动物源性食品中211种农药及相关化学品的保留时间、定量离子对、定性离子对

1、附录A211 种农药及相关化学品的保留时间、定量离子对、定性离子对?211种农药及相关化学品的保留时间、定量离子对、定性离子对，见表B.1 。表 A.1211 种农药及相关化学品的保留时间、定量离子对、定性离子对序号英文名称中文名称保留时间定量离子对碰撞电压定性离子对碰撞电压minvv1Acrinathrin氟丙菊酯14.94181-15230207.8-181.1102Alachlor甲草胺9.19188.1-160.210160-132.1103Aldrin艾氏剂9.87262.9-192.935254.9-220204Ametryn莠灭净9.18227-58.110185-17055An

2、thraquinone蒽醌9.89208-152.220208-180.2106Atrazine-desethyl去乙基莠去津7.20186.9-172.15171.9-94157Azinphos-ethyl乙基谷硫磷 ( 乙基保棉15.13160-132.10132-77.115磷)8Benalaxyl苯霜灵12.78148-7735148-105.1209Bendiocarb恶虫威7.25166-151.110126-52.11510Benfluralin乙丁氟灵7.25292-2645292-2061011Benfuresate呋草磺 / 呋草黄8.85255.9-163.25163.1

3、-121.1512BHC-alpha - 六六六7.61180.9-14515216.9-181513BHC-beta - 六六六8.01216.9-181.15181-1451514BHC-delta - 六六六8.48181.1-145.115217-181.1515BHC-epsilonepsilon- 六六六8.64180.9-144.915180.9-1093016BHC-gamma- 六六六 / 林丹8.10181-14515216.9-1815(Lindane)17Bifenox甲羧除草醚14.13189.1-12620340.9-309.91018Bifenthrin联苯菊酯1

4、3.83181.2-165.225181.2-166.21019Bioresmethrin生物苄呋菊酯13.32123-81.15171-143.1520Bromacil除草定9.56205-18815205-1621521Bromophos甲基溴硫磷 ( 溴硫磷 )10.22330.8-315.815124.9-471022Bromophos-ethyl乙基溴硫磷10.95358.7-302.815302.8-284.71523Bromopropylate溴螨酯13.83338.8-182.920183-1551524Buprofezin噻嗪酮11.70105-10410172-571525

5、Butachlor丁草胺11.13176.1-147.110188.1-160.21026Butamifos抑草磷11.30285.9-20215200-921027Butralin地乐胺 ( 双丁乐灵 )10.15266-220.210266-174.22028Cadusafos硫线磷7.39158.8-9715158.8-1315表 B.1 211种农药及相关化学品的保留时间、定量离子对、定性离子对（续）序号英文名称中文名称保留时间定量离子对碰撞电压定性离子对碰撞电压minvv29Carbophenothion三硫磷12.74153-96.910199-1431030Chlorbensid

6、e氯杀螨10.85125-8915125-991531Chlordane-cis顺式氯丹11.05372.9-265.920374.8-265.82032Chlordane-oxy氧氯丹10.56114.9-51.125114.9-871533Chlordane-trans反式氯丹11.22374.8-265.815372.8-265.81534Chlorfenapyr虫螨腈 ( 溴虫腈）11.96136.9-10215246.9-2271535Chlorfenson杀螨酯11.30175-11110111-751536Chlorfenvinphos毒虫畏10.59266.9-159.1153

7、22.8-266.81037Chlorobenzilate乙酯杀螨醇12.10139.1-11110251.1-139.11538Chlorpropham氯苯胺灵7.09127-65.125153-125.11039Chlorpyrifos毒死蜱9.89313.8-257.815196.9-1691540Chlorpyrifos-methyl甲基毒死蜱9.09285.9-92.915124.9-47541Chlozolinate克氯得10.50186-14515188.1-1471542Clomazone异恶草松7.94125-8915204.1-107.12043Cloquintocet-m

8、exyl解毒喹13.93192-19015192-1622544Cyanophos杀螟腈8.12242.9-10910124.9-471545Cyflufenamid环氟箘胺11.88118.1-9010118.1-892546Cyfluthrin氟氯氰菊酯16.18162.9-1275162.9-90.91547Cyhalofop-butyl氰氟草酯14.61256.2-120.110120.1-911548Cyhalothrin高效氯氟氰菊酯14.79197-14110208-1815(lambda)49Cypermethrin氯氰菊酯16.49163-1275163-911050Cyph

9、enothrin苯醚氰菊酯 / 赛乐灵15.27181-152.125123-81.1551Cyproconazole环丙唑醇11.95139-11115222-125.11552Cyprodinil嘧菌环胺10.34225.2-224.310224.2-208.22053Chlorthal-dimethyl氯酞酸甲酯9.99298.9-22125300.9-2232554DDD-o，p'o，p'- 滴滴滴11.70235-165.220237-165.22055DDD-p，p'p，p'- 滴滴滴12.29234.9-165.120236.9-165.22056

10、DDE-o，p'o，p'- 滴滴伊11.00248-176.230317.8-2481557DDE-p，p'p，p'- 滴滴伊11.54246.1-176.230315.8-2461558DDT-o，p'o，p'- 滴滴涕12.35235-165.220237-165.22059DDT-p，p'p，p'- 滴滴涕12.95235-165.220237-165.22060DEET避蚊胺6.61119.1-9110119.1-65.12061Tribufos脱叶磷11.50169-57.15202-147062Deltamethrin

11、溴氰菊酯18.02250.7-1725252.9-931563Diazinon二嗪磷8.23137.1-8410137.1-542064Dichlofenthion除线磷8.91278.9-222.915222.9-204.915表 B.1211 种农药及相关化学品的保留时间、定量离子对、定性离子对（续）序号英文名称保留时间碰撞电压碰撞电压中文名称定量离子对定性离子对minvv序号英文名称中文名称保留时间定量离子对碰撞电压定性离子对碰撞电压minvv65Diclobutrazol苄氯三唑醇11.76269.8-158.920271.8-160.91566Diclofop-methyl二氯硫醚磷

12、13.19253-162.115339.9-252.91067Dicloran氯硝胺7.78206.1-17610160.1-124.11068Dicofol三氯杀螨醇9.98139-11115139-753569Dicrotofos百治磷7.23127-10915127-951570Dieldrin狄氏剂11.63262.9-19335277-241571Difenoconazole苯醚甲环唑17.79322.8-264.815324.8-266.81572Difenzoquat methyl野燕枯甲基硫酸盐11.66233.9-233.115233.9-130.125sulfate73Di

13、mepiperate哌草丹10.67119-9110118-117.11074Dimethenamid二甲吩草胺8.96230-154.110154.1-111.11075Dimethipin噻节因7.90118-585124-76576Dimethylvinphos甲基毒虫畏9.87294.9-108.915296.9-108.91577Dioxabenzofos蔬果磷7.33215.9-20110183-1531078Dioxathion敌杀磷15.86271-96.930124.9-96.9579Diphenamid双苯酰草胺10.21167.1-165.120167.1-152.115

14、80Diphenylamine二苯胺6.95169-168.215168-167.21581Disulfoton乙拌磷8.3788-605153-96.91082Dithiopyr氟硫草定9.42353.9-3065305.9-286.1583Edifenphos敌瘟磷12.84172.9-1095108.9-65.11584Endosulfan-alpha- 硫丹11.18194.9-12520194.9-159585Endosulfan-beta- 硫丹12.19206.9-17215194.9-158.91086Endosulfan sulfate硫丹硫酸酯12.93273.8-238.

15、915271.9-2371587Endrin异狄氏剂12.03262.8-19335244.8-1733088EPN苯硫磷13.86169-141.15169-77.12589Ethalfluralin乙丁烯氟灵7.11275.9-202.115315.9-275.91090Ethion乙硫磷12.34152.9-96.910124.9-96.9091Ethofumesate乙氧呋草黄9.55206.9-161.15161-105.11092Ethoprophos灭线磷6.99157.9-9715157.9-114593Ethychlozate吲熟酯10.49238-165.115167-13

16、9.91594Etofenprox醚菊酯16.69163-107.120163-135.11095Etrimfos乙嘧硫磷8.49181-153.15168-153.1596Etoxazole乙螨唑、依杀螨13.99141-63.130141-113.01597Famoxadone恶唑菌酮18.35197-141.115223.9-196.21098Fenamidone咪唑菌酮14.06238-237.210268-180.22099Fenamiphos苯线磷11.26154-13910217-202.110100Fenarimol氯苯嘧啶醇15.00139-7530219-107.110表B

17、.1211 种农药及相关化学品的保留时间、定量离子对、定性离子对（续）保留时间碰撞电压碰撞电压序号英文名称中文名称定量离子对定性离子对minvv序号英文名称中文名称保留时间定量离子对碰撞电压定性离子对碰撞电压minvv101Fenitrothion杀螟硫磷（杀螟松）9.53125.1-4715125.1-795102Fenothiocarb苯硫威 ( 苯丁硫威 )10.99160.1-72.110106.9-77.110103Fenpropathrin甲氰菊酯13.95181.1-152.125125-55.110104Fensulfothion丰索磷12.18291.8-15615156-1

18、4110105Fenthion倍硫磷9.85278-10915124.9-4710106Fenthion sulfone倍硫磷砜12.29124.9-4710124.9-795107Fenthion sulfoxide倍硫磷亚砜12.20278-10915125-4710108Fenvalerate&EsFenval氰戊菊酯 &高效氰17.31181-152.120167-125.15erate戊菊酯109Fipronil氟虫腈10.58350.8-254.815366.8-212.825110Fluacrypyrim嘧螨酯12.51145.1-102.125204-189.2

19、5111Flucythrinate氟氰戊菊酯16.61156.9-107.115198.9-15710112Fluoroglycofen-ethyl乙羧氟草醚15.04222.9-195.110343.8-300.215113Fluquinconazole氟喹唑15.77340-107.840340-29815114Fluridone氟啶草酮17.05328.9-328.115328-258.930115Flurochloridone氟咯草酮 / 氟氯戊10.07311-174.115187.1-159.110菊酯116Flusilazole氟硅唑11.70233-165.115233-912

20、0117Flutolanil氟酰胺11.32173-145.115280.9-17310118Fluvalinate-tau氰戊菊酯17.48250-20040250-5540119Fonofos地虫硫磷8.20136.9-1095108.9-80.95120Furalaxyl呋霜灵10.71242-951594.9-6715121Heptachlor七氯9.27271.7-236.915273.7-238.915Heptachlor122exo-epoxide (isomer环氧七氯10.54352.8-262.915354.8-264.915B)123Heptenophos庚烯磷6.591

21、24-8910124-6335124Hexachlorobenzene六氯苯7.74283.8-213.930283.8-248.815125Hexaconazole六那唑 / 己唑醇11.36231-17510256-15915126Hexazinone环嗪酮13.13171-71.110171-85.110127Iprodione异菌脲13.62187-12425313.8-55.920128Isazofos氯唑磷8.47161-119.15161-1465129Isocarbophos水胺硫磷10.01120-9210135.9-10815130Isodrin异艾氏剂10.37193-1

22、2330193-15720131Isofenphos异柳磷10.58212.9-121.110212.9-185.15132Isofenphos-methyl甲基异柳磷10.33199-12115241-198.95133Mecarbam灭蚜磷10.59158.9-1315130.9-745表B.1211 种农药及相关化学品的保留时间、定量离子对、定性离子对（续）保留时间碰撞电压碰撞电压序号英文名称中文名称定量离子对定性离子对minvv序号英文名称中文名称保留时间定量离子对碰撞电压定性离子对碰撞电压minvv134Mepronil灭锈胺12.47269-119.115119.1-9110135

23、Metalaxyl甲霜灵9.27234-146.120220-192.15136Methoxychlor甲氧氯13.94227-141.140227-169.125137Methyl-pentachloropheny甲基五氯苯硫9.69295.7-262.820295.7-245.835l sulfide醚138Metribuzin嗪草酮8.95198-8215198-5530139Mirex灭蚁灵14.78271.8-236.815273.8-238.815140Monocrotophos久效磷7.3197-8210127.1-9515141Myclobutanil灭克落 / 腈菌唑11.6

24、6179-125.110179-9030142Napropamide敌草胺11.33128-72.15128-100.110143Nitrofen除草醚11.94202-139.120282.9-25310144Nitrothal-isopropyl酞菌酯9.98236-194.110194-148.110145Oxadiazon恶草酮11.55174.9-11215257.8-175.15146Oxadixyl恶霜灵12.35163-132.15163-117.125147Paclobutrazol多效唑11.02236-125.110125.1-8920148Parathion对硫磷9.9

25、1290.9-10910138.9-1095149Parathion-methyl甲基对硫磷9.17125-4710125-795150Penconazole戊菌唑10.48248-157.125248-192.115151Pendimethalin二甲戊乐灵10.45251.8-162.210251.8-161.115152Pentachloroaniline五氯苯胺8.87262.8-19220264.9-19420153Pentachloroanisole五氯茴香醚7.79236.7-142.925236.7-166.930154Pentachloronitrobenzene五氯硝基苯8

26、.18249-21415295-23720155Pentoxazone戊基恶唑酮 / 环14.43284.8-69.910286.8-69.910戊恶草酮156Permethrin氯菊酯15.65183.1-168.110183.1-165.110157Phenothrin苯醚菊酯14.31183-16810122.9-81.15158Phenthoate稻丰散10.65274-12110274-12515159Phenylphenol ， 2-邻苯基苯酚6.25169-115.125169-141.115160Phorate甲拌磷7.47121-6510121-4730161Phorate

27、sulfone甲拌磷砜9.81153-9710124.9-96.95162Phorate Sulfoxide甲拌磷亚砜9.6996.9-64.92096.9-78.915163Phosalone伏杀硫磷14.50182-11115182-102.115164Phosfolan硫环磷10.56196-14010168-6025165Phosphamidon I磷胺 I8.30127-10910127-9515166Phosphamidon II磷胺 II8.89127-10910127-9515167Phthalide四氯苯酞10.25242.9-214.920271.8-242.810表 B.

28、1211 种农药及相关化学品的保留时间、定量离子对、定性离子对（续）序号英文名称中文名称保留时间定量离子对碰撞电压定性离子对碰撞电压minvv168Piperonyl butoxide增效醚13.29176.1 -103.125176.1-131.120169Pirimicarb抗蚜威8.67238-166.210166-55.120170Pirimiphos-ethyl嘧啶磷10.22318.1-166.110318.1-18210171Pirimiphos-methyl甲基嘧啶磷9.52290-12520232.9-1515172Procymidone腐霉利10.77282.8-96109

29、6-67.110173Profenofos丙溴磷11.46207.9-6330338.8-268.715174Prometryn扑草净9.23226-184.210199-184.15175Propyzamide炔苯酰草胺8.14173-14515175-14715176Propanil敌稗8.93161-9930161-9025177Propaphos丙虫磷10.88220.1-140.110220.1-125.125178Propargite炔螨特13.23135-107.110149.9-135.15179Propetamphos胺丙畏（巴胺磷，8.05138-11010138-6415

30、烯虫磷）180Propham苯胺灵5.79136.9-9310119-9110181Propiconazole丙环唑13.02172.9-14515172.9-7445182Prothiofos丙硫磷11.41266.9-2395113-94.910183Pyraclofos吡唑硫磷15.19194-13815138.9-975184Pyrazophos吡菌磷15.04221-193.110232-204.110185Pyridaben哒螨灵15.68147.2-117.120147.2-132.210186Pyriminobac-methyl嘧草醚13.01302-256.115302-230.115187Pyriproxyfen蚊蝇醚（吡丙醚）14.54136.1-78.120136.1-9615188Quinalphos喹硫磷10.66146-11810146-9130189Fenchlorphos皮蝇磷9.33125-47.115285-269.915190Silafluofen硅醚菊酯16.83179.2-151.110286-258.110191Simazi