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分析化学常用仪器英文名称玻璃漏斗Glassfunnellongstem试管testtubetesttubebrushtesttubeholdertesttuberack蒸发皿evaporatingdishsmall烧杯beaker锥形瓶Erlenmeyer量筒gradcylinder洗瓶plasticwashbottle勺皿casserole,smallstopperedflask分液漏斗separaloryfunnelwaterbath/oilbathstrringbarmagneticstirrer冷凝器condenserBallastbottle圆颈烧瓶Round-buttomflask试剂瓶reagentbottles托盘天平platform.balance台秤0.1g托盘pan指针刻度表pointerandscalecrossbeamsandslidingweights游码分析天平two-pan/single-pananalyticalbalance滴定管buretteglassbead(basic)nozzle移液管pipette胖肚elongatedglassbulb洗耳球rubbersuctionbulb玻棒glassrod玻璃活塞stopcock容量瓶pyknowmeterflasks比重瓶(one-mark)volumetricflasks胖肚吸管one-markpipette刻度吸管graduatedpipettes实验仪器清单1、柜子中四、抽屉中:锥形瓶(conicalflask)250ml×4药匙(medicinespoon)×1(Erlenmeyerflask)100ml×3滴管(driptube;dropper)×2烧杯(beaker)500ml×1玻棒(Glassstic)×2250ml×3木试管夹(testtubeclamp;testtubeholder)×1100ml×3胖肚吸管(straws)25ml×150ml×210ml×1容量瓶(volumetricflask)100ml×2乳钵(morta)×150ml×4洗耳球(earwadhingbulb)碘量瓶(iodinnumoeflask;iodineflask)500ml×3试剂瓶(reagentbottle)(无色)×2(棕色)×2配洗液:量筒(cylinder)100ml×1K2Cr2O72g+5ml水→65mlH2SO4(graduatedcylinder)10ml×1边加边搅拌(stir)。二、台面上仪器:一般仪器的洗涤(wash)铁支架(siderocradle)+蝴蝶架白瓷板(WhitePorcelainBoard)(一)清点仪器(tocount;tomakeaninventory)酸式滴定管(Acidburette)25ml×1配洗液(Lotion)碱式滴定管(Alkaliburette)25ml×1一般仪器的洗涤三、公用柜中:(二)滴定管(buret;burette)直型冷凝器(rectocondensor)×1容量瓶(volumetricflask)漏斗架(funnelstand)×2移液管(pipe)水浴锅(waterbathkettle)×1温度计(Thermometer;hygrometer;hydroscope)×1电炉(electricfurnace;electrichotplate;electricstove)四人一个《分析化学》上册第一章绪论分析化学:analyticalchemistry定性分析:qualitativeanalysis定量分析:quantitativeanalysis物理分析:physicalanalysis物理化学分析:physico-chemicalanalysis仪器分析法:instrumentalanalysis流动注射分析法:flowinjectionanalysis;FIA顺序注射分析法:sequenticalinjectionanalysis;SIA化学计量学:chemometrics第二章误差的分析数据处理绝对误差:absoluteerror相对误差:relativeerror系统误差:systematicerror可定误差:determinateerror随机误差:accidentalerror不可定误差:indeterminateerror准确度:accuracy精确度:precision偏差:debiation,d平均偏差:averagedebiation相对平均偏差:relativeaveragedebiation标准偏差(标准差):standerddeviation;S相对平均偏差:relatibestandarddeviation;RSD变异系数:coefficientofvariation误差传递:propagationoferror有效数字:significantfigure置信水平:confidencelevel显著性水平:levelofsignificance合并标准偏差(组合标准差):pooledstandarddebiation舍弃商:rejectionquotient;Q化学定量分析第三章滴定分析概论滴定分析法:titrametricanalysis滴定:titration容量分析法:volumetricanalysis化学计量点:stoichiometricpoint等当点:equivalentpoint电荷平衡:chargebalance电荷平衡式:chargebalanceequation质量平衡:massbalance物料平衡:materialbalance质量平衡式:massbalanceequation第四章酸碱滴定法酸碱滴定法:acid-basetitrations质子自递反应:autoprotolysisreaction质子自递常数:autoprotolysisconstant质子条件式:protonbalanceequation酸碱指示剂:acid-baseindicator指示剂常数:indicatorconstant变色范围:colourchangeinterval混合指示剂:mixedindicator双指示剂滴定法:doubleindicatortitration第五章非水滴定法非水滴定法:nonaqueoustitrations质子溶剂:protonicsolvent酸性溶剂:acidsolvent碱性溶剂:basicsolvent两性溶剂:amphototericsolvent无质子溶剂:aproticsolvent均化效应:differentiatingeffect区分性溶剂:differentiatingsolvent离子化:ionization离解:dissociation结晶紫:crystalviolet萘酚苯甲醇:α-naphthalphenolbenzylalcohol奎哪啶红:quinadinered百里酚蓝:thymolblue偶氮紫:azoviolet溴酚蓝:bromophenolblue第六章配位滴定法配位滴定法:compleximetry乙二胺四乙酸:ethylenediaminetetraaceticacid,EDTA螯合物:chelatecompound金属指示剂:metallochromeindcator第七章氧化还原滴定法氧化还原滴定法:oxidation-reductiontitration碘量法:iodimetry溴量法:bromimetry]溴量法:brominemethod铈量法:cerimetry高锰酸钾法:potassiumpermanganatemethod条件电位:conditionalpotential溴酸钾法:potassiumbromatemethod硫酸铈法:ceriumsulphatemethod偏高碘酸:metaperiodicacid高碘酸盐:periodate亚硝酸钠法:sodiumnitritemethod重氮化反应:diazotizationreaction重氮化滴定法:diazotizationtitration亚硝基化反应:nitrozationreaction亚硝基化滴定法:nitrozationtitration外指示剂:externalindicator外指示剂:outsideindicator重铬酸钾法:potassiumdichromatemethod第八章沉淀滴定法沉淀滴定法:precipitationtitration容量滴定法:volumetricprecipitationmethod银量法:argentometricmethod第九章重量分析法重量分析法:gravimetricanalysis挥发法:volatilizationmethod引湿水(湿存水):waterofhydroscopicity包埋(藏)水:occludedwater吸入水:waterofimbibition结晶水:waterofcrystallization组成水:waterofcomposition液-液萃取法:liquid-liquidextration溶剂萃取法:solventextration反萃取:counterextraction分配系数:partitioncoefficient分配比:distributionratio离子对(离子缔合物):ionpair沉淀形式:precipitationforms称量形式:weighingforms《分析化学》下册仪器分析概述物理分析:physicalanalysis物理化学分析:physicochemicalanalysis仪器分析:instrumentalanalysis第十章电位法及永停滴定法电化学分析:electrochemicalanalysis电解法:electrolyticanalysismethod电重量法:electtogravimetry库仑法:coulometry库仑滴定法:coulometrictitration电导法:conductometry电导分析法:conductometricanalysis电导滴定法:conductometrictitration电位法:potentiometry直接电位法:dirextpotentiometry电位滴定法:potentiometrictitration伏安法:voltammetry极谱法:polarography溶出法:strippingmethod电流滴定法:amperometrictitration化学双电层:chemicaldoublelayer相界电位:phaseboundarypotential金属电极电位:electrodepotential化学电池:chemicalcell液接界面:liquidjunctionboundary原电池:galvaniccell电解池:electrolyticcell负极:cathrode正极:anode电池电动势:eletromotiveforce指示电极:indicatorelectrode参比电极:referenceelectroade标准氢电极:standardhydrogenelectrode一级参比电极:primaryreferenceelectrode饱和甘汞电极:standardcalomelelectrode银-氯化银电极:silversilver-chlorideelectrode液接界面:liquidjunctionboundary不对称电位:asymmetrypotential表观PH值:apparentPH复合PH电极:combinationPHelectrode离子选择电极:ionselectiveelectrode敏感器:sensor晶体电极:crystallineelectrodes均相膜电极:homogeneousmembranceelectrodes非均相膜电极:heterogeneousmembranceelectrodes非晶体电极:non-crystallineelectrodes刚性基质电极:rigidmatrixelectrode流流体载动电极:electrodewithamobilecarrier气敏电极:gassensingelectrodes酶电极:enzymeelectrodes金属氧化物半导体场效应晶体管:MOSFET离子选择场效应管:ISFET总离子强度调节缓冲剂:totalionstrengthadjustmentbuffer,TISAB永停滴定法:dead-stoptitration双电流滴定法(双安培滴定法):doubleamperometrictitration第十一章
光谱分析法概论普朗克常数:Plankconstant电磁波谱:electromagneticspectrum光谱:spectrum光谱分析法:spectroscopicanalysis原子发射光谱法:atomicemissionspectroscopy质量谱:massspectrum质谱法:massspectroscopy,MS第十二章紫外-可见分光光度法紫外-可见分光光度法:ultravioletandvisiblespectrophotometry;UV-vis肩峰:shoulderpeak末端吸收:endabsorbtion生色团:chromophore助色团:auxochrome红移:redshift长移:bathochromicshift短移:hypsochromicshift蓝(紫)移:blueshift增色效应(浓色效应):hyperchromiceffect减色效应(淡色效应):hypochromiceffect强带:strongband弱带:weakband吸收带:absorptionband透光率:transmitance,T吸光度:absorbance谱带宽度:bandwidth杂散光:straylight噪声:noise暗噪声:darknoise散粒噪声:signalshotnoise闪耀光栅:blazedgrating全息光栅:holographicgraaing光二极管阵列检测器:photodiodearraydetector偏最小二乘法:partialleastsquaresmethod,PLS褶合光谱法:convolutionspectrometry褶合变换:convolutiontransform,CT离散小波变换:wavelettransform,WT多尺度细化分析:multiscaleanalysis供电子取代基:electrondonatinggroup吸电子取代基:electronwith-drawinggroup第十三章荧光分析法荧光:fluorescence荧光分析法:fluorometryX-射线荧光分析法:X-rayfulorometry原子荧光分析法:atomicfluorometry分子荧光分析法:molecularfluorometry振动弛豫:vibrationalrelexation内转换:internalconversion外转换:externalconversion体系间跨越:intersystemcrossing激发光谱:excitationspectrum荧光光谱:fluorescencespectrum斯托克斯位移:Stokesshift荧光寿命:fluorescencelifetime荧光效率:fluorescenceefficiency荧光量子产率:fluorescencequantumyield荧光熄灭法:fluorescencequemchingmethod散射光:scatteringlight瑞利光:Reyleithscantteringlight拉曼光:Ramanscatteringlight第十四章红外分光光度法红外线:infraredray,IR中红外吸收光谱:mid-infraredabsorptionspectrum,Mid-IR远红外光谱:Far-IR微波谱:microwavespectrum,MV红外吸收光谱法:infraredspectroscopy红外分光光度法:infraredspectrophotometry振动形式:modeofvibration伸缩振动:stretchingvibration对称伸缩振动:symmetricalstretchingvibration不对称伸缩振动:asymmetricalstretchingvibration弯曲振动:bendingvibration变形振动:formationvibration面内弯曲振动:in-planebendingvibration,β剪式振动:scissoringvibration,δ面内摇摆振动:rockingvibration,ρ面外弯曲振动:out-of-planebendingvibration,γ面外摇摆振动:waggingvibration,ω蜷曲振动:twistingvibration,τ对称变形振动:symmetricaldeformationvibration,δs不对称变形振动:asymmetricaldeformationvibration,δas特征吸收峰:charateristicavsorptionband特征频率:characteristicfrequency相关吸收峰:correlationabsorptionband杂化影响:hybridizationaffect环大小效应:ringsizeeffect吸收峰的强度:intensityofabsorptionband环折叠振动:ringprckeringvibration第十五章
原子吸收分光光度法原子光谱法:atomicspectroscopy原子吸收分光光度法:atomicabsorptionspectrophotometry,AAS原子发射分光光度法:atomicemmsionspectrophotometry,AES原子荧光分光光度法:atomicfluorescencespectrophotometry,AFS第十六章核磁共振波谱法核磁共振:nuclearmagneticresonance,NMR核磁共振波谱:NMRspectrum核磁共振波谱法:NMRspectroscopy扫场:sweptfield扫频:seeptfrequency连续波核磁共振:continuouswaveNMR,CWNMRFourier变换NMR:PFT-NMR,FT-NMR二维核磁共振谱:2D-NMR质子核磁共振谱:protonmagneticresonancespectrum,PMR氢谱:1H-NMR碳-13核磁共振谱:13C-NMRspectrum,13CNMR自旋角动量:spinangularmomentum磁旋比:magnetogyricratio磁量子数:magneticquantumnumber,m进动:precession弛豫历程:relaxationmechanism局部抗磁屏蔽:localdiamagneticshielding屏蔽常数:shieldingconstant化学位移:chemicalshift国际纯粹与应用化学协会:IUPAC磁各向异性:magneticanisotropy远程屏蔽效应:longrangeshieldingeffect结面:nodalplane自旋-自旋偶合:spin-spincoupling自旋-自旋分裂:spin=spinsplitting单峰:singlet,s双峰:doublet,d三重峰:triplet,t四重峰:quartet五重峰:quintet六重峰:sextet偕偶:geminalcoupling邻偶:vicinalcoupling远程偶合:longrangecoupling磁等价:magneticeqivalence自旋系统:spinsystem一级光谱:firstorderspectrum二级光谱(二级图谱):secondorderspectrumC-H光谱:C-Hcorrelatedspectroscopy,C-HCOSY第十七章质谱法质谱分析法:massspectrometry质谱:massspectrum,MS棒图:bargraph选择离子检测:selectedionmonitoring,SIM直接进样:directprobeinlet,DPI接口:interface气相色谱-质谱联用:gaschromatography-massspectrometry,GC-MS高效液相色谱-质谱联用:highperformanceliquidchromatography-massspectrometry,HPLC-MS电子轰击离子源:electronimpactsource,EI离子峰:quasi-molecularions化学离子源:chemicalionizationsource,CI场电离:fieldionization,FI场解析:fielddesorptiion,FD快速原子轰击离子源:faststombombardment,FAB质量分析器:massanalyzer磁质谱仪:magnetic-sectormassspectrometer四极杆质谱仪(四极质谱仪):quadrupolemassspectrometer原子质量单位:amu离子丰度:ionabundance相对丰度(相对强度):relativeavundance基峰:basepeak质量范围:massrange分辨率:resolution灵敏度:sensitivity信噪比:S/N分子离子:molecularion碎片离子:fragmention同位素离子:isotopicion亚稳离子:metastableion亚稳峰:metastablepeak母离子:parenion子离子:daughter含奇数个电子的离子:oddelectron含偶数个电子的离子:eveneletron,EE均裂:homolyticcleavage异裂(非均裂):heterolyticcleavage半均裂:hemi-homolysiscleavage重排:rearragement分子量:MWα-裂解:α-cleavage第十八章
色谱分析法概论色谱法(层析法):chromatography固定相:stationaryphase流动相:mobilephase超临界流体色谱法:SFC高效毛细管电泳法:highperformancecapillaryelectroporesis,HPEC气相色谱法:gaschromatography,GC液相色谱法:liquidcromatography,LC超临界流体色谱法:supercriticalfluidchromatography,SFC气-固色谱法:GSC气-液色谱法:GLC液-固色谱法:LSC液-液色谱法:LLC柱色谱法:columnchromatography填充柱:packedcolumn毛细管柱:capillarycolumn微填充柱:icroborepackedcolumn高效液相色谱法:highperformanceliquidchromatography,HPLC平板色谱法:planar平板色谱法:planechromatography纸色谱法:paperchromatography薄层色谱法:thinlayerchromatography,TLC薄膜色谱法;thiinfilmchomatography毛细管电泳法:capillaryelectrophoresis,CE分配色谱法:partitionchromatography吸附色谱法:adsorpionchromaography离子交换色谱法:ionexchangechromatography,IEC空间排阻色谱法:stericexclusionchromatography,SEC亲和色谱法:affinitychromatography分配系数:distributioncofficient狭义分配系数:partitioncoefficient凝胶色谱法:gelchromatography凝胶渗透色谱法:gelpermeationchromatography,GPC凝胶过滤色谱法:gelfiltrationchromatography,GFC渗透系数:permeationcoefficien;Kp化学键合相色谱法:chemicallybonded-phasechromatography分配系数:distributioncoefficient靛菁绿:indocyanine气相色谱-傅立叶变换红外光谱:GC-FTIR第十九章经典液相色谱法薄层色谱法:TLC吸附:adsorption活化:activation脱活性:deactivation交联度:degreeofcrosslinking交换容量:exchangecapacity薄层板:thinlayerplate展开剂:developingsolvent,developer临界胶束浓度:criticakmicolleconcentration,CMC相对比移值:relativeRf,Rr分离度:resolution,R分离数:separationnumber,SN煅石膏:Gypsum羧甲基纤维素钠:CMC-Na吸收光谱联用:TLC-UV薄层色谱-荧光联用:TLC-F薄层色谱-红外吸收光谱联用:TLC-IR薄层色谱法:TLC-MS纸色谱法:paperchromatography上行展开:ascendingdevelopment下行法展开:descendingdevelopment双向展开:twodimensionaldeveloooment第二十章气相色谱法气相色谱法:gaschromatography前延峰:leadingpeak拖尾峰:tailingpeak对称因子:symmetryfactor,fs保留时间:retentiontime保留体积:retentionvolume死时间:deadtime调整保留时间:asjustedretentiontime半峰宽:peakwidthathalfheight,W1/2orY1/2峰宽:peakwidth,W等温线:isotherm理论塔板高度:heightequivalenttoatheoreticalplate化学键合相:chemicallybondedphase丁二酸二乙二醇聚酯:polydiethyleneglycolsuccinate,PDEGS,DEGS高分子多孔微球:GDX苯乙烯:STY乙基乙烯苯:EST二乙烯苯:DVB涂壁毛细管柱:wallcoatedopentubularcolumn,WCOT载体涂层毛细管柱:supprotcoatedopentubularcolumn,SCOT热导检测器:thermalconductivitydetector,TCD氢焰离子化检测器:hydrogenflameionizationdetector,FID电子捕获检测器:electroncapturedetector,ECD噪声:noise,N漂移:drift,d灵敏度:sensitivity检测限(敏感度):detectability,D,M分离度:resolution归一化法:normalizationmethod外标法:externalstandardization第二十一章高效液相色谱法高效液相色谱法:highperformanceliquidchromatography,HPLC高速液相色谱法:highspeedLC,HSLC高压液相色谱法:highpressureLC,HPLC高分辨液相色谱法:highresolutionLC,HRLC液固吸附色谱法(液固色谱法):liquid-solidadsorptionchromatography,LSC液液色谱法:liquid-liquidchromatography,LLC正相:normalphase,NP反相:reversedphase,RP化学键合相色谱法:bondedphasechromatography,BPC十八烷基:octadecylselyl,ODS离子对色谱法:pairedionchromatography,PIC反相离子对色谱法:RPIC离子抑制色谱法:ionsuppressionchromatography,ISC离子色谱法:ionchromatography,IC手性色谱法:chiralchromatography,CC环糊精色谱法:cyclodextrinchromatography,CDC胶束色谱法:micellarchromatography,MC亲和色谱法:affinitychromatography,AC固定相:stationaryphase化学键合相:chemicallybondephase封尾、封顶、遮盖:endcapping手性固定相:chiralstationaryphase,CSP恒组成溶剂洗脱:isocraicelution梯度洗脱:gradientelution紫外检测器:ultravioletdetector,UVD荧光检测器:fluorophotomericdetector,FD电化学检测器:ECD示差折光检测器:RID光电二极管检测器:photodiodearraydetector,DAD三维光谱-波谱图:3D-spectrochromatogram蒸发光散射检测器:evaporativelightscatteringdetector,ELSD安培检测器:amperedetector,AD高效毛细管电泳法:highperformancecapillaryelectrophoresis,HPCE淌度:mobility电泳:electrophoresis电渗:electroosmosis动力进样:hydrodynamicinjection电动进样:electrokineticinjection毛细管区带电泳法:capillaryzoneelectrophoresis,CZE胶束电动毛细管色谱:micellarelectrokineticcapillarychromatography,MECC毛细管凝胶电泳:capillarygelelectrophoresis,CGE筛分:sieving绪论释药系统(drugdeliverysystem,DDS)中国药典(ChinesePharmacopoeia,ChP)美国药典(TheUnitedStatesPharmacopoeia,USP)美国国家处方集(TheNationalFormulary,NF)英国药典(BritishPharmacopoeia,BP)欧洲药典(EuropeanPharmacopoeia,Ph.Eup)国际药典(TheInternationalPharmacopoeia,Ph.Int)良好药品实验研究规范(GoodLaboratoryPractice,GLP)良好药品生产规范(GoodManufacturePractice,GMP)良好药品供应规范(GoodSupplyPractice,GSP)良好药品临床试验规范(GoodClinicalPractice,GCP)分析质量管理(AnalyticalQualityControl,AQC)第1章药物的鉴别试验药物的鉴别试验identificationtest一般鉴别试验generalidentificationtest专属鉴别试验specificidentificationtest灵敏度sensitivity最低检出量minimumdetectablequantity最低检出浓度minimumdetectableconcentration第2章药物的杂质检查巯基醋酸mercaptoaceticacid古蔡Gutzeit二乙基二硫代氨基甲酸银siliverdiethyldithio-carbamate硫酸灰分sulphatedash炽灼残渣residueonignition热重分析法thermogravimetricanalysis,TGA差示热分析法differentialthermalanalysis,DTA差示扫描量热法differentialscanningcalorimetry,DSC碱性酒石酸铜试验Fehling’sreagent异红紫酸盐isopurpurate2,3-二氨基萘2,3-diaminonaphthalene4,5-苯并苯硒二唑4,5-benzopiazselenol第三章定量分析样品前处理与测定方法的效能指标汞齐化法amalgamationmethod氧瓶燃烧法oxygenflaskcombustionmethod葡萄糖醛酸甙glucuronides硫酸酯sulphates血浆plasma血清serum全血wholeblood治疗药物浓度监测therapeuticdrugmonitoring,TDM结合bound游离free缀合物conjugate液-液提取法liquid-liquidextraction,LLE离子对试剂ionpairreagent离子对提取法ionpairextractionmethod反离子counter液-固提取法liquid-solidextractionLSE半自动样品制备系统advancedautomatedsampleprocessor,AASP烷基化alkylations酰基化acylations硅烷化silylations精密度precision标准差standarddeviation,SDorS相对标准差relativestandarddeviation,RSD变异系数coefficientofvariation,CV批内精密度within-runprecision日内精密度within-dayprecision批间精密度between-runprecision日间精密度daytodayprecision准确度accuracy定量限limitofquantitation,LOQ检测限limitofdetection,LOD选择性selectivity专属性specificity线性与范围linearityandrange重现性ruggedness耐用性robustness散布图scatterdiagram荧光偏振免疫测定法fluorescencepolarizationimmunoassay,FPIA第4章巴比妥类药物的分析溴化十六烷基三甲基苄铵cetyltrimethylbenzylammoniumbromide,CTMA氯化四癸基二甲基苄铵Tetradacyldimethybenzylammoniumchloride,TDBA第5章芳酸及其酯类药物的分析苯甲酸及其钠盐benzoicacidandsodiumbenzoate布美他尼bumetanide羟苯乙酯ethylparoben丙磺舒probenecid酚黄乙胺etamsylate第6章胺类药物的分析第七章杂环类药物的分析二硝基氯苯反应Vongerichten反应戊烯二醛反应K?nig反应第8章
生物碱类药物的分析生物碱alkaloids阿片gumopium扫尾剂tailing-suppressingreagent蒂巴因thebaine诺司卡品noscapine竞争离子competingions亲脂性lipophicity拖尾因子tailingfactor金刚烷adamantane第9章维生素类药物的分析维生素vitamin去氢维生素Adehydroretinol去水维生素Aanhydroretinol鲸醇kitol三氯化锑反应Carr-Price反应维生素B1thiaminehydrochloride;盐酸硫胺2,3,5-三苯基氯化四氮唑2,3,5-triphenyltetrazoliumchlorid,TTC红四氮唑redtetrazoline,RT蓝四氮唑bluetetrazoline,BT3,3’-二甲基氧苯基-双-4,4’-(3,5-二苯基)氯化四氮唑{3,3’-dianisole-bis[4,4’-(3,5-dipheny)tetrazoliumchloride]}有色甲……formazan铁-酚试剂iron-phenolreagent铁-柯柏试剂iron-Koberreagent第十一章抗生素类药物的分析6-氨基青霉烷酸6-aminopenicillanicacid,6-APA7-氨基头孢菌烷酸7-aminocephalosporanicacid,7-ACA氨苄西林ampicillin5-甲基-3-邻氯苯基-4-异……唑青霉素钠cloxacillinsodium羟氨苄青霉素amoxicillin氨基糖甙类抗生素aminoglycosidesantibiotics链霉素streptomycin麦芽酚maltolN-甲基葡萄糖胺反应Elson-Morgan反应坂口反应Sakaguchi反应庆大霉素gentamycin四环素类tetracyclines4-差向脱水四环素4-ejpianhydrotetracycline,EATC第十二章药物制剂分析含量均匀度contentuniformity溶出度dissulution离子对高效液相色谱法ion-pair,HPLC第十三章生化药物分析概论第十四章
中药制剂分析概论超临界流体萃取supercriticalfluidextraction,SFE过弗罗里Florisil第十五章药品质量标准的制定国际非专利药名InternationalNamesforPharmaceuticalSubstances,INN去氧麻黄碱Metamfetaminum国际理论和应用化学联合会InternationalunionofPureandAppliedChemistry,IUPAC有机化学命名原则NomenclatureofOrganicChemistry可待因Codeinum地塞米松Dexamethasonum氯……Chloroquinum青蒿素Artemisininum吗啡Morphinum苯扎溴铵BenzalkoniiBromidum1-(3,4-二羟苯基)-2-氨基乙醇重酒石酸盐一水合物[1-(3,4-Dihydroxyphenyl)-2-AminoethanolBitartratemono-hydrate]第十六章药品质量控制中的新方法与新技术填充柱packedcolumn开管柱opentubularcolumn空心柱capillarycolumn熔融石英开管柱fusedsilicaopentubularcolumn,FSOT高分辨率气相色谱法highresolutiongaschromatography,HRGC壁涂开管柱wall-coatedopentubularcolumn,WCOT柱固定化相开管柱immobilizedphaseopentubularcolumn,IPOT柱交联柱crosslinkingcolumn键合相柱bondingphasecolumn不可提取相开管柱nonextractablephaseopentubularcolumn,NPOT柱多孔层开管柱porous-layeropentubularcolumn,PLOT柱担体涂渍开管柱support-coatedopentubularcolumn,SCOT柱分流进样splitinjection不分流进样splitlessinjection柱头进样on-columninjection直接进样directinjection手性分离色谱chiralseparationchromatography,CSC普萘洛尔propranolol沙粒度胺thalidomide测定对映体enantiomer手性固定化chiralstationaryphase,CSP手性衍生试剂chiralderivatizationreagent,CDR非对映异构体diastereoisomer,DSTM配基交换型手性添加剂
chiralligand-exchangecomplexes,CLEC手性离子对络合剂chiralionpaircomplex,CIPC环糊精cyclodextrins,CD葡聚糖sephadex配基交换剂ligandexchanger手性传荷chargetransfer(R)-N-3,5-二硝基苯甲酰苯基苷氨酸dimitrobenzylphenylglycin;DNBPG三点手性识别模式three-pointchiralrecognitionmodel噻吗洛尔thimolol曲洛磷胺trofosfamide乙酰葡萄糖异硫氰酸酯(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosylisothiocyanate,GITC左旋比喹酮L-praziquantel比喹胺praziquanamine苯丙胺phenylpropamine异氰酸-α-萘酯(α-naphthylisocyanae,NI美西律mexiletine氯胺酮ketamine本芴醇benflumelol苯丙醇phenylpropanol烯丙洛尔alprenolol普萘洛尔propranolol氧烯洛尔oxyprenolol麻黄碱ephedrine毛细管电泳capillaryelectrophoresis,CE毛细管区带电泳capillaryzoneelectrophoresis,CZE胶束动电毛细管色谱mcellarelectrokineticcapillarychromatography,MECC胶束动电色谱miccellarelectrokineticchromatography,MEKC环糊精动电色谱cyclodextrinselectrokineticchromatography,CDEKC离子交换动电色谱ion-exchangeelectrokineticchromatography,IEEKC微滴乳状液动电色谱microemulsionelectrokineticchromatography,MEEKC毛细管凝胶电泳capillarygelelectrophoresis,CGE毛细管等电聚焦capillaryisoelectricfocusing,CIEF毛细管等速电泳capillaryisotachorphoresis,CITP毛细管电色谱capillaryelectrochromatography,CEC色谱响应函数chromatographicresponsefunction,CRF色谱优化函数chromatographicoptimizationfunction,COF等级色谱响应函数hierarchicalchromatographicresponsefunction,HCRF差示分光光度法differencespectrophotometry近红外光谱nearinfra-redspectrum,NIRS中红外光谱midinfra-redspectrum,MIRS合谱combinations光谱匹配法spectralmatching匹配指数matchindex,M.I.主成分分析法principalcomponentregression,PCR人工神经网络方法artificialneuralnetworks,ANN核磁共振nuclearmagneticresonance,NMR二维NMRtwodimensionalNMR六甲基三硅氧烷hexamethylcyclotrisiloxane吡嗪pyrazine普鲁卡因procaine色谱联用技术hyphenatedtechniqueschromatography,HTC接口interface重建色谱图reconstructivechromatogram命中质量系数hitqualityindex,HQI最小二乘方程序leastsquaresalgothm导数绝对值程序absolutederivativealgothm导数平方程序squarederivativealgothm空心柱opentubularcolumn,OTC总离子流totalioncarrent,TIC选择性离子监测xelectedionmonitoring,SIM多离子检测multipleiondetection,MID质量碎片图谱法massfragmentography冰片borneal川芎嗪tetramethyloyrazine,TMP电子轰击离子化electronimpactionization,EI化学离子化chemicalionization,CI场解吸fielddesorption,EI快原子轰击fastatombombardment,FAB热喷雾thermospray,TSP电喷雾electrospray,ESP大气压离子化atmosphericpressureionization,API粒子束接口particalbeam动态快原子轰击法FAB离子喷雾接口ISP电子喷雾法ESP大气压离子化接口API大气压化学电离APCI串联质谱MS-MS丽江山慈姑IphigeniaindicaKunthetBenth托非索泮tofisopam色谱字典\术语大全中文英文色谱图chromatogram色谱峰chromatographicpeak峰底peakbase峰高h,peakheight峰宽W,peakwidth半高峰宽Wh/2,peakwidthathalfheight峰面积A,peakarea拖尾峰tailingarea前伸峰leadingarea假峰ghostpeak畸峰distortedpeak反峰negativepeak拐点inflectionpoint原点origin斑点spot区带zone复班multiplespot区带脱尾zonetailing基线baseline基线漂移baseline
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