因瓦条码水准标尺检定规程试验报告

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--2/22/2附件6-3因瓦条码水准标尺试验报告试验目的通过试验，验证规程中计量方法和计量性能、技术指标的合理性及可行性，试验内容为因瓦条码水准标尺检定试验。试验设备标准设备序号名称型号规格出厂编号生产厂家1激光干涉仪（0～40）mUS52140353Keysight2钢直尺（0～1000）mm新宇3全站仪（0～360）°1398729Leica4平板（300×300）mm20200267泊头市宏泰量具有限公司被校设备1因瓦条码水准标尺LD1254715/54752Trimble2因瓦条码水准标尺LD1270386/71590Trimble试验环境环境温度：19.5℃环境湿度：35%RH试验方法按规程中有关条文进行。试验结果标尺分划面弯曲差（矢距）、标尺中轴线与标尺底面的垂直度、一副标尺零点差之差、标尺基本码分划误差、标尺米间隔长度平均值与标称值之差的试验。试验目的：验证本规程对药因瓦条码水准标尺检定方法的可行性。结论：根据两次试验结果可以看出应用本规范给出的方法进行药物溶出度仪的校准方法可行。因瓦条码水准标尺试验记录制造单位：Trimble型号规格：LD12（2m）出厂编号：A尺：54715/B尺：54752环境温度：20.5℃环境湿度：35％RH计量标准器名称制造单位型号/规格出厂编号测量范围证书编号不确定度或准确度等级或最大允许误差有效期至双频激光干涉仪KEYSIGHT5519BUS52140353（0～40）mCDcd2021-10113U=2.5E-08（k=2）2023年09月13日平板泊头市宏泰量具有限公司（300×300）mm20200267（300×300）mm2022J10980级2023年08月04日钢直尺新宇工具（0～1000）mm（0～1000）mm2022J0766U=0.05mm（k=2）2023年05月26日全站仪LeicaTS0913987292021C0766Ⅱ级2022年9月13日标准器使用前正常☑异常□标准器使用后正常☑异常□检定结果：合格序号检定项目检定结果1外观合格2标尺上圆水准器安置的正确性合格3标尺分划面弯曲差（矢距）/mmA尺0.9合格B尺0.94标尺中轴线与标尺底面的垂直度/＇A尺3.6合格B尺3.75一副标尺零点差之差/mm0.02合格6标尺基本码分划误差/mm偏差A尺0.007合格B尺0.018标准差A尺0.007合格B尺0.0037标尺米间隔长度平均值与标称值之差/mmA尺-0.009合格B尺0.019检定日期：年月日检定员：核验员：型号:LD12条码水准标尺编号:54715-A尺1.检定项目:米长实测平均值与标称值之差[(MeterLength)totalnums:29,kick-off:0,times=2.0,Maxdiff=0.026]1000.00791000.00151000.0096999.9982999.9951999.9956999.9965999.9981999.9878999.9874999.9873999.9880999.9896999.9832999.9836999.9845999.9831999.9856999.9879999.9861999.9926999.9914999.9938999.9909999.9904999.9889999.9932999.9894Average=999.9915mm,StandardDeviation=0.0067mmStandardValue=1000.0000mm,Deviation=-0.008mm,rms=0.0109mmMaxDeviation=-0.0169mmMeterScale:V=-6.6530x+17.0395(um),std=4.1325um,nKicks=1[(BasicCodeWidth)totalnums:175,kick-off:1,times=2.0,Maxdiff=0.013]0.0066-0.00150.0001-0.00040.0042-0.0014-0.00250.0057-0.00510.00420.00120.00160.0012-0.00380.00010.00240.0016-0.00110.0028-0.0006-0.00210.00270.0016-0.00270.00180.0013-0.00320.00190.00040.0009-0.00330.00200.0014-0.00170.0027-0.00370.0023-0.00390.00090.00140.00050.0003-0.00180.00080.0009-0.00050.0003-0.0002-0.0001-0.00150.00020.0024-0.0002-0.00420.00160.0014-0.00220.00060.00040.0019-0.0007-0.00070.0039-0.0013-0.00290.0029-0.0007-0.00320.0032-0.0012-0.00290.0032-0.0001-0.00310.0041-0.00510.0017-0.00110.0038-0.00590.0059-0.00100.00080.00020.0021-0.0004-0.0043-0.0009-0.00310.00490.0003-0.0003-0.0001-0.00290.00010.0024-0.00310.0023-0.00420.0056-0.0058-0.00280.0020-0.00450.0037-0.00070.0040-0.0019-0.0008-0.00510.0030-0.0022-0.00090.0043-0.0022-0.0000-0.00060.0005-0.00030.0003-0.00080.0012-0.00080.0019-0.0007-0.00050.0040-0.00520.00210.0017-0.0006-0.00550.0022-0.0015-0.00120.0025-0.00060.0025-0.0021-0.00300.0040-0.0014-0.0036-0.00040.0017-0.00070.00200.0025-0.00050.0011-0.00190.00010.00230.00210.0024-0.00490.0030-0.00260.0015-0.00210.00090.0013-0.00190.00010.0011-0.00030.0016-0.0012-0.0005-0.00330.00200.00030.0013-0.00130.6255Average=0.0000mm,StandardDeviation=0.0025mmStandardValue=0.0000mm,Deviation=0.000mm,rms=0.0025mmMaxabsoluteDeviation=0.0066mm检定结果:米长实测平均值与标称值之差:-0.009mm基本码宽最大偏差:0.007mm基本码宽标准偏差:0.003mm2.检定项目:标尺中轴线与标尺底面的垂直度盘左盘右均值Dab/mm垂直度正面1.00.70.8518111.6′侧面1.82.01.9017983.6′检定结果：标尺中轴线与标尺底面的垂直度:3.6′3.检定项目:一副标尺零点差之差123均值A尺0.72730.72730.72730.72730.72730.72730.727300.72730.72730.7273B尺0.72730.72730.72730.72730.72730.72730.727320.72730.72740.7274检定结果：一副标尺零点差之差:0.02mm4.检测项目:标尺分划面弯曲差（矢距）双频值/mm矢距/mm-0.00153.315995.28552.418检定结果:矢距:0.9mm型号:LD12条码水准标尺编号:54752-B尺1.检定项目:米长实测平均值与标称值之差[(MeterLength)totalnums:30,kick-off:0,times=2.0,Maxdiff=0.127]1000.02661000.01191000.09351000.10091000.09241000.09461000.09021000.08761000.09411000.0956999.9889999.9855999.9915999.9944999.9950999.9880999.9877999.9891999.9919999.9923999.9937999.9976999.9944999.9990999.9876999.9821999.9795999.9744Average=1000.0185mm,StandardDeviation=0.0472mmStandardValue=1000.0000mm,Deviation=0.018mm,rms=0.0508mmMaxDeviation=0.1009mmMeterScale:V=-2.1797x+90.6636(um),std=8.7431um,nKicks=17[(BasicCodeWidth)totalnums:177,kick-off:4,times=2.0,Maxdiff=0.027]0.06880.00450.00200.0030-0.00020.00040.00030.00030.0027-0.0014-0.00220.0057-0.00370.0019-0.00110.00320.0003-0.00130.00360.00050.0024-0.00140.0018-0.0005-0.00080.00380.0008-0.00240.00330.0001-0.00010.0008-0.0044-0.00210.0007-0.00040.0022-0.00120.0022-0.00250.0027-0.00440.0006-0.00050.00120.0019-0.00370.0027-0.0005-0.00140.0023-0.00130.0002-0.0015-0.00040.0007-0.0005-0.00160.00190.0007-0.0003-0.00150.00920.00690.00220.00440.0014-0.00450.0043-0.0004-0.00270.0038-0.0015-0.00080.0038-0.00190.0020-0.0008-0.00410.0020-0.01800.0008-0.00540.0077-0.00320.0018-0.0008-0.00070.0029-0.0032-0.0008-0.00260.00370.0028-0.0025-0.00270.0003-0.00110.00680.07940.0029-0.00450.0052-0.0027-0.0007-0.0012-0.00110.0032-0.00220.0070-0.00360.00070.00050.00160.0052-0.10450.0016-0.0006-0.0003-0.00150.0029-0.00060.0005-0.00260.0015-0.00320.00420.0016-0.00130.0028-0.00630.00200.00350.0002-0.00250.0018-0.00470.0014-0.0005-0.00130.0030-0.0002-0.00170.0010-0.00160.0026-0.00760.00240.00090.00140.0027-0.00130.0006-0.00280.00220.00230.00090.0021-0.00400.0031-0.00220.0021-0.0008-0.00020.0014-0.00020.00040.0004-0.00030.0025-0.0003-0.0000-0.0012-0.00000.0040-0.00511.5025Average=0.0002mm,StandardDeviation=0.0031mmStandardValue=0.0000mm,Deviation=0.000mm,rms=0.0031mmMaxabsoluteDeviation=0.0180mm检定结果:米长实测平均值与标称值之差:0.019mm基本码宽最大偏差:0.018mm基本码宽标准偏差:0.003mm2.检定项目:标尺中轴线与标尺底面的垂直度盘左盘右均值Dab/mm垂直度正面0.50.60.5517501.1′侧面2.01.91.9517993.7′检定结果：标尺中轴线与标尺底面的垂直度:3.7′3.检定项目:一副标尺零点差之差123均值A尺0.72730.72730.72730.72730.72730.72730.727300.72730.72730.7273B尺0.72730.72730.72730.72730.72730.72730.727320.72730.72740.7274检定结果：一副标尺零点差之差:0.02mm4.检测项目:标尺分划面弯曲差（矢距）双频值/mm矢距/mm-0.00953.631995.02252.743检定结果:矢距:0.9mm因瓦条码水准标尺试验记录制造单位：Trimble型号规格：LD12（2m）出厂编号：A尺：70386/B尺：71590环境温度：20.5℃环境湿度：35％RH计量标准器名称制造单位型号/规格出厂编号测量范围证书编号不确定度或准确度等级或最大允许误差有效期至双频激光干涉仪KEYSIGHT5519BUS52140353（0～40）mCDcd2021-10113U=2.5E-08（k=2）2023年09月13日平板泊头市宏泰量具有限公司（300×300）mm20200267（300×300）mm2022J10980级2023年08月04日钢直尺新宇工具（0～1000）mm（0～1000）mm2022J0766U=0.05mm（k=2）2023年05月26日全站仪LeicaTS0913987292021C0766Ⅱ级2022年9月13日标准器使用前正常☑异常□标准器使用后正常☑异常□检定结果：合格序号检定项目检定结果1外观合格2标尺上圆水准器安置的正确性合格3标尺分划面弯曲差（矢距）/mmA尺0.8合格B尺1.14标尺中轴线与标尺底面的垂直度/＇A尺3.6合格B尺4.55一副标尺零点差之差/mm0.05合格6标尺基本码分划误差/mm偏差A尺0.020合格B尺0.020标准差A尺0.008合格B尺0.0097标尺米间隔长度平均值与标称值之差/mmA尺0.040合格B尺0.037检定日期：年月日检定员：核验员：型号:LD12条码水准标尺编号:70386-A尺1.检定项目:米长实测平均值与标称值之差[(MeterLength)totalnums:84,kick-off:0,times=2.0,Maxdiff=0.063]1000.05841000.07251000.04761000.05621000.05731000.03631000.05081000.06981000.05811000.06281000.05031000.04851000.05281000.05481000.04871000.04241000.04511000.04091000.04211000.04481000.04961000.04591000.02731000.04211000.03781000.03591000.03501000.03831000.04721000.03281000.04681000.04581000.04511000.04481000.02791000.02381000.04121000.01201000.04131000.05181000.02011000.04671000.04541000.03241000.03451000.04251000.02321000.02571000.04281000.04011000.04041000.02361000.04041000.02811000.04461000.03441000.04561000.03171000.02581000.04441000.03701000.02271000.03431000.01271000.00911000.03071000.05041000.01061000.05161000.03091000.01971000.03891000.02811000.01961000.03821000.03411000.03841000.03511000.04691000.04911000.02871000.04121000.04671000.0430Average=1000.0396mm,StandardDeviation=0.0125mmStandardValue=1000.0000mm,Deviation=0.040mm,rms=0.0417mmMaxDeviation=0.0725mmMeterScale:V=38.6493x+26170.5805(um),std=8.6377um,nKicks=1[(BasicCodeWidth)totalnums:308,kick-off:12,times=2.0,Maxdiff=0.040]17.41048.7711-0.0280-0.00290.01950.00260.0048-0.0074-0.01030.00570.0065-0.0005-0.0032-0.01160.00040.0243-0.02330.0100-0.01100.00980.00650.0002-0.0012-0.00780.0070-0.0016-0.00890.0092-0.00680.00780.00480.0043-0.00950.0057-0.00590.0114-0.01310.00750.0108-0.0026-0.0008-0.0052-0.0039-0.00660.00800.00500.00040.00240.00550.00860.0045-0.02210.00820.0036-0.00980.0077-0.0020-0.00370.00040.01210.0002-0.0068-0.01070.00640.0190-0.0042-0.0141-0.00380.01670.00630.0023-0.0248-0.00280.01190.01000.0068-0.0173-0.00720.01140.0080-0.0030-0.0128-0.00130.00220.0048-0.00070.00030.0011-0.01820.01170.0063-0.0018-0.0087-0.00190.01350.0005-0.00580.00030.01250.0091-0.0021-0.02190.00470.01150.0137-0.0002-0.02220.0155-0.00520.0130-0.0114-0.0040-0.01510.01990.0091-0.0011-0.0237-0.00240.00890.0173-0.0049-0.00880.00500.00380.0091-0.0127-0.00490.0012-0.00470.0123-0.00690.0020-0.01360.00470.00910.0058-0.0033-0.0070-0.00960.0133-0.0051-0.00040.00050.00250.0149-0.0011-0.01360.0022-0.00560.0092-0.0023-0.00510.0110-0.00470.01080.0031-0.01270.00200.00870.0096-0.0048-0.0165-0.00080.00610.0095-0.00980.0077-0.01050.00310.0081-0.01140.00860.0060-0.01580.0066-0.0019-0.00690.01080.00140.0060-0.0025-0.0055-0.00230.00200.0127-0.0106-0.00320.0050-0.00480.0080-0.00270.0038-0.0167-0.00550.00840.0074-0.00370.0049-0.01170.00350.0053-0.00280.0031-0.00610.0098-0.0016-0.00880.0089-0.01220.00400.0069-0.00740.00460.00490.00070.00090.0221-0.03190.01250.0097-0.0032-0.00400.0050-0.00510.00100.0073-0.0117-0.01060.0074-0.00070.0024-0.00630.0111-0.00460.0112-0.0028-0.00580.00410.0021-0.00620.0093-0.0003-0.0084-0.00670.00750.0071-0.0071-0.01320.01550.0003-0.00550.00980.0000-0.0143-0.00150.0156-0.0053-0.00790.0106-0.00280.0052-0.00390.0059-0.0115-0.00220.00510.0107-0.0053-0.00570.00290.01030.0006-0.0107-0.0037-0.00230.0063-0.00210.0062-0.00640.01110.0013-0.01210.0162-0.0196-0.00350.00860.00630.0055-0.01710.01130.0070-0.00260.0010-0.0010-0.0017-0.00230.0142-0.0082-0.00300.00120.00800.0079-0.0179-0.00340.00890.00190.0073-0.0092Average=0.0007mm,StandardDeviation=0.0082mmStandardValue=0.0000mm,Deviation=0.001mm,rms=0.0082mmMaxabsoluteDeviation=0.0199mm检定结果:米长实测平均值与标称值之差:0.040mm基本码宽最大偏差:0.020mm基本码宽标准偏差:0.008mm2.检定项目:标尺中轴线与标尺底面的垂直度盘左盘右均值Dab/mm垂直度正面0.90.90.9018251.7′侧面1.82.01.9018103.6′检定结果：标尺中轴线与标尺底面的垂直度:3.6′3.检定项目:一副标尺零点差之差123均值A尺0.72740.72740.72740.72740.72740.72740.727400.72740.72740.7274B尺0.72750.72740.72740.72750.72750.72740.727450.72740.72740.7274检定结果：一副标尺零点差之差:0.05mm4.检测项目:标尺分划面弯曲差（矢距）双频值/mm矢距/mm0.00053.297995.14452.542检定结果:矢距:0.8mm型号:LD12条码水准标尺编号:71590-B尺1.检定项目:米长实测平均值与标称值之差[(MeterLength)totalnums:87,kick-off:0,times=2.0,Maxdiff=0.054]1000.03511000.05361000.06261000.04711000.05621000.06261000.05591000.04731000.06201000.02991000.04291000.05821000.03511000.04581000.04751000.03631000.04491000.05641000.04201000.04041000.04341000.02841000.02611000.04591000.03581000.03631000.03211000.01881000.04541000.03441000.02931000.02781000.02931000.04261000.02511000.04351000.04271000.04471000.03561000.02901000.02791000.03621000.01551000.03241000.03431000.01561000.03151000.03681000.01841000.02711000.03081000.00851000.02891000.03051000.03041000.03791000.01741000.03831000.01861000.03651000.03021000.03821000.03981000.03091000.03891000.03941000.01081000.01231000.01991000.05571000.03061000.03331000.01231000.03271000.03321000.02891000.01241000.03961000.03651000.04801000.04151000.05421000.05931000.03281000.04361000.05391000.0481Average=1000.0364mm,StandardDeviation=0.0126mmStandardValue=1000.0000mm,Deviation=0.036mm,rms=0.0387mmMaxDeviation=0.0626mmMeterScale:V=38.7359x+11.7789(um),std=9.0251um,nKicks=1[(BasicCodeWidth)totalnums:313,kick-off:10,times=2.0,Maxdiff=0.039]0.01590.0045-0.0067-0.01820.00690.00330.00710.0071-0.03120.01110.0068-0.00130.0105-0.0027-0.01660.01090.01000.0011-0.0066-0.01130.00020.01300.0038-0.00960.0017-0.00720.01090.0064-0.0042-0.00450.00250.0075-0.01800.0049-0.00760.01060.00900.00690.0021-0.02600.0205-0.00310.0088-0.00990.0103-0.00530.00680.0014-0.01780.0068-0.00740.00400.0119-0.00550.00210.00370.00660.0038-0.01980.00650.0060-0.00540.00230.00120.0022-0.00320.0105-0.0045-0.0089-0.00530.00790.0174-0.0089-0.00840.00500.00030.00680.0053-0.0182-0.00510.00820.01240.0084-0.0173-0.00500.00470.0130-0.0100-0.01270.00050.00130.00890.0020-0.00080.0056-0.02440.01330.0103-0.0026-0.0107-0.00170.01250.0020-0.0103-0.00670.01490.00470.0078-0.02150.00570.01200.00030.0072-0.01210.0130-0.00560.0126-0.01950.0080-0.02300.0184-0.00240.0358-0.03890.0026-0.00680.01500.0060-0.0055-0.00140.00440.0077-0.0053-0.01760.0093-0.01750.00810.00290.0056-0.01460.00440.00560.00470.00180.0012-0.01470.0095-0.00390.0032-0.0074-0.00240.0159-0.0008-0.0078-0.00920.00260.00510.0048-0.00690.0117-0.00730.0108-0.0007-0.01060.0105-0.00080.0090-0.0028-0.0056-0.00640.00310.0127-0.00580.0006-0.01500.00530.0121-0.00240.0012-0.0008-0.00830.00650.0011-0.01230.00750.0042-0.00030.0072-0.01700.0049-0.00500.00840.0100-0.01750.0108-0.00570.0127-0.0023-0.0021-0.0148-0.0037-0.00080.0112-0.00660.0067-0.00660.00040.0217