基于分子识别的农产品中有机磷农药新型检测技术研究与应用

1、序号知识产权名称知识产权类别发明人知识产权人知识产权号取得日期国（区）别发明专利有效状态证明材料1一种同时检测九种有机磷农药的方法发明专利权徐志祥；王玺龙；赵涛山东农业大学2014-8-6中国有效附件-12一种同时检测敌百虫和久效磷的方法发明专利权徐志祥；辛军红；乔旭光山东农业大学2013-10-16中国有效附件-23一种酶标记仿生免疫分析检测敌百虫和乙酰甲胺磷的方法发明专利权徐志祥；时辰；高绘菊山东农业大学2016-9-21中国有效附件-34敌百虫仿生酶联免疫吸附检测方法发明专利权徐志祥；孟玲；乔旭光山东农业大学2013-7-31中国有效附件-4序号论文专著名称发表刊物（出版社）发表（出版）

2、时间作者（按刊物发表顺序）证明材料1Study of an online molecularly imprinted solid phase extraction coupled to chemiluminescence sensor for the determination of trichlorfon in vegetablesJournal of Agricultural and Food Chemistry2011-12Ling Meng; Xuguang Qiao; Jiaming Song; Zhixiang Xu*; Junhong Xin; Yue Zhang附件-52Sim

3、ultaneous determination of nine trace organophosphorous pesticide residues in fruit samples using molecularly imprinted matrix solid-phase dispersion followed by gas chromatographyJournal of Agricultural and Food Chemistry2013-4Xilong Wang; Xuguang Qiao; Yue Ma; Tao Zhao; Zhixiang Xu*附件-63Simultaneo

4、us separation and determination of 8 organophosphorous pesticide residues in vegetables through molecularly imprinted solid-phase extraction coupled to gas chromatographyJournal of Separation Science2012-12Junhong Xin; Xuguang Qiao; Yue Ma; Zhixiang Xu*附件-74Molecularly imprinted polymer as sorbent f

5、or solid-phase extraction coupling to gas chromatography for the simultaneous determination of trichlorfon and monocrotophos residues in vegetablesFood Analytical Methods2013-1Junhong Xin; Xuguang Qiao; Zhixiang Xu*; Jie Zhou附件-85Simultaneous determination of three trace organophosphorus pesticide r

6、esidues in vegetables using molecularly imprinted solid-phase extraction coupled with high performance liquid chromatographyFood Analytical Methods2016-1Qingqing Wang; Xin Zhang#; Zhixiang Xu; Huiju Gao*附件-96Molecularly imprinted solid-phase extraction coupled with high-performance liquid chromatogr

7、aphy for the determination of trace trichlorfon and monocrotophos residues in fruitsFood Analytical Methods2017-4Deqing Li; Xin Zhang#; Feifan Kong; Xuguang Qiao*; Zhixiang Xu*附件-107Development of a direct competitive biomimetic enzyme-linked immunosorbent assay based on a hydrophilic molecularly im

8、printed membrane for the determination of trichlorfon residues in vegetablesFood Analytical Methods2012-9Ling Meng; Xuguang Qiao; Zhixiang Xu*; Junhong Xin; Lei Wang附件-118A study on biomimetic immunoassay-capillary electrophoresis method based on molecularly imprinted polymer for determination of tr

9、ace trichlorfon residue in vegetablesFood Chemistry2016-12Jie Li; Juxiu Lu#; Xuguang Qiao*; Zhixiang Xu*附件-129The biomimetic immunoassay based on molecularly imprinted polymer: A comprehensive review of recent progress and future prospectsJournal of Food Science2011-3Zhixiang Xu; Huiju Gao; Limin Zh

10、ang; Xueqing Chen; Xuguang Qiao*附件-1310Development of molecularly imprinted electrochemical sensors based on Fe3O4MWNTs-COOH/CS nanocomposite layers for detecting traces of acephate and trichlorfonAnalyst2014-11Qinghua Tang; Xiujuan Shi#; Xiaolin Hou; Jie Zhou; Zhixiang Xu*附件-14姓名排序职称工作单位对成果创造性贡献曾获省

11、级以上科技奖励情况徐志祥1/6教授山东农业大学主持人，负责项目整体设计实施、协调，对创新点一、二、三、四做出了创造性贡献。制备了高选择性的分子印迹吸附功能材料和识别元件，并对吸附性能进行表征；优化了与色谱、化学发光体系、毛细管电泳、电化学传感器的匹配性，解决了化学反应与生化反应的协同性，建立了农产品等复杂基质中有机磷农药残留高精准检测新方法；研发了MI-SPE有机磷农药专用固相萃取柱产品。无乔旭光2/6教授山东农业大学本项目主要成员，负责项目的技术指导和实施，对创新点一、二、三有创造性贡献。具体参与高选择性的分子印迹吸附功能材料的表征；有机磷农药痕量残留分子印迹吸附检测方法的建立及其在农产品等

12、复杂基质有机磷农药残留检测中的应用。无高绘菊3/6副教授山东农业大学本项目主要成员，负责项目的实施，对创新点二、三有创造性贡献。具体负责仿生抗体的制备及性能表征；仿生免疫分析以及仿生电化学传感器检测方法的建立及其在实际样品检测中的应用与方法评价。无张丽敏4/6讲师山东农业大学本项目技术骨干，负责项目的实施，对创新点一有创造性贡献，创新点二做出了重要贡献。具体负责对敌百虫等具有高选择识别能力的分子印迹毛细管整体柱的制备；分子印迹固相萃取与毛细管电泳联用检测葡萄酒中有机磷农药新方法的建立及应用。无孔非凡5/6高级工程师山东五洲检测 本项目技术骨干，负责项目的实施，对创新点四做出了重要贡献。参与MI-SPE有机磷专用固相萃取柱性能改善与产品研发，有机磷农药多残留仿生检测技术集成；负责有机磷农药残留高