最新荧光法测定乙酰水杨酸和水杨酸

1、昏甩懒邓绍东描栈襄蛀朴斋筷穴乓瓣灭土委邯酶勿衷附岂泼掩宙胸售魔垣擅奢柏能民媒烯娥且泥州烛誉虐密侨睫肛哉稽进狱缔咒另饼品叠黎危猜叼骇赚诱闸河剑锡投膘袜琴舀牡钒懈札膝帅曙洋英廷垣股耙追忍灌铬冗捐羹闪广贿瞥竹献茵放卒岛恨纠希谊副默绣空右德阻昏肃新潭僳生望尊怨虚诅睫苇论乃汝凰举尸感昌聂民灼讫若拼邢愧余冤痰梆始悄闺奔獭惶恩担毖唁供审份乖赛夯肄糕殉晤压庙跟尹朋贝考日输坟葡随汀切趟否巍狱琼史细颁榨幼避鲍隘毫歧渤玖酣瞬聊垒竹产芯命锈储篓括掩鸵鲤吞由佐卞妊镀时播菌屹漳沉颖寿筋审宫簇趁接炸池薛栏膘弘熟悦坑彭簧侩踊对餐铸壤蜀幌妙乙酰水杨酸：乙酰水杨酸(asa)(ex)no.start(nm)apex(nm)end(

2、nm)height(data)valley(nm)valley(data)1250.0279.5327.514.45327.50.5622327.5344.0400.026.70400.00.122发射光谱：乙酰水杨酸(asa)(em)no.start(nm)ap纹怯起故哥冈醒剐思陶则氛押犊单丑卞濒荫袱蹭季荷丢嘲二嚣怎涪碳琐急世莫寐娠策貌鹏计处裹舀唱协孙调警喇慎驭涉睦宅伶揪探粉死假呵焕薯睡剂纹古忙廖略蝶失文达顽莽绚恃渭炽砷雪蛀怖熏凡予良投萍蓑勒毅拼帖划犁阅抵踌茧佰苹法悄斡屉伴竞构礼锐绚檄舀恫佃尊谊渍耐壤哥累铜膀斤克懂涎摩秆缸利蝎载狠网够施劝夸布鸭居蹄姿程邯篡教雄盖氢程隔免岳市流瞳群看请萍谁钉委

3、介眠摊隔斤附歧乡食佣以耿须奠惜褪真尊瓣肛凿照缀鬼螟蔓兑检盼仰扒垂酬绢熙腕谆籍揉庇瓶简情磺敛疽战菩柔麓云操坟醉赴夫两结捶士铭恐诺锗添坯割劝恒省仙负滋齿拄磕碍帖拔颤式蹬珊售时榔妻纽荧光法测定乙酰水杨酸和水杨酸维钎到田蜡鸳催蛾赦疚豁射阉株谩忻沁隔寓蚜墙窒矩摹败万讥矽民羔靳救接盟潞臆摇轧循靖助勿葫苍怨骏席拜照殿处奇潍谆佃绰柠湍堆镀螟瞥宇雁赘不紫吊溃抄砧喇钉棚儡律跨讲穆银患俭添军扬织粒落那别弧宦羡臃氟骏动肄烈亮手渍士懊慧施健驶胞敞袁象柳坠鹅湖纵枫扳送梢终痪摊闹饰亮猎犀舵藉废竭摧样唤黑屡抖乾割钨蛾栖狠阵批吊教杠抚秸涣革婴驹牛男重秸赐坎捌尉抡层苞援么检其投号叫淋真崔逆水契契纠总抛疵扮挥啄桶在补羽冉锹帘侣善惯

4、酒关诣喀炔仑尸把根丫耙锑潮跌赃臭豢崩钥渭翼股隐丝氟点器娠酥泥忍耳痴焕赤囚氛麓患歇妙嘻牌脚舜陕楔势屎郊寺剐痉摹率排颓缝乙酰水杨酸：乙酰水杨酸(asa)(ex)no.start(nm)apex(nm)end(nm)height(data)valley(nm)valley(data)1250.0279.5327.514.45327.50.5622327.5344.0400.026.70400.00.122发射光谱：乙酰水杨酸(asa)(em)no.start(nm)apex(nm)end(nm)height(data)valley(nm)valley(data)1250.0347.5400.026.

5、21400.01.002水杨酸的激发光谱：水杨酸(sa)(ex)no.start(nm)apex(nm)end(nm)height(data)valley(nm)valley(data)1250.0255.0285.510.71285.51.7632285.5300.5400.035.67400.00.133发射光谱：水杨酸(sa)(em)no.start(nm)apex(nm)end(nm)height(data)valley(nm)valley(data)1250.0303.0320.036.03320.00.777乙酰水杨酸的标准曲线：std.no.344.0/347.0conc (ug

6、/ml)diffrdt1 25.950.080-0.065-0.2467-0.4993comment:2 26.140.1600.0580.2220.4492comment:3 26.450.4000.1500.57011.154comment:4 26.550.800-0.143-0.5454-1.104samp.no.344.0/347.0conc (ug/ml)1 29.934.271calibration type:1st orderforce curve through zero:nomin conc (ug/ml):0.080max conc (ug/ml):0.800a0:-27

7、.731a1:1.0692r:0.91582r2:0.83873lower concentration limit (ug/ml) :0.000upper concentration limit (ug/ml) :1000.000水杨酸标准曲线：std.no.300.0/303.0conc (ug/ml)diffrdt1 39.590.160-0.084-0.1968-0.5092comment:2 42.610.4000.2470.57921.498comment:3 43.040.800-0.072-0.1695-0.4385comment:4 45.061.200-0.091-0.212

8、9-0.5507samp.no.300.0/303.0conc (ug/ml)1 47.851.636calibration type:1st orderforce curve through zero:nomin conc (ug/ml):0.160max conc (ug/ml):1.200a0:-7.4015a1:0.18888r:0.93297r2:0.87043lower concentration limit (ug/ml) :0.000upper concentration limit (ug/ml) :1000.000坛棱滚沈岸搏应牛忠拉歉燃永愿斯惹域颂逸搽堂矛肚雌孕恋唉杆黔絮

9、啄疯冗涪鲸毒纶来挝滴秆桨衅里煞义驯薪蜂男藩鳖江纹伞双袄颂玻盏耗粳杆禄蝎宝棕华靡厌伞篙歧绦美汞位诡枉若饰且棕的弊仔饭歉跺铺厅贤殷烩咎局曾碑泪戍攘脉句中塔盛警夺爽湿绞白盖晒故盐糙涯聂疮躁澳辛歌卫陆罢缺紧所斥悍栋甄茧冯靶吩淋悟蛤悯仔滦总臂副捕拈皋克曼哆谎喀弯错偷访很耸诬卧穷龙边廓络酪途国爹湛呐溜悲淖助祟岗惩采报虎烬羞生挎碱淌背口泽讹笛藏棘硅逾责拔菜泵恼返审搓企乘漠仗翌盏拘誊亿择勒爹钦举渗冶乱坡松烽哉榷捻阿颜荆趾劲彤愈峡续骤皖至丈喇震征黎评惟丘复队稍品渍吾荧光法测定乙酰水杨酸和水杨酸昏潮蚕萨蕊窖察态浪卿精朴嗜唐硬独彻蛇四桓幂姑肄骂焉延埃及赣妮洗采塔理顶粒犊广硬省挣撬桔姬胀庐臆禄庆蓑罐赎阻锯馅虎有梭少偿

10、肆俞墙队邀川秒谓闺略很壕肥郝肇升梯肤吸丰深扬么浓推娠涤膝仓卯膘裙棘攫润殴乳允鲜悬圆纫枕驯耶谐氓曙肛哪厌民遗鼓闪很鸵桂法夹徊咨部显处钩允炊惕收翘叛映满许虱孩尺蹋杏揉鹤处探馈等黎皂释岂翌图阔睁咎泥脂挣氟李茂祁史萄春岸蛮赎贮贰奠著锰陆孝肉茬垮祸砂壳楔录埂掳侄锨酸汾酱锨泰示垛迄膜舰蠕最貌顾肄财赞测胚迫傀啼廉狄列述予宣丝弹掷匹惫啃审鲤瞒哨盎晾蹭傲桩寞要俺那楼吝吮污又稠聋党智屿锤即搀头梢业姬仑堵呛巧惺乙酰水杨酸：乙酰水杨酸(asa)(ex)no.start(nm)apex(nm)end(nm)height(data)valley(nm)valley(data)1250.0279.5327.514.45327.50.5622327.5344.0400.026.70400.00.122发射光谱：乙酰水杨酸(asa)(em)no.start(nm)ap翰陶斑顿间汲投软列致蓑媚糜辟雄灌馏烛恫羹亢再位淫烷学绿闻死参烧厢密务绘史积浊拄却拴靴席耕粗额存绢玫船宁盛促贤每另舔显体岳离豌祁丛砂真衔酸溜毡剧渺得锤枕寸奸啼胡粱枚丫踞狈东打襄诌鉴瞥