S2RangerEDXRFMaintenanceRemark

1、S2 Ranger EDXRF Maintenance Remark2012.08Introduction 1. What is the S2 Ranger: EDXRF/From Na to U/Measures all elements simultaneously using an energy dispersive detector(Flash SDD) 2. Key differences of the S2 Ranger: Self contained instrument/integrated PC and touch screen/all software install in

2、side, no need a extra PC/Start,Stop,Measurement etc with touch screen/no extra cooling water needed/allow the user measure mixed batches of liquids and solidsIntroduction 3. Modem Support: troubleshooting and diagnosis is possible from remote serviceIntroduction 4Introduction 5. S2 Main power supply

3、Introduction 6. Status indicator on S2 main power supplyAdventage 1. No Goniometer(Theta/2Theta etc) 2. No Crystal Changer 3. No moving parts 4. Low power consume 5. Easy installation & make a move 6. Lowest failure rateControl Electronics 1. A20B203 BackplaneControl Electronics 2. A20B223 USBCo

4、ntrol Electronics 3. A20B205 Pressure boardControl Electronics 4. A20B202 Stepper motor boardControl Electronics 5. A20B211(Magnet & Filter board)Control Electronics 6. A20B204 DC Motor boardControl Electronics 7. A20B205 Safety boardControl Electronics 8. A20B208 Temperature boardControl Electr

5、onics 9. A20B207 HV boardControl Electronics 10. A20B206 Pressure Sensor boardControl Electronics 11. A20B209 Mains input boardAtmospheric Handling System 1. Atmospheric handling systemAtmospheric Handling System 2. Manifold and sensorAtmospheric Handling System 3. He valve and He gas inlet valveAtm

6、ospheric Handling System 4. He inlet & pressure sensor feed on sample chamberSample Chamber & Handling 1. Diagram of the Analysis Chamber A20B1Sample Chamber & Handling 2. Diagram of the Shutter Chamber A20B2Sample Chamber & Handling 3. X-DriverSample Chamber & Handling 4. Y-Z Dr

7、iverX-Ray Control & Safety 1. X-Ray Control systemDetector & Counting 1. X-Flash DetectorDetector & Counting 2. X-Flash Detector ElectronicsDetector & Counting 3. Location of detector & MIN-SVES2 Troubleshooting 1. Log file: Save to D:S2ResultsLogs 2. ActivityX.log: contain all o

8、f the information about the actions that the S2 is performing. 3. MainX.log: contain a summary of the actions that S2 is performing. 3. tmprt_N.log-temperature 4. pres_N.log-pressure 5. filt_N.log-filter 6. srce_N.log-source 7. Rt_Cal.log-Copper Disk Calibration historyS2 Troubleshooting 1. Safety C

9、ircuit Test StepS2 Troubleshooting 1. Safety Circuit Test StepS2 Start-up procedure 1. Safety board & internal safety circuit test 2. Sample Handling test 3. Chamber CheckS2 Registry Reference 1. S2Server Registry Reference 1.1 HKEY_Current_UserSoftwareS2Analysis 1.2 HKEY_Current_UserSoftwareS2F

10、ilter 1.3 HKEY_Current_UserSoftwareS2In2k 1.4 HKEY_Current_UserSoftwareS2Machine 1.5 HKEY_Current_UserSoftwareS2Method Times 1.6 HKEY_Current_UserSoftwareS2Pressure 1.7 HKEY_Current_UserSoftwareS2Safety 1.8 HKEY_Current_UserSoftwareS2Sample Handler 1.9 HKEY_Current_UserSoftwareS2SourceS2 Registry Re

11、ference 1. S2Server Registry Reference 1.10 HKEY_Current_UserSoftwareS2Temperature 1.11 HKEY_Current_UserSoftwareS2Tray 2. Explorer Registry Reference 2.1 HKEY_Current_UserSoftwareBruker AXSSplashS2Autostart 2.2 HKEY_Current_UserSoftwareBruker AXSSplashS2 Program S2 Registry Reference 3. S2Client Re

12、gistry Reference 3.1 HKEY_Current_UserSoftwareBruker AXSS2ClientGraph Options 3.2 HKEY_Current_UserSoftwareBruker AXSS2ClientLocale 3.3 HKEY_Current_UserSoftwareBruker AXSS2ClientMCA 3.4 HKEY_Current_UserSoftwareBruker AXSS2ClientNetwork 3.5 HKEY_Current_UserSoftwareBrukerr AXSS2ClientOutput Options

13、 3.6 HKEY_Current_UserSoftwareBruker AXSS2ClientTemperaturesS2 Wiring LayoutHow to Enter WindowsToolsSystem ToolsServer CommandsExecuteserverClick ExecuteToolsSystem ToolsServer CommandsExecutelaunch commandExecute then go to DOS Command PromptToolsSystem ToolsServer CommandsAnalyse-Can bypass the w

14、armup(20min)ToolsSystem ToolsServer CommandsSet(item,var)-Can set the vacuum valueToolsSystem ToolsServer CommandsLoad(pos)-Can load a sampleToolsSystem ToolsMachine OperationsHome-Initialize Sample Handler进入Windows的方法：ToolsSystem ToolsServer CommandsExecutelaunch controlExecute then go to WindowsS2

15、 Conditioning Advice 1. Air Condition 2. UPS 3. Clean room 4. External PC 5. GroundS2 Advice Detector1. Two type of detector: LE Flash SDD/Flash2. LE Flash SDD: 0.3um聚合物(C2205N2H14) 3. Flash SDD: 8um Be Window4. Replace LE Flash SDD with Flash SDDInnovation with IntegrityS2 Ranger User Names and Pas

16、swords12/15/2021Innovation with IntegrityInnovation with IntegrityUser name = AdminPassword = adminUser name = ManagerPassword = managerUser name = IUserPassword = iuserUser name = UserPassword = userSpectraEDX User Login12/15/2021Innovation with IntegrityInnovation with IntegrityUser Name = adminPa

17、ssword = passS2 Ranger User Login (touchscreen)12/15/2021Innovation with IntegrityInnovation with IntegrityCurrentUser name = servicePassword = XRF-ServicePreviousUser name = devPassword = quitS2 Ranger Service Login (touchscreen)12/15/2021Innovation with IntegrityInnovation with IntegrityCurrentPas

18、sword = XRF-ServicePreviousPassword = Mupp4tS2 Ranger Exiting to Windows (ETW)12/15/2021Innovation with IntegrityInnovation with IntegrityCurrentUser name = s2Password = Spectra+PreviousUser name = s2Password = s2S2 Ranger SPBrowser12/15/2021Innovation with IntegrityInnovation with IntegrityPassword

19、 = baxsS2 Ranger Unlock Safety Board Password12/15/2021Innovation with IntegrityInnovation with IntegrityRight Click on Settings and choose unlockPassword = adminS2 Ranger Results Engine Password12/15/2021Innovation with IntegrityInnovation with IntegrityUsername = brukerPassword = brukerUsername =

20、s2Password = s2PC Anywhere Password12/15/2021Innovation with IntegrityS2 Maintenance 1. 准备工作 2. Spare Parts 3. Year maintenanceS2 MaintenanceS2 Ranger Annual Maintenance S2 年年 度维护及度维护及 保保 养养 CUSTOMER:_ MACHINE:_ SAP No.:_ 告知用户：告知用户：由于保养涉及仪器内部的一些光路部分，有可能使仪器光路部分在保养前后发生变化，导致原来的由于保养涉及仪器内部的一些光路部分，有可能使仪器光

21、路部分在保养前后发生变化，导致原来的工作曲线与保养后的仪器状态工作曲线与保养后的仪器状态不完全一致不完全一致，我们将通过仪器重校正来解决，有时用户设定的重校正，我们将通过仪器重校正来解决，有时用户设定的重校正样品是用户自己的标样，所以请用户事先准备好这些标样，以避免保养过后样品测试数据误差偏大。样品是用户自己的标样，所以请用户事先准备好这些标样，以避免保养过后样品测试数据误差偏大。保养中所需更换的材料，请用户事先准备并到货。保养中所需更换的材料，请用户事先准备并到货。 保养操作之前，首先检查如下内容：保养操作之前，首先检查如下内容： 1. 仪器动作功能：从loader送进样品，仪器是否能够正常

22、动作。2. 样品室真空度：先将光谱室置为空气状态，等待半小时以上，再由空气状态开始抽真空，在软件上观察真空度，记录达到真空状态时所耗时间T及半小时后所达到的真空值S2 Maintenance3. X射线状态： 设定到最大功率，保持半小时，是否正常：4. Cu片校正，检查探测器的峰位及能量分辨率（Cu=8035-40ev, R=0.50-0.60）是否正常5. BAXS-S2标样校正及测量，是否与出厂数据符合6. 半定量测试： 用半定量方法测试BAXS-S2样品，测试结果记录下来。与出厂数据比较，检查是否在正常范围之内7. 定量分析： 用户工作曲线测试用户标样，检查结果是否在正常范围内 清洁清洁

23、： 1. 样品室：清扫吸尘，样品室盖板密封圈检查,必要时进行更换。2. 控制柜：电路板清灰吸尘，每个电路板都要插拔。3. 仪器内部：风扇叶，内部部件表面，风冷散热器。4. 各光电传感器：清洁进样器各轴的初始化位置的传感器，清洁晶体转换器电机上的位置传感器。5. 样品杯：用酒精棉球擦拭清洁。S2 Maintenance检查与更换检查与更换： 1. 真空系统：a. 更换真空泵油(请注意：使用一年后真空泵油一定要进行更换，否则真空泵可能比较容易漏油)b. 更换过滤器（视用户仪器样品类型及仪器使用频率等具体情况确定是否需要更换）c. 更换O型圈及抹真空脂。2. 进样器：进样器位置检查，是否所有的位置样

24、品杯都能被抓起，有必要则调整位置。机械手传感器清洁3. Shutter： a. 开关动作测试 b. 传感器位置检测4. Filter： a. 拆卸 b. 灰尘清理 c. 润滑5. X光管： a. 拆卸 b. 光管头清洁c. 安全电路触点处理（打磨、抛光）6. Detector: a. 拆卸 b. Be窗口检测c. 必要时对Be窗口进行清理 d. 对LE Flash SDD，不能使用溶剂/固体部件进行清理，可以使用洗耳球轻轻吹S2 Maintenance保养后仪器测试保养后仪器测试： 1. 仪器动作功能： 对28位系统, 使用软件进样，检查仪器是否能够进行样品测试工作。对手动进样系统, 放置一个

25、样品进行测试检查 2. 真空检测： 由于真空在作保养时完全暴露在空气中，而维护中有对各密封圈可能会使用密封脂，所以本测试与保养前使用步骤略有不同，先由空气状态开始抽真空，观察真空度，达到真空状态后需要保持半小时以上，然后再将系统放回到空气状态，等5分钟后再抽真空，达到真空状态后20分钟再转到空气状态， 等待半小时。开始抽真空，并记录：达到真空状态时所耗时间T及半小时后所达到的真空值V, 要求T 与V要优于或相当于保养前的值，否则查找原因。3. X射线/高压检查： 设定X射线到额定功率，保持半小时，是否正常：4. Cu片校正： 峰位Cu(8035-8045)ev (Cu Kalpha) 分辨率 R(0.50-0.60)(Resolution)S2 Maintenance 5. 半定量测试： 用半定量方法测试BAXS-S2样品， 如果超差，则需要对仪器进行漂移校正。漂移校正结束后还需要对BAXS-S2样品再