标准文本-食品安全标准

ICSDBS22吉林省食品安全地方标准DBSxx/xx—xxxx食品安全地方标准动物源性食品中24种B2-受体激动剂

及受体阻断剂残留量的测定

液相色谱-串联质谱法（报批稿）2012-XX-XX发布2012-XX-XXXX2012-XX-XX发布吉林省卫生厅发布吉林省卫生厅发布DBSXX/XXXDBSXX/XXX—201X#附录C

(资料性附录)表C.124种B2-受体激动剂及B-受体阻断剂的不同基质、三个水平添加回收率范围化合物添加水平(ug/kg)猪肾/%猪肝/%牛肉/%猪肉/%奥西那林0.572.5〜88.272.3〜86.174.6〜90.571.7〜85.25.080.5〜94.175.9〜90.883.8〜100.678.8〜89.710.074.6〜101.180.7〜91.282.0〜91.584.2〜93.3非诺特罗0.572.0〜80.673.1〜86.975.6〜89.073.4〜87.35.073.6〜83.372.5〜87.876.4〜101.174.2〜92.110.078.2〜102.274.6〜91.575.0〜93.373.6〜104.7西马特罗0.580.5〜91.482.7〜91.880.0〜93.481.5〜95.25.074.9〜90.080.4〜94.971.2〜93.674.6〜95.210.072.7〜92.683.8〜97.980.5〜105.380.4〜95.9沙丁胺醇0.572.6〜87.874.4〜107.282.1〜93.472.9〜91.75.079.1〜95.277.3〜93.873.9〜96.075.6〜95.810.080.8〜96.485.3〜94.980.8〜95.783.5〜104.0塞布特罗0.573.5〜93.179.3〜93.686.7〜102.572.4〜94.75.085.2〜96.875.6〜95.878.4〜92.485.2〜106.210.073.6〜94.582.2〜96.483.6〜95.078.3〜96.2丙卡特罗0.578.1〜93.777.7〜93.575.2〜102.680.0〜103.35.083.4〜96.682.1〜95.673.8〜93.376.6〜94.710.078.5〜103.476.7〜98.082.8〜97.374.2〜106.3克仑塞罗0.578.1〜93.675.9〜103.781.5〜96.480.5〜94.65.074.9〜97.680.5〜94.573.7〜98.879.7〜96.710.082.3〜96.973.9〜105.082.0〜95.678.5〜94.8克仑丙罗0.578.5〜104.681.3〜95.372.6〜105.282.8〜96.35.074.1〜95.080.2〜94.983.0〜95.681.5〜95.910.081.6〜96.981.6〜105.982.4〜98.677.9〜97.0利妥特灵0.573.8〜93.677.3〜97.482.2〜95.282.7〜94.35.078.6〜97.279.2〜96.880.6〜97.580.6〜97.510.084.5〜95.883.4〜107.378.7〜96.673.6〜96.4妥布特罗0.582.6〜97.374.5〜95.872.2〜103.579.2〜97.95.076.5〜95.276.9〜97.173.6〜96.480.7〜98.010.075.9〜102.177.7〜96.676.2〜105.476.9〜94.1克伦特罗0.575.2〜95.274.3〜90.983.8〜105.281.8〜97.15.073.4〜92.983.2〜98.184.0〜96.971.2〜93.610.080.2〜103.584.2〜95.975.8〜95.683.5〜98.5S-美托洛尔0.588.3〜106.381.7〜94.373.6〜89.886.6〜95.55.085.1〜93.978.4〜96.177.5〜90.485.8〜96.110.082.9〜98.485.8〜94.880.9〜96.184.2〜95.9

化合物添加水平(ug/kg)猪肾/%猪肝/%牛肉/%猪肉/%R-美托洛尔0.581.0〜108.075.8〜95.683.1〜96.577.9〜94.65.067.9〜89.883.1〜108.280.8〜92.381.1〜93.810.075.6〜95.378.4〜105.890.3〜106.485.4〜99.0莱卡多巴胺0.571.2〜93.686.6〜95.578.6〜93.477.0〜92.85.073.4〜92.985.8〜96.175.7〜93.875.4〜107.410.081.8〜96.284.2〜95.980.3〜92.785.6〜97.3溴氯布特罗0.570.2〜85.168.9〜88.775.8〜95.666.8〜94.25.076.3〜90.774.5〜91.983.1〜108.279.7〜98.910.073.5〜92.080.3〜96.278.4〜105.884.5〜97.6福莫特罗0.581.0〜108.073.4〜95.879.9〜90.376.7〜96.15.074.9〜92.876.1〜102.676.8〜96.184.2〜106.610.075.6〜95.384.3〜93.773.7〜89.977.5〜96.3溴布特罗0.585.2〜98.683.8〜96.879.9〜95.084.3〜98.65.086.4〜100.982.9〜104.383.7〜97.982.5〜99.210.083.8〜99.085.5〜98.787.6〜104.480.8〜95.7马布特罗0.588.3〜106.379.9〜94.882.6〜96.385.7〜97.25.085.1〜93.983.9〜96.085.8〜103.783.6〜95.110.082.9〜98.486.5〜98.279.2〜95.975.4〜101.1克仑潘特0.583.1〜96.571.2〜93.281.7〜94.384.5〜104.55.080.8〜92.373.9〜91.778.4〜96.181.0〜95.210.090.3〜106.488.2〜98.385.8〜94.884.5〜96.4苯氧丙酚胺0.580.3〜97.178.7〜96.579.9〜104.382.1〜93.95.083.5〜96.982.4〜95.280.6〜94.785.3〜98.410.085.2〜98.281.6〜96.886.1〜95.884.4〜97.5拉贝特罗0.578.8〜95.585.1〜95.577.9〜94.682.3〜93.35.083.2〜94.984.3〜96.181.1〜93.885.1〜106.610.085.9〜95.887.7〜105.685.4〜99.079.9〜93.8异克仑潘特0.583.4〜89.978.4〜90.282.0〜89.575.5〜90.35.080.0〜92.484.5〜95.083.3〜107.476.7〜91.210.079.7〜96.182.6〜93.177.7〜90.483.8〜93.2马喷特罗0.576.6〜94.371.2〜87.270.0〜96.778.6〜105.35.070.2〜97.579.5〜96.378.3〜101.271.7〜90.910