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牵牛化学成分的研究A1A0A2A4A5A3A6A4A8A7A4A1A9A10A4A12A11A13A14A14A15A16A17A18A19A18A20A19A18A21A22A18A23A24A14A14A15A16161006A25A26A27A28A29A30A31A32A33A34A35A36PHARBITISNILLCHIOSYA37A38A39A40A41A42A43A44A40A45A46A47A48A49A50A51A52A53A54A55A44A40A49A56A57A58A59A60A61PHARBITISPURPUREALVOIGTA37A38A39A40A41A42A43A44A40A45A46A62A63A64A65A66A65A66A67A68A69A70A71A72A73HPLCA73A74A75A76A77A78A79A45A46A40A80A81A42A49A82A83A84A42A55A85A86A87A88A40A72A89A90A75A91A64A92A93A92A93A67A40A80A56A89A90A9410A95A96A97A42A98A99A100A40A101A102A103A104A105A106A107A108A109A103A104A105A110A111A1121A113A114A115A116A117A118A119A120A121A122A1232A113A118A119A120A121A122A1233A1137A119A120A124A125A1264A113A127A128A129A130A131A132A1335A113A127A128A1296A1137A119A120A127A128A1297A113A134A135A1363A1378A113A138A139A1269A113A140A141A142A12610A143A144A145A144A145A146A147A148A149A150A113A151A152A153A154A155A156A152A153A154A157A158A159A160A161A162A163A164A160A165A166A167A168A169A170A171A164A160A172A173A174A175A176A177A155A178A179A180A177A162A181A182A183A162A181A18215A184A151A152A153A154A157A158A159A160A185A186A160A187A188A189A190A183A162A181A1827A1918A192A193A194A195A196A197A198A199A200A201A202A203A204110A205A192A193A194A195A206A207A196A197A198A199A200A208A209A210A211A212A213A214A215A216A217A215A218A219A220A215A221A222A223STUDIESONTHECHEMICALCONSTITUENTSOFPHARBITISNILLCHIOSYWANGYUQI,LILINGNA,HUAZHUN,WANGJINLAN,ZHAOMINGCOLLEGEOFCHEMISTRYANDCHEMICALENGINEERING,QIQIHARUNIVERSITY,QIQIHAR,161006ABSTRACTOBJECTIVETHECHEMICALCONSTITUENTSOFTHEAERIALPARTOFPHARBITISNILLCHIOSYWERESTUDIEDFORSEARCHINGBIOACTIVENATURALPRODUCTSANDCOMPAREDWITHPHARBITISPURPUREALVOIGTMETHODSTHECONSTITUENTSWEREISOLATEDANDPURIFIEDTHROUGHCOLUMNCHROMATOGRAPHY,HPLCANDRECRYSTALLIZEDANDIDENTIFIEDONTHEBASISOFTHEIRPHYSIOCHEMICALANDSPECTRALDATARESULETSTENCOMPOUNDSWEREISOLATEDANDIDENTIFIEDASNPHYDROXYTRANSCOUMAROYLTYRAMINE1,CINNAMOYLTYRAMINE2,TYRAMINE3,7HYDROXYCOUMARIN4,SITOSTEROL3ODGLUCOSIDE5,SITOSTEROL6,PORIFERAST5EN3,7DIOL7A224FREDELIN8A224LUTEIN9,CAROTENE10CONCLUSIONTHECONSTITUENTSOFPHARBITISNILLCHIOSYWERESIMILARBYCOMPAREINGWITHPHARBITISPURPUREALVOIGTTHECOMPOUNDS7,8AREISOLATEDFROMPHARBITISFORTHEFIRSTTIMETHECOMPOUNDS110AREISOLATEDFROMPHARBITISNILLCHOISYFORTHEFIRSTTIMEKEYWORDSPHARBITISNILLCHIOSYAMIDECOUMARINFRIEDELANEA225A226A227A228A229A230CONVOLVOULAEAEA231A232A233A234A235A236A237A238A239A240A241A225A226PHARBITISPURPUREALVOIGTA242A243A241A225A226PHARBITISNILLCHOISYA244A245A246A227A247A248A249A225A226A250A234A251A252A253A254A238A255A44A225A226A46A0A1A2A238A50A3A52A4A54A240A241A225A226A55A5A6A254A7A251A252A253A254A8A9A247A248A249A238A61A10A254A11A12A13A24714A66A67A68A251A40A2371,2A246A70A14A72A54A243A241A225A226A55A5A6A254A7A251A252A253A254A8A9A247A248A249A238A61A10A254A11A15A12A13A24710A66A67A68A251A40A237A238A74A16A17A251A18A19A242A20A21A22A23A12A13A238A83A24A254A43A227A54A25A26A27A28A29A30A54A25A26A31A32A331A34A88A35A36A37A38A39A41A42A45A472A34A38A39A41A42A45A473A347A39A41A86A48A494A34A98A51A53A56A57A58A595A34A98A51A536A347A39A41A98A51A537A34A105A60A623A1088A34叶黄素9A34胡萝卜素10A63A109A64A34A65A69A7115A73A75A76A77A78A79A80A81A82A110A84A82A85A87A89A90A91A65A69A717A928A93A94A95A73A77A78A96A82A85A114A97,A65A69A71110A116A93A94A95A73A99A76A77A78A96A82A114A117A1181A119A1001A101A102A103A104A106A102A103A104A106X6A120A107A111A112A113A115A121A122A126A123A124A125A127A128A119A129BRUKERAM400A132A130A131A133A134A135A136A121A137TMSA138A139A140A141HITACHIL7100A142A143A144A145A146A147A148A141A149A150A146A147A151A152A153A154A155A156A157A158A159A160A161A162A141A163A146A147A151A152A154200300A164A137A165A166A167A168A157A158A159A161A169A162A137A170A171A172A173A174A175A176A177A138A178A179A180A181A182A167A183A176A159A160A161A184A185A186A1872006A1887A189A190A187A191A191A192A193A194A195A196A197A137A198A191A191A192A193A194A195A199A200A201A202A203A204A138PHARBITISNILLCHIOSYA184R1ONH2HORNHOOHOHOOHHHORR1ROH2RHR2345R1GLCR2H6R1HR2H7R1HR2OH89ROH10RHA2051A206A207A208A209A210A211A2122A213A214A215A216A214A215A217A218A219A220A221A222A223A22407A225A226A227A228A22695A229A230A231A232A226A233A234A235A236A237A238A239A240A241A242400MLA243A244A245A246A247A248A249A239A250A251A250A252A239A253A254A255A130A0A4A201A1A2A3A5A6A7A8A233A9A243A250A251A250A252A8A207A0A10A236A111A11A12A143A13A14A15A4A247A248A249A250A251A250A252A93A16A17A18A4A211A19A142A20A213A14A4A246A47A21A22A239HPLCA216A23A24A25A26A27A245A14A15A43A28A5A6A28A115A10110A353A29A30A31A32A30A31A40A33A3415A58A36A37A38A39A41A61A42A44A45A46A55A48A49A50A110A51A50A52A53A54A56A40A33A341A59A57A60A62A63A64A65A66A67A68A69A70A71A72A73A67A68A69A74A75A761A63A70A71A72A73A67A68A69A74A75A762A63A67A68A69A74A75A763A637A68A69A86A77A784A63A98A79A80A81A82A83A845A85A87A88A896A90A226A91A92A94A95A96A97A99A97A100A101MP135137OCA1021HNMR400MHZ,CDCL3A10313CNMR100MHZ,CDCL3A223A104A1053A106A107A108A109A102A233A112A113A114A116A117A102A118A119A1207A90A234A91A92A94A95A96A97A99A97A100A101MP225226OCA1011HNMR400MHZ,CDCL3A235A236A121A122A123A124A125A126A1270683H,SA1281013H,SA131A239A122A129A124A125A126A1270933H,D,J65HZA1280843H,D,J70HZ,0833H,D,J70HZA132A133A122A239A134A124A125A126A1270853H,T,J70HZA128A133A122A135A136A137A125A138A126A1275721H,DD,J48,20HZA128A121A122A136A137A125A139A140A141A144A125A1454161H,DT,J48,16HZA1283621H,MA13213CNMRA146A23629A122A141A128A133A122A129A1471489,1199A128A121A122A148A140A125A136A137A141785,714A132A249A149A150A144A151A152A153A154A155A156A157A158A159A133A12229A160A161A128A162A163A164A1656A166A167A168A221A169A170A171A172A173A174A175A176A177A178A17913CNMR100MHZ,CDCL3113,120,182,188,190,198,209,231,245,259,282,291,314,339,361,368,371,374,390,422,424,436,459,491,556,714,785,1199,1489A179A180A181A182A183A184A1854A186A187A169A188A168A189A190A191A192A193A1947A195A196A197A198A199A200A202A203A2048A205A206A208A209A210A212A214A215A214A217A2181HNMRA219400MHZ,CDCL3A220A222A2240613A225A227A228A229A230A231A232A237A238A240A241A242A250A243A244A228A245A230A231A232A237A238A240A241A242A2461225A222A224A247A24826A228A251A231A238A240A24613CNMRA222A224A252A253A254A255A22530A228A66A16A0A246A73A18A109A1A253A2A19A32132A21A222A224A244A228A4A22A237A231A247A248A246DEPTA222A224A2258A228A232A237A66A231A238A240A241A242A24610A228A23A232A237A66A231A238A240A241A242A2464A228A5A232A237A66A231A238A240A241A242A35A24A69A250A6A241A11A246A254A7A252A253A69A40A8A9A10A12A13A239A26A254A255A13A14A3513CNMR100MHZ,CDCL368,146,179,182,186,202,223,281,300,305,318,321,324,327,350,353,356,360,374,383,391,392,413,415,421,428,531,582,594,2132A8A223A155A1A9A10A123A4A54A17A244A20A246A64A25A27A9A10A123A4A35A253A69A409A28A29A143A30A31A32A33A34A36A37MP790810OCA371HNMR400MHZ,CDCL3A3813CNMR100MHZ,CDCL3A39A41A426A43A44A45A46A37A233A47A48A83A49A50A51A52A97A53A55A56A5710A58A58A59A60A61A62A63A65A67A68A70MP17701800OCA701HNMR400MHZ,CDCL3A7113CNMR100MHZ,CDCL3A72A74A756A76A77A70A78A79A80A81A82A84A85A86A87A88A894A90A91A92A92A93A93A250A94A95A96A98A99A100A101A102A103A94A104A105A106A107A108A110A105A111A112A113A114A115A99A100A101A102A116A117A100A101A102A103A94A104A105A118A119A118A120A121A122A123A106A107A108A110A105A124A125A126A127A115A128A129A110A105A130A131A132A133A134A135A116A136A137A138A135A107A139A123A140A107A139A12315A141A142A144A145A146A147A148A149A150A151A152A150A153A154A155A156A157A158A159A1607A1618A162A163A164A141A145A146A165A150A166,A158A159A
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