二氯甲烷2//1反式-1,2-二氯乙烯2//11,1-二氯乙烷2//1顺式-1,2-二氯乙烯2//1氯仿2//11,1,1-三氯乙烷2//1四氯化碳2//1苯2//11,2-二氯乙烷2//1三氯乙烯2//11,2-二氯丙烷2//1第第50页共27页土壤、底泥质控数据统计表质控措施检测项目加标回收平行值质控样实验室空白数量回收率%数量相对偏差%保证值测得值数量甲苯//11,1,2-三氯乙烷//1四氯乙烯//1氯苯//11,1,1,2-四氯乙烷//1乙苯//1间，对-二甲苯//1邻二甲苯//1苯乙烯//11,1,2,2-四氯乙烷//11,2,3-三氯丙烷//11,4-二氯苯//11,2-二氯苯//1苯胺//12-氯苯酚//1硝基苯//1萘//1苯并(a)蒽//1䓛//1苯并(b)荧蒽//1苯并(k)荧蒽//1苯并(a)芘//1茚并(1,2,3-cd)芘//1二苯并(a,h)蒽//1底泥、包气带质控数据统计表质控措施检测项目加标回收平行值质控样实验室空白数量回收率%数量相对偏差%保证值测得值数量底泥pH值//21.4/0.15.130±0.1905.16/汞//33.0~5.20.116±0.012（mg/kg）0.110（mg/kg）4砷//30.6~1.613.3±1.1（mg/kg）13.9（mg/kg）4铜//3054±2（mg/kg）55（mg/kg）4铅//31.0~2.441±2（mg/kg）40.2（mg/kg）4镍//31.1~4.743±2（mg/kg）43（mg/kg）4镉//30.6~1.10.59±0.04（mg/kg）0.59（mg/kg）4铬//1092±4（mg/kg）92（mg/kg）2锌//11.4127±4（mg/kg）128（mg/kg）2包气带氟化物铅铬锌铜甲苯对二甲苯间二甲苯邻二甲苯苯乙烯以下空白检测方法及仪器一览表检测类别检测项目方法依据检出限仪器设备设备编号地表水化学需氧量水质化学需氧量的测定重铬酸盐法HJ828-20174mg/L滴定管ZQ-GW078地表水氟化物水质氟化物的测定离子选择电极法GB/T7484-19870.05mg/L台式PH酸度计PHSJ-4FZQ-IE031地表水氨氮水质氨氮的测定纳氏试剂分光光光度法HJ535-20090.025mg/L可见分光光度计T6新悦ZQ-IE015地表水总磷水质总磷的测定钼酸铵分光光度法GB/T11893-19890.01mg/L可见分光光度计T6新悦ZQ-IE015地表水铅(第四版增补版)20023.4.16（5）1.0μg/L石墨炉原子吸收分光光度计TAS-990GZQ-IE013地表水石油类水质石油类的测定紫外分光光度法（试行）HJ970-20180.01mg/L紫外可见分光光度计T6新世纪ZQ-IE016地表水六价铬水质六价铬的测定二苯碳酰二分光光度法 GB/T7467-19870.004mg/L可见分光光度计T6新悦ZQ-IE015地表水锌GB/T7475-19870.02mg/L火焰原子吸收分光光度计TAS-990FZQ-IE012地表水铜(第四版增补版)20023.4.10（5）1.0μg/L石墨炉原子吸收分光光度计TAS-990GZQ-IE013地表水甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005地表水对二甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005地表水间二甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005地表水邻二甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005地表水苯乙烯水质苯系物的测定顶空/气相色谱法HJ1067-20193μg/L气相色谱8890GCZQ-IE005海水化学需氧量海洋监测规范第4部分：海水分析碱性高锰酸钾法GB17378.4-2007（32）0.15mg/L滴定管ZQ-GW079海水氨海洋监测规范第4部分：海水分析靛酚蓝分光光度法GB17378.4-2007（36.1）0.0008mg/L可见分光光度计T6新悦ZQ-IE015检测方法及仪器一览表检测类别检测项目方法依据检出限仪器设备设备编号海水硝酸盐4GB17378.4-2007（38.1）0.0006mg/L可见分光光度计T6新悦ZQ-IE015海水亚硝酸盐4GB17378.4-2007（37）0.0003mg/L可见分光光度计T6新悦ZQ-IE015海水活性磷酸盐4GB17378.4-2007（39.1）0.0006mg/L可见分光光度计T6新悦ZQ-IE015海水六价铬水质六价铬的测定二苯碳酰二肼分光光度法GB/T7467-19870.004mg/L可见分光光度计T6新悦ZQ-IE015海水石油类水质石油类的测定紫外分光光度法（试行）HJ970-20180.01mg/L紫外可见分光光度计T6新世纪ZQ-IE016地下水钾水质钾和钠的测定火焰原子吸收分光光度法GB/T11904-19890.03mg/L火焰原子吸收分光光度计TAS-990FZQ-IE012地下水钠水质钾和钠的测定火焰原子吸收分光光度法GB/T11904-19890.010mg/L火焰原子吸收分光光度计TAS-990FZQ-IE012地下水钙水质钙和镁的测定原子吸收分光光度法GB/T11905-19890.02mg/L火焰原子吸收分光光度计TAS-990FZQ-IE012地下水镁水质钙和镁的测定原子吸收分光光度法GB/T11905-19890.002mg/L火焰原子吸收分光光度计TAS-990FZQ-IE012地下水碳酸根《水和废水监测分析方法》（第四版增补版）国家环境保护总局（2002年）酸碱指示剂滴定法3.1.12（1）5mg/L滴定管ZQ-GW079地下水碳酸氢根（第四版增补版）（2002年3.1.12（1）5mg/L滴定管ZQ-GW079地下水氯化物水质氯化物的测定 硝酸银滴定法GB/T11896-198910mg/L滴定管ZQ-GW079（F-Cl-NO2-Br-、离子色谱仪CIC-D120地下水硫酸根NO-、PO3-、SO2-、SO2-）3 4 3 40.018mg/LZQ-IE055的测定离子色谱法HJ84-2016地下水pH值水质pH的测定玻璃电极法GB/T6920-1986—台式PH酸度计PHSJ-4FZQ-IE031地下水耗氧量（CODMn）生活饮用水标准检验方法有机物综合指标GB/T5750.7-2006/1.1酸性高锰酸钾滴定法1.2碱性高锰酸钾滴定法0.05mg/L电热恒温水浴锅DK-S28ZQ-IE019地下水总硬度水质钙和镁总量的测定 滴定法GB/T7477-19875.00mg/L滴定管ZQ-GW079检测方法及仪器一览表检测类别检测项目方法依据检出限仪器设备设备编号地下水溶解性总固体GB/T5750.4-2006/8.1称量法10mg/L电子天平ATX224ZQ-IE063地下水硝酸盐氮生活饮用水标准检验方法无机非金属指标GB/T5750.5-2006/5.2紫外分光光度法0.2mg/L紫外可见分光光度计T6新世纪ZQ-IE016地下水亚硝酸盐氮水质亚硝酸盐氮的测定分光光度法GB/T7493-19870.003mg/L可见分光光度计T6新悦ZQ-IE015地下水氨氮水质氨氮的测定纳氏试剂分光光光度法HJ535-20090.025mg/L可见分光光度计T6新悦ZQ-IE015地下水六价铬5750.6-2006/10.1二苯碳酰二肼分光光度法0.004mg/L可见分光光度计T6新悦ZQ-IE015地下水铜《水和废水监测分析方法》(第四版增补版)国家环境保护总局2002年石墨炉原子吸收法3.4.10（5）1.0μg/L石墨炉原子吸收分光光度计TAS-990GZQ-IE013地下水铅《水和废水监测分析方法》(第四版增补版)国家环境保护总局2002年石墨炉原子吸收法3.4.16（5）1.0μg/L石墨炉原子吸收分光光度计TAS-990GZQ-IE013地下水锌水质铜、锌、铅、镉的测定 原吸收分光光度法GB/T7475-19870.02mg/L火焰原子吸收分光光度计TAS-990FZQ-IE012地下水甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005地下水对二甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005地下水间二甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005地下水邻二甲苯水质苯系物的测定顶空/气相色谱法HJ1067-20192μg/L气相色谱8890GCZQ-IE005环境空气氨环境空气和废气氨的测定纳氏试剂分光光度法HJ533-20090.01mg/m³可见分光光度计T6新悦ZQ-IE015环境空气硫化氢（第四版增补版）20030.001mg/m³可见分光光度计T6新悦ZQ-IE015环境空气臭气浓度空气质量恶臭的测定三点比较式臭袋法GB/T14675-199310无量纲无臭气体制备系统ZQ-IE148环境空气氯化氢环境空气和废气氯化氢的测定离子色谱法HJ549-20160.02mg/m³离子色谱仪CIC-D120ZQ-IE055检测方法及仪器一览表检测类别检测项目方法依据检出限仪器设备设备编号环境空气氟化物环境空气氟化物的测定滤膜采样/氟离子选择电极法HJ955-20180.5μg/m³台式PH酸度计PHSJ-4FZQ-IE031环境空气铅环境空气铅的测定石墨炉原子吸收分光光度法HJ539-20150.009μg/m³石墨炉原子吸收分光光度计TAS-990GZQ-IE013环境空气甲苯环境空气苯系物的测定活性炭吸附/二硫化碳解吸-气相色谱法HJ584-20100.5×10-3mg/m³气相色谱8890GCZQ-IE005环境空气对二甲苯环境空气苯系物的测定活性炭吸附/二硫化碳解吸-气相色谱法HJ584-20100.5×10-3mg/m³气相色谱8890GCZQ-IE005环境空气间二甲苯环境空气苯系物的测定活性炭吸附/二硫化碳解吸-气相色谱法HJ584-20100.5×10-3mg/m³气相色谱8890GCZQ-IE005环境空气邻二甲苯环境空气苯系物的测定活性炭吸附/二硫化碳解吸-气相色谱法HJ584-20100.5×10-3mg/m³气相色谱8890GCZQ-IE005环境空气苯乙烯环境空气苯系物的测定活性炭吸附/二硫化碳解吸-气相色谱法HJ584-20100.5×10-3mg/m³气相色谱8890GCZQ-IE005环境空气硫酸雾固定污染源废气硫酸雾的测定离子色谱法HJ544-20160.002mg/m³离子色谱仪CIC-D120ZQ-IE055环境空气甲醇（第四版增补版（2003年）6.1.6(1)0.2mg/m³气相色谱SP3420AZQ-IE009环境空气乙醇《空气和废气监测分析方法》（第四版增补版（2003年）6.1.6(1)0.2mg/m³气相色谱SP3420AZQ-IE009环境空气非甲烷总烃环境空气总烃、甲烷和非甲烷总烃的测定直接进样气相色谱法HJ604-20170.07mg/m³气相色谱GC9790IIZQ-IE010土壤pH值土壤pH值的测定电位法HJ962-2018—台式PH酸度计PHSJ-4FZQ-IE031土壤容重土壤检测第4部分:土壤容重的测定NY/T1121.4-2006—YP系列电子天平YP10002ZQ-IE034土壤阳离子交换量土壤阳离子交换量的测定三氯化六氨合钴浸提-分光光度法HJ889-20170.8cmol+/kg可见分光光度计T6新悦ZQ-IE015土壤氧化还原电位土壤氧化还原电位的测定电位法HJ746-2015—土壤ORP计TR-901ZQ-IE176土壤镉土壤质量铅、镉的测定石墨炉原子吸收分光光度法GB/T17141-19970.01mg/kg石墨炉原子吸收分光光度计TAS-990GZQ-IE013检测方法及仪器一览表检测类别检测项目方法依据检出限仪器设备设备编号土壤汞土壤质量总汞、总砷、总铅的测定原子荧光法第一部分：土壤中总汞的测定GB/T22105.1-20080.002mg/kg原子荧光光度计AFS-8220ZQ-IE003土壤砷土壤质量总汞、总砷、总铅的测定原子荧光法第二部分：土壤中总砷的测定GB/T22105.2-20080.01mg/kg原子荧光光度计AFS-8220ZQ-IE003土壤铅土壤质量铅、镉的测定石墨炉原子吸收分光光度法GB/T17141-19970.1mg/kg石墨炉原子吸收分光光度计TAS-990GZQ-IE013土壤铜土壤和沉积物铜、锌、铅、镍、铬的测定火焰原子吸收分光光度法HJ491-20191mg/kg火焰原子吸收分光光度计TAS-990FZQ-IE012土壤镍土壤和沉积物铜、锌、铅、镍、铬的测定火焰原子吸收分光光度法HJ491-20193mg/kg火焰原子吸收分光光度计TAS-990FZQ-IE012土壤六价铬土壤和沉积物六价铬的测定碱溶液提取-火焰原子吸收分光光度法HJ1082-20190.5mg/kg火焰原子吸收分光光度计TAS-990FZQ-IE012土壤四氯化碳土壤和沉积物挥发性有机物的测定吹扫捕集/气相色谱-质谱法HJ605-20111.3μg/kg气质联用仪8890-5977BZQ-IE008土壤氯仿土壤和沉积物挥发性有机物的测定吹扫捕集/气相色谱-质谱法HJ605-20111.1μg/kg气质联用仪8890-5977BZQ-IE008土壤氯甲烷土壤和沉积物挥发性有机物的测定吹扫捕集/气相色谱-质谱法HJ605-20111.0μg/kg气质联用