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1、Quotation No.:GQD140756Report No.:GSTA2014100862-23ENRandom Code:385876 Page 16 of 16 pagesTest ReportGlobal-Standard (Shanghai) Testing Technology Co., Ltd.冠标(上海)检测技术Client: Address:Shanghai Hanshi Molding Shape Co., Ltd. No. 355, YouDong Road,Shanghai, P.R ChinaDUNS:Tested Sample:Door inner with b
2、in Part Number: 1148071Sample Description:Model: OmegaMaterial and grade: PP/PE-M15 EF267AIC Manufacture Date:2014-12-08Color: BlackWeight: 150gReceiving Date:2014-12-09Evaluation Type: PV Technical Specification: TS-INT-001-2014Test Items:1 Fogging Characteristics2 Odor3 VOCs/SVOC4 Aldehyde and Ket
3、one EmissionsDate of issue:2015-03-31Test Results:According to clients requirements, the test has been conducted on received samples. Refer to page 2 for details of results.Edited by:Zhang WeiqiChecked by:Yu YaApproved by:Guo XiaofangSignature:Signature:Signature:Test SummarySection No.Clause No.Tes
4、t ItemRef. StandardEvaluationSection 001TS-INT-001-20143.2FoggingCharacteristicsGMW3235-2011PassSection 002TS-INT-001-20143.3OdorGMW3205-2011PassSection 003TS-INT-001-20143.4VOCs/SVOCGMW15634-2009PassSection 004TS-INT-001-20143.5Aldehyde andKetone EmissionsGMW15635-2012PassA14086206A14086206Sample P
5、hotosSection 001 Fogging CharacteristicsTestStandardGMW3235-2011 Method BDate of Test2014-12-11 2014-12-13TestedSample ID.A140862060304TestConditionsSee the Test Process & Test Conditions belowTest InstrumentsNo.NameTypeNumberCalibrationValid Date1Analytical BalanceBT125DEQ-00122015.06.222Fogging Te
6、sterPC201EQ-00732015.06.22Test ResultsMethodUnitMDLRequirementResultAverageVerdictMethod Bmg2.00.660.65P0.630.67TestConclusionsPassRemarkP: Pass; F: Fail; : Not ApplicableRemove circular specimens with diameters (801)mm from the sample.Then put specimens into beakers after they are dried for 24h. Th
7、ree parallel tests are taken for each sample.Put each beaker into the oil bath of 100. Place the sealing ring, weighed Aluminum foil (G0) and the cooling plate of 21successively.Heat the beaker sealed for 18h. Then, transfer the aluminum foil to the dry container.Preserve each aluminum foil in the d
8、ry container for 24h. Then take it out and weigh it, G1.Section 001 Fogging Characteristics Test Process & Test ConditionsCalculation MethodThe condensable constituents Gj=G1-G0Where: G1weight of the Aluminum foil disc after fogging test G0 weight of the Aluminum foil disc before fogging testTesting
9、Section 001 Fogging Characteristics Test PicturesSection 002 OdorTestStandardGMW3205-2011Date of Test2014-12-09 2014-12-11TestedSample ID.A140862060305TestConditionsSee the Test Process &Test Conditions belowTest InstrumentsNo.NameTypeNumberCalibrationValid Date1ConstantTemperature ChamberLC-233B1EQ
10、-00072015.09.022Analytical BalanceBT125DEQ-00122015.06.22Test ResultsMethodUnitRequirementSample SizeTest ResultsVerdictCoding ARating610cm*10cm*0.4cm6.0PCoding BRating10cm*10cm*0.4cm6.0Personnel assessmentMethodPersonABCDEFCoding A666666Coding B666766TestConclusionsPassRemark(1) P: Pass; F: Fail; :
11、 Not Applicable(2) Odor classificationRatingDescription10Odorless9Just noticeable8Noticeable, trace7Clearly noticeable, but not objectionable6Tolerable5Borderline tolerable4Objectionable3Annoying2Severe1IntolerableSection 002 OdorPut specimens in 4 L containers: Coding A: add 400ml deionized water;
12、Coding B: add no water.Store containers in a constant temperature chamber:Coding A,B: (702),(240.5)hRemove the containers from the constant temperature chamber, and cool them down to room temperature (about 1h).Perform evaluation with at least six examiners. The result is the average of the individu
13、al ratings, excluding the highest and the lowest ratings.Test Process & Test ConditionsTestingSection 002 Odor Test PicturesSection 003 VOCs/SVOCTestStandardGMW15634-2009Date of Test2014-12-10 2014-12-14TestedSample ID.A140862060306TestConditionsSee the Test Process &Test Conditions belowTest Instru
14、mentsNo.NameTypeNumberCalibrationValid Date1Analytical BalanceBT125DEQ-00122015.06.222TD-GC-MSTD100/7890A/5975CEQ-00182015.06.22Test ResultsTest ItemsUnitMDLRequirementTest ResultsVerdictVOCg/g1000556PSVOCg/g1000993PBenzeneg/g0.21N.D.PTolueneg/g0.28N.D.PEthylbenzeneg/g0.28N.D.PDimethylbenzeneg/g0.68
15、N.D.PStyreneg/g0.28N.D.PTest Result- Top10Retention Time(min)SubstanceCASResult(g/g)50.0Octadecane, 2-methyl-1560-88-975.352.2Heptacosane593-49-774.447.5Hexadecane544-76-358.052.9Hexadecanamide629-54-945.444.3Dodecane, 2,6,11-trimethyl-31295-56-437.250.4Heneicosane629-94-723.839.4Branched paraffin17
16、.348.0Branched paraffin14.445.0Branched paraffin10.048.7Octadecane593-45-38.9TestConclusionsPassRemarkN.D.: Not Detected; P: Pass; F:Fail; : Not ApplicableWeigh of sample should range from 10 to 30mg into tube with deactivated glass surface, sealed as the following. Two parallel tests are taken for
17、each sample.Section 003 VOCs/SVOC Test Process & Test ConditionsThe IM GTDT is heated to 90for 30min. The trapped VOC is analysised with GC-MS.The second thermal desorption stage is performed after VOC analysis. The same IM GTDT is heated to 120for 60min. The trapped SVOC is analysised with GC-MS.Al
18、l peaks in the corresponding chromatogram have to be integrated. The total amount of VOCs is calculated as toluene equivalent, and the total amount of SVOCs as n-hexadecane (n-C16) equivalent.Calculation MethodCalculation of the concentration in g/g (ppm) toluene and hexadecane equivalents:Emission
19、= Mass(S) Area(P) Area(S)Weight(P)Where:Area (S): Peak area in SCAN mode for the individual standard (counts)Area (P): Peak area in SCAN mode for the individual analysis or the total peak area for the calculation of the total amountMass (S): Injected mass of the individual standard in g (toluene for
20、 VOCs, nhexadecane for SVOCs)Weight (P): Weight of the sample in gramsTestingSection 003 VOCs/SVOC Test PicturesSection 004 Aldehyde and Ketone EmissionsTest.StandardGMW15635-2012Date of Test2014-12-10 2014-12-11TestedSample ID.A140862060307TestConditionsSee the Test Process & Test Conditions belowT
21、est InstrumentsNo.NameTypeNumberCalibrationValid Date1ConstantTemperatureChamberLC-233B1EQ-00082015.09.022Analytical BalanceBT125DEQ-00122015.06.223Liquid ChromatographLC1260EQ-00192015.08.30Test ResultsTest ItemsUnitMDLRequirementTest ResultsVerdictFormaldehydeg/g0.105N.D.PAcetaldehydeg/g0.100.5N.D
22、.PAcroleing/g0.050.5N.D.PAcetoneg/g0.10N.D.TestConclusionsPassRemarkN.D.: Not Detected; P: Pass; F: Fail; : Not ApplicableRemove a specimen of 410cm from the sample. Add 50mL ultra-pure water to 1L PE bottle, and attach the specimen weighed (m) to the hook. Two parts are used for determination forma
23、ldehyde.Section 004 Aldehyde and Ketone Emissions Test Process & Test ConditionsSeal and store the bottle in a heating cabinet of 60C for 3 hours, then take it out and cool it at room temperature for 1h.In an HPLC autosampler vial, mix 1mL of the test water with 1mL of derivatized solution and 100L
24、(two drops) of concentrated phosphoric acid. Shake and allow 30 minutes for the derivatization reaction to occur.The concentrations of aldehydes and ketones are determined by high performance liquid chromatography (HPLC) with ultraviolet (UV) detection.Calculation MethodAldehyde and Ketone Emissions
25、 Test - Calculation MethodThe moisture content H%:Where:H (%) = (m1 - m0 ) 100 m0m1mass of the test piece before drying (g) m0mass of the test piece after drying (g)The concentrations of aldehydes and ketones: C1 V1 V2 = 100 mL C1Where:Cald _ ket =M 0 V3M 0Cald_ketconcentration of aldehyde or ketone (g/g /g) in test sample. C1 concentration of aldehyde or ketone by HPLC ( g/mL) M0weight of the dr
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