化学反应工程实验数据处理

1、李贺 19112211实验：连续均相反应器停留时间分布的测定实验装置及流程：实验数据记录流量：20L/H 示踪剂注入量：3ml釜ABC单釜平均t/s100.81182.9293.68139.4方差0.760.310.010.6釜数1.313.2678.281.66流量：20L/H 示踪剂注入量：4ml釜ABC单釜平均t/s113.96190.5322.44149.18方差0.720.28-0.050.52釜数1.393.52-21.61.91流量：15L/H 示踪剂注入量：4ml流量：15L/H 示踪剂注入量：3ml实验：液固催化反应动力学测定温度/初始PH初始碱浓度/(mol/L)NaOH流

2、量/(m3/h)酯流量/(m3/h)最终PH最终碱浓度/(mol/L)27.411.850.0070794584.28.8210.440.00027542311.850.0070794585.2511.1310.690.00048977911.850.0070794586.5113.8610.850.00070794637.511.850.0070794584.28.8210.260.0001819711.850.0070794585.2511.1310.420.00026302711.850.0070794586.5113.8610.540.00034673735.012.10.012589

3、2545.2511.1310.420.00026302712.10.0125892546.5113.8610.540.00034673745.011.80.0063095734.28.829.948.70964E-0511.580.0038018945.2511.539.999.77237E-0511.580.0038018946.5113.869.989.54993E-0555.010.90.0007943284.28.827.442.75423E-0710.880.0007585785.2511.537.11.25893E-0710.840.0006918316.5113.866.918.

4、12831E-08温度/CA0/CAtk27.425.703957837.33333E-0561000014.454397715.86667E-05104.73118E-0535.047.863009235.86667E-05100000036.307805484.73118E-0537.538.90451457.33333E-0572000026.915348045.86667E-0520.417379454.73118E-0545.072.443596017.33333E-05130000038.90451455.86667E-0539.810717064.73118E-0555.0288

5、4.0315037.33333E-05-2200000006025.5958615.86667E-058511.3803824.73118E-05温度T/K温度倒数1/T(K-1)k'lnk'300.550.00332723361000013.32121424308.150.003245173100000013.81551056310.650.00321905772000013.48700649318.150.003143171130000014.07787482328.150.003047387-220000000无解实验：气升式环流反应器流体力学及传质性能的测定H0=942

6、mmH=948mm时间t/s流量L/(kg/h)导电率时间t/s流量L/(kg/h)导电率020000.1291420000.1540.520000.12914.520000.156120000.1041520000.1561.520000.10415.520000.156220000.1041620000.1632.520000.08616.520000.163320000.0861720000.1693.520000.13517.520000.169420000.1351820000.1684.520000.21318.520000.168520000.2131920000.1665.52

7、0000.20419.520000.166620000.2042020000.1616.520000.18220.520000.161720000.1822120000.1627.520000.13721.520000.162820000.1372220000.1648.520000.14422.520000.164920000.1442320000.1669.520000.16123.520000.1661020000.1612420000.16610.520000.18124.520000.1661120000.1812520000.16411.520000.17725.520000.16

8、41220000.1772620000.16312.520000.16426.520000.1631320000.1642720000.16313.520000.154时间t/s电压U/VUmax-U*ln(Umax-U*)/(Umax-U)时间t/s电压U/VUmax-U*ln(Umax-U*)/(Umax-U)83.411.9012310.84.50.9724610038.53.411.90123.510.84.50.97246100393.511.80.00843886912410.84.50.9724610039.53.511.80.008438869124.510.74.60.950

9、482097103.611.70.01694955812510.74.60.95048209710.53.611.70.016949558125.510.74.60.950482097113.611.70.01694955812610.74.60.95048209711.53.611.70.016949558126.510.64.70.928975891123.611.70.01694955812710.64.70.92897589112.53.411.90127.510.74.60.950482097133.411.9012810.74.60.95048209713.53.611.70.01

10、6949558128.510.94.40.994933859143.611.70.01694955812910.94.40.99493385914.53.611.70.016949558129.510.94.40.994933859153.611.70.01694955813010.84.50.97246100315.53.711.60.025533302130.510.84.50.972461003163.711.60.02553330213110.94.40.99493385916.53.611.70.016949558131.510.94.40.994933859173.611.70.0

11、16949558132114.31.01792337717.53.611.70.016949558132.5114.31.017923377183.611.70.01694955813311.14.21.04145387518.53.611.70.016949558133.511.14.21.041453875193.611.70.01694955813411.24.11.06555142619.53.811.50.034191365134.511.24.11.065551426203.811.50.03419136513511.24.11.06555142620.53.711.60.0255

12、33302135.511.24.11.065551426213.711.60.02553330213611.24.11.06555142621.53.711.60.025533302136.511.24.11.065551426223.711.60.02553330213711.24.11.06555142622.53.711.60.025533302137.511.24.11.065551426233.611.70.01694955813811.24.11.06555142623.53.611.70.016949558138.511.24.11.065551426243.711.60.025

13、53330213911.24.11.06555142624.53.711.60.025533302139.511.341.090244039253.711.60.02553330214011.341.09024403925.53.711.60.025533302140.511.43.91.115561847263.611.70.01694955814111.43.91.11556184726.53.611.70.016949558141.511.43.91.115561847273.811.50.03419136514211.43.91.11556184727.53.811.50.034191

14、365142.511.341.090244039283.811.50.03419136514311.341.09024403928.53.811.50.034191365143.511.341.090244039293.811.50.03419136514411.341.09024403929.53.811.50.034191365144.511.43.91.115561847303.811.50.03419136514511.43.91.11556184730.5411.30.051735674145.511.53.81.14153733331411.30.05173567414611.53

15、.815411.30.051735674146.511.53.81.14153733332411.30.05173567414711.53.8154.111.20.060624622147.511.53.81.141537333334.111.20.06062462214811.63.71.1682055833.54.3110.078643127148.511.63.71.16820558344.3110.07864312714911.63.71.1682055834.54.3110.078643127149.511.63.71.168205

16、58354.3110.07864312715011.73.61.19560455535.54.3110.078643127150.511.73.61.195604555364.3110.07864312715111.93.41.25276296836.54.410.90.087775611151.511.93.41.252762968374.410.90.08777561115211.83.51.22377543237.54.510.80.096992266152.511.83.51.223775432384.510.80.09699226615311.93.41.25276296838.54

17、.810.50.125163143153.511.93.41.252762968394.810.50.12516314315411.93.41.25276296839.54.810.50.125163143154.511.93.41.252762968404.810.50.12516314315511.93.41.25276296840.54.810.50.125163143155.511.93.41.252762968414.910.40.13473259415611.93.41.25276296841.54.910.40.134732594156.511.93.41.25276296842

18、5.110.20.1541506815711.93.41.25276296842.55.110.20512.92.41.601069663435.49.90.18400364315812.92.41.60106966343.55.49.90.184003643158.512.82.51.560247668445.110.20.1541506815912.82.51.56024766844.55.110.20512.72.61.521026955455.3100.17395330716012.72.61.52102695545.55.3100.

19、173953307160.512.72.61.521026955465.3100.17395330716112.72.61.52102695546.55.3100.173953307161.513.12.21.68808104475.69.70.20441251516213.12.21.6880810447.55.69.70.204412515162.511.83.51.223775432485.69.70.20441251516311.83.51.22377543248.55.69.70.204412515163.512.72.61.521026955495.69.70.2044125151

20、6412.72.61.52102695549.55.79.60.214775302164.512.82.51.560247668505.79.60.21477530216512.82.51.56024766850.55.89.50.225246602165.512.82.51.560247668515.89.50.22524660216612.82.51.56024766851.55.89.50.225246602166.512.82.51.560247668525.89.50.22524660216713.22.11.73460105552.569.30.246524167.513.22.1

21、1.7346010555369.30.24652416812.92.41.60106966353.56.29.10.268263987168.512.92.41.601069663546.29.10.26826398716913.12.21.6880810454.56.29.10.268263987169.513.12.21.68808104556.29.10.26826398717013.12.21.6880810455.56.48.90.290487123170.513.12.21.68808104566.48.90.29048712317112.92.41.60106966356.56.

22、48.90.290487123171.512.92.41.601069663576.390.279313823172132.31.64362927757.56.390.279313823172.5132.31.643629277586.390.27931382317313.12.21.6880810458.56.390.279313823173.513.12.21.68808104596.48.90.29048712317413.12.21.6880810459.56.48.90.290487123174.5132.31.643629277606.58.80.301786679175132.3

23、1.64362927760.56.58.80.301786679175.5132.31.643629277616.68.70.313215374176132.31.64362927761.56.68.70.313215374176.512.82.51.560247668626.68.70.31321537417712.82.51.56024766862.56.68.70.313215374177.512.82.51.5602476686378.30.36028288517812.82.51.56024766863.578.30.360282885178.512.72.61.5210269556

24、46.98.40.34830669417912.72.61.52102695564.56.98.40.348306694179.512.72.61.5210269556578.30.36028288518012.72.61.52102695565.578.30.360282885180.512.72.61.5210269556678.30.36028288518112.72.61.52102695566.57.18.20.372404246181.513.321.78339122677.18.20.37240424618213.321.7833912267.57.28.10.384674338

25、182.513.41.91.834684514687.28.10.38467433818313.41.91.83468451468.57.380.397096858183.513.41.91.834684514697.380.39709685818413.41.91.83468451469.57.380.397096858184.513.41.91.834684514707.380.39709685818512.62.71.48328662770.57.57.80.422414666185.512.62.71.483286627717.57.80.42241466618613.41.91.83

26、468451471.57.67.70.435318071186.513.41.91.834684514727.67.70.43531807118713.321.7833912272.57.77.60.448390153187.513.321.78339122737.77.60.44839015318813.51.81.88875173573.57.67.70.435318071188.513.51.81.888751735747.67.70.43531807118913.321.7833912274.57.67.70.435318071189.513.321.78339122757.77.60

27、.44839015319013.41.91.83468451475.57.77.60.448390153190.513.41.91.834684514767.77.60.44839015319113.51.81.88875173576.57.77.60.448390153191.513.51.81.888751735777.87.50.4616353819213.51.81.88875173577.57.87.50.46163538192.513.51.81.8887517357887.30.48866405219313.51.81.88875173578.587.30.48866405219

28、3.513.51.81.8887517357987.30.48866405219413.51.81.88875173579.587.30.488664052194.513.61.71.945910149808.27.10.51644361619513.61.71.94591014980.58.27.10.516443616195.513.71.62.006534771818.27.10.51644361619613.71.62.00653477181.58.27.10.516443616196.513.61.71.945910149828.27.10.51644361619713.61.71.

29、94591014982.58.27.10.516443616197.513.71.62.006534771838.46.90.54501698919813.71.62.00653477183.58.46.90.545016989198.513.91.42.140066163848.46.90.54501698919913.91.4258.56.80.559615788199.513.81.52.071073292858.56.80.55961578820013.81.52.07107329285.58.66.70.574430874200.513.81.52.0710

30、73292868.66.70.57443087420113.81.52.07107329286.58.76.60.589468751201.513.81.52.071073292878.76.60.58946875120213.91.4258.76.60.589468751202.513.91.42.140066163888.76.60.58946875120314.11.22.29421684388.58.76.60.589468751203.514.11.22.294216843898.76.60.589468751204141.32.21417413689.58

31、.76.60.589468751204.5141.32.214174136908.76.60.58946875120513.91.4258.76.60.589468751205.513.91.42.140066163918.76.60.58946875120613.81.52.07107329291.58.86.50.604736223206.513.81.52.071073292928.86.50.604736223207141.32.21417413692.58.86.50.604736223207.5141.32.214174136938.76.60.58946

32、8751208141.32.21417413693.58.76.60.589468751208.5141.32.214174136948.76.60.58946875120913.91.4258.76.60.589468751209.513.91.42.140066163958.86.50.60473622321013.91.4258.86.50.604736223210.513.91.42.1400661639696.30.63598876721113.91.42596.30.635988767211.514.21

33、.12.381228229796.30.63598876721214.21.12.3812282297.596.30.635988767212.514.50.82.6996819519896.30.63598876721314.50.82.69968195198.596.30.635988767213.514.312.47653849996.30.63598876721414.312.476538499.596.30.635988767214.5141.32.21417413610096.30.635988767215141.32.214174136100.596.30.63598876721

34、5.514.312.476538410196.30.63598876721614.312.4765384101.59.360.684778931216.514.312.47653841029.360.68477893121714.312.4765384102.59.45.90.701586049217.514.312.47653841039.45.90.70158604921814.312.4765384103.59.45.90.701586049218.514.312.47653841049.45.90.70158604921914.312.4765384104.59.95.40.79013

35、9447219.514.312.47653841059.95.40.79013944722014.312.4765384105.59.65.70.736072225220.514.312.47653841069.65.70.73607222522114.40.92.581898916106.5105.30.80883158221.514.40.92.581898916107105.30.8088315822214.40.92.581898916107.59.85.50.771790308222.514.40.92.5818989161089.85.50.77179030822314.50.82

36、.699681951108.5105.30.80883158223.514.50.82.699681951109105.30.8088315822414.50.82.699681951109.510.15.20.827879775224.514.50.82.69968195111010.15.20.82787977522514.60.72.833213344110.510.15.20.827879775225.514.60.72.83321334411110.25.10.8472978622614.70.62.987364024111.510.25.10.84729786226.514.70.

37、62.98736402411210.25.10.8472978622714.70.62.987364024112.510.25.10.84729786227.514.70.62.98736402411310.25.10.8472978622814.70.62.987364024113.510.25.10.84729786228.514.70.62.98736402411410.44.90.88730319522914.70.62.987364024114.510.44.90.887303195229.514.60.72.83321334411510.44.90.88730319523014.6

38、0.72.833213344115.510.44.90.887303195230.5150.33.68051120411610.44.90.887303195231150.33.680511204116.510.44.90.887303195231.5150.33.68051120411710.44.90.887303195232150.33.680511204117.510.44.90.887303195232.5150.33.68051120411810.54.80.907922482233150.33.680511204118.510.54.80.907922482233.5150.33

39、.68051120411910.25.10.84729786234150.33.680511204119.510.25.10.84729786234.5150.33.68051120412010.54.80.907922482235150.33.680511204120.510.54.80.907922482235.5150.33.68051120412110.54.80.907922482236150.33.680511204121.510.64.70.928975891236.5150.33.68051120412210.64.70.928975891237150.33.680511204

40、122.510.84.50.972461003237.5150.33.680511204实验：非稳态导热法测定颗粒物料的导热系数水浴温度Tb=30时间t/s物料温度T/（Tb-T）/ln（Tb-T）017.29999912.7000012.5416020721018.111.92.47653842018.79999911.2000012.4159138683019.70000110.2999992.3321437984020.59.52.2512917995021.48.62.1517622036022.17.92.0668627597022.7999997.2000011.974081165

41、8023.46.61.8870696499024.2000015.7999991.75785774510024.7999995.2000011.64865881811025.2000014.7999991.5686157112025.7999994.2000011.43508476313026.2000013.7999991.33500080414026.7999993.2000011.1631511221502731.09861228916027.52.50.91629073217027.92.10.74193734518028.2000011.7999990.58778610919028.

42、51.50.40546510820028.7000011.2999990.262363495210291022029.2999990.700001-0.35667351523029.50.5-0.69314718124029.60.4-0.91629073225029.7999990.200001-1.609432912水浴温度Tb=35时间t/s物料温度T/（Tb-T）/ln（Tb-T）023122.484906651023.79999911.2000012.4159138682024.79999910.2000012.3223878183025.7000019.2999992.230014

43、2934026.48.62.1517622035027.17.92.0668627596027.97.11.9600947847028.56.51.8718021778029.2000015.7999991.7578577459029.7000015.2999991.66770663210030.2000014.7999991.5686157111030.7000014.2999991.4586147912031.13.91.36097655313031.63.41.22377543214031.93.11.13140211115032.2999992.7000010.99325214316032.5