版权说明:本文档由用户提供并上传,收益归属内容提供方,若内容存在侵权,请进行举报或认领
文档简介
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BRITISHSTANDARD
Compressedair—
Part6:Testmethodsforgaseouscontaminantcontent
ICS71.100.20
NOCOPYINGWITHOUTBSIPERMISSIONEXCEPTASPERMITTEDBYCOPYRIGHTLAW
BSISO
8573-6:2003
Britishstandards
BSISO8573-6:2003
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
Nationalforeword
ThisBritishStandardreproducesverbatimISO8573-6:2003andimplementsitastheUKnationalstandard.
TheUKparticipationinitspreparationwasentrustedtoTechnicalCommitteeMCE/8,Compressors,pneumatictools,pneumaticmachinesandvacuum
technology,whichhastheresponsibilityto:
—aidenquirerstounderstandthetext;
—presenttotheresponsibleinternational/Europeancommitteeany
enquiriesontheinterpretation,orproposalsforchange,andkeepthe
UKinterestsinformed;
—monitorrelatedinternationalandEuropeandevelopmentsandpromulgatethemintheUK.
Alistoforganizationsrepresentedonthiscommitteecanbeobtainedonrequesttoitssecretary.
Cross-references
TheBritishStandardswhichimplementinternationalpublicationsreferredtointhisdocumentmaybefoundintheBSICatalogueunderthesectionentitled“InternationalStandardsCorrespondenceIndex”,orbyusingthe“Search”
facilityoftheBSIElectronicCatalogueorofBritishStandardsOnline.
Thispublicationdoesnotpurporttoincludeallthenecessaryprovisionsofacontract.Usersareresponsibleforitscorrectapplication.
CompliancewithaBritishStandarddoesnotofitselfconferimmunityfromlegalobligations.
ThisBritishStandardwas
publishedundertheauthorityoftheStandardsPolicyand
StrategyCommitteeon
16June2003
©BSI16June2003
ISBN0580420566
Summaryofpages
Thisdocumentcomprisesafrontcover,aninsidefrontcover,theISOtitlepage,pagesiitov,ablankpage,pages1to12,aninsidebackcoverandabackcover.TheBSIcopyrightdatedisplayedinthisdocumentindicateswhenthe
documentwaslastissued.
Amendmentsissuedsincepublication
Amd.No.
Date
Comments
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
INTERNATIONAL
STANDARD
ISO
8573-6
Firstedition2003-05-01
Compressedair—
Part6:
Testmethodsforgaseouscontaminantcontent
Aircomprimé—
Partie6:Méthodesd'essaipourladéterminationdelateneurenpolluantsgazeux
ReferencenumberISO8573-6:2003(E)
ii
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
iii
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
Page
Contents
Foreword iv
Introduction v
1Scope
1
2Normativereferences
1
3Terms,definitions,unitsandsymbols
1
4Selectionguideandavailablemethods
2
5Samplingtechniques
3
6Measurementmethods
5
7Referenceconditions
5
8Evaluationoftestresult
5
9Uncertainty
5
10Testreport
6
AnnexA(informative)Compressedaircontaminantconcentrationreport—Example
7
AnnexB(informative)Measurementandsamplingproceduresonsiteandanalysisinlaboratory
8
AnnexC(informative)Analyticalandon-linesamplingsystems
9
AnnexD(informative)Equipmentforon-sitemeasurement—Samplingandmeasurement
procedures—Samplingingasdetectortube
11
Bibliography
12
iv
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
Foreword
ISO(theInternationalOrganizationforStandardization)isaworldwidefederationofnationalstandardsbodies(ISOmemberbodies).TheworkofpreparingInternationalStandardsisnormallycarriedoutthroughISOtechnicalcommittees.Eachmemberbodyinterestedinasubjectforwhichatechnicalcommitteehasbeenestablishedhastherighttoberepresentedonthatcommittee.Internationalorganizations,governmentalandnon-governmental,inliaisonwithISO,alsotakepartinthework.ISOcollaboratescloselywiththe
InternationalElectrotechnicalCommission(IEC)onallmattersofelectrotechnicalstandardization.
InternationalStandardsaredraftedinaccordancewiththerulesgivenintheISO/IECDirectives,Part2.
ThemaintaskoftechnicalcommitteesistoprepareInternationalStandards.DraftInternationalStandardsadoptedbythetechnicalcommitteesarecirculatedtothememberbodiesforvoting.PublicationasanInternationalStandardrequiresapprovalbyatleast75%ofthememberbodiescastingavote.
Attentionisdrawntothepossibilitythatsomeoftheelementsofthisdocumentmaybethesubjectofpatentrights.ISOshallnotbeheldresponsibleforidentifyinganyorallsuchpatentrights.
ISO8573-6waspreparedbyTechnicalCommitteeISO/TC118,Compressors,pneumatictoolsandpneumaticmachines,SubcommitteeSC4,Qualityofcompressedair.
ISO8573consistsofthefollowingparts,underthegeneraltitleCompressedair:
—Part1:Contaminantsandpurityclasses
—Part2:Testmethodsforaerosoloilcontent
—Part3:Testmethodsformeasurementofhumidity
—Part4:Testmethodsforsolidparticlecontent
—Part5:Testmethodsforoilvapourandorganicsolventcontent
—Part6:Testmethodsforgaseouscontaminantcontent
—Part7:Testmethodforviablemicrobiologicalcontaminantcontent
—Part8:Testmethodsforsolidparticlecontentbymassconcentration
—Part9:Testmethodsforliquidwatercontent
v
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
Introduction
ThispartofISO8573isoneinaseriesofstandards(plannedorpublished)withtheambitionofharmonizingaircontaminationmeasurements.ItisalsointendedtobeusedforreferencewhenstatingpurityclassesaccordingtoISO8573-1.
InthispartofISO8573,gaseouscontaminationofcompressedairmeansthatasampleofcompressedaircouldcontainsmallquantitiesofcarbonmonoxide(CO),carbondioxide(CO2),sulphurdioxide(SO2),hydrocarbonsandoxidesofnitrogen(NOx)—thelatterbeingamixtureofnitricoxide(NO)andnitrogendioxide(NO2),withoutaspecifiedratiobetweenthetwocomponents.ItispossibletoobtainseparateconcentrationvaluesforNOandNO2usingeitherthelaboratoryequipmentrecommendedhereoron-siteequipment,whileundertherecommendedlaboratoryanalyticalprocedure,hydrocarbonsarethesumofavarietyofspeciesassumingaratioofC1H1,85.
blank
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
1
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
Compressedair—
Part6:
Testmethodsforgaseouscontaminantcontent
1Scope
ThispartofISO8573providesaselectionofsuitabletestmethodsfromthoseavailableforthemeasurementofcontaminationgasesincompressedair.Itspecifiessamplingtechnique,measurementandevaluation,uncertaintyconsiderationsandreportingfortheapplicablegaseouscontaminantscarbonmonoxide,carbondioxide,sulphurdioxide,nitricoxide,nitrogendioxideandhydrocarbonsintherangeC1toC5(seeISO8573-5forC6andabove).Themethodsgivenarealsosuitableforothergases.
2Normativereferences
Thefollowingreferenceddocumentsareindispensablefortheapplicationofthisdocument.Fordatedreferences,onlytheeditioncitedapplies.Forundatedreferences,thelatesteditionofthereferenceddocument(includinganyamendments)applies.
ISO1219-1,Fluidpowersystemsandcomponents—Graphicsymbolsandcircuitdiagrams—Part1:Graphicsymbols
ISO2602,Statisticalinterpretationoftestresults—Estimationofthemean—Confidenceinterval
ISO2854,Statisticalinterpretationofdata—Techniquesofestimationandtestsrelatingtomeansandvariances
ISO8573-1,Compressedair—Part1:Contaminantsandpurityclasses
3Terms,definitions,unitsandsymbols
Forthepurposesofthisdocument,thetermsanddefinitionsgiveninISO8573-1,andthesymbolsgiveninISO1219-1apply.SeeTable1foranexplanationoftheunitsandothersymbolsused.
2
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
Table1—Preferredunitsandsymbols(andtheirnon-preferredequivalents)usedinthispartofISO8573
Unit/symbol
Explanation
MPa[bar]
1bar=100000Pa=0,1MPa
ml/m3(=ppmV)a
Volumefractionexpressedinmillilitrespercubicmetre[=onepartpermillion(1ppm)onavolumebasis:1/106(m3/m3)]
ml/m3(=ppmV)C1
Volumefractionexpressedinmillilitrespercubicmetre[=onepartpermillion(1ppm)onavolume
basis:1/106(m3/m3)],referredtoatheoreticalC1-molecule
µg/g(=ppmW)
Massfractionexpressedinmicrogramspergram[=partspermilliononaweightbasisb]
1%byvolume
Volumefractionof1%:1/102(m3/m3)
MPa(e)[bar(e)]
Effectivepressure
MPa(a)[bar(a)]
Referenceconditionabsolutepressure
aPartspermillion(ppm)isadeprecatedunit,i.e.notacceptedbytheInternationalSystemofUnits,SI.See,forexample,ISO31-0:1992,2.3.3.
bIncommonparlance,theword"weight"continuestobeusedtomeanmass,butthispracticeisdeprecated.SeeISO31-3.
4Selectionguideandavailablemethods
Therearetwooptionsforthemeasurementofcontaminantcontent:
a)samplingandanalysison-site;
b)samplingon-site,analysisinthelaboratory.
TherecommendedmethodsandequipmentwithintheseoptionsaregiveninTable2.
Table2—Recommendedmeasurementmethods/equipment
Gaseous
contaminant
Measurementequipment
Off-site
Carbonmonoxide
(CO)
Non-dispersiveinfrared(NDIR)absorptionspectrometer
Carbondioxide(CO2)
Non-dispersiveinfrared(NDIR)absorptionspectrometer
Sulphurdioxide(SO2)
Non-dispersiveinfrared(NDIR)absorptionspectrometer
UV-fluorescence
Hydro-carbons(HC)(C1toC5)
Heatedflameionisationdetector(HFID)
Nitrogenoxides(NOx)
Chemiluminescentdetector(CLD)withanNO2/NOconverter,andinaheatedversion(HCLD)
On-site
Allidentifiedgases
Gasdetectortubeswithcolourchange
3
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
5Samplingtechniques
5.1Gassamplinginbags
Thegassampleshallbetakenatatmosphericconditionsandcollectedinaspecialgassamplingbagmadeforthepurpose.Asampleofthecompressedairshallbecollectedinagassamplingbagfortheevaluationofthecontaminantconcentrationvalues.Allmeasurementsonthesampleshallbecarriedoutunderatmosphericpressureconditions.
Useofacommerciallyavailablegassamplingbag(e.g.onemadeoffluoroethylenepropylene)tocollectasampleofairforanalysisshouldbemadebythefollowingmethod.
Thegassamplingbagshouldbeofthetypesuitableforgascollection.Turbulentflowconditionsarerequiredinthemainsystempipetoensureamixingofthegaseouscontaminantstogivearepresentativesampleoftheair.
Connectthegassamplingbagtothesamplingpointusingaprobe(seeFigure1),throughapressurereducingvalve,byapolytetrafluoroethylene(PTFE)tubeandaPTFE,orstainlesssteel,connector,dependingupontheexpectedgasimpurities.Thepipingshouldbeprotectedfromthepossibleformationcondensation.Thebagshouldhaveaventvalvetoallowforflushing.Flushingshouldtakeplacefor5minwithsystemairbeforetakingthesample.Careshouldbetakentoensurethatthebagisnotover-inflatedandofasizeconsistentwiththesamplerequired.Thebagshouldonlybere-usedifpermittedbythemanufacturer.
Togetherwiththefilledgas-samplingbaganemptyunusedgas-samplingbagshallbebroughttothelaboratoryforablindtest.
5.2On-linesampling
Thegassampleshallbetakenatsystempressureusingastainlesssteelprobe(seeFigures1and2).Theendoftheprobeoutsidethecompressedairpipeshallhaveavalve,whichshallbesuitableforallpressureconditionsofthecompressedairpipe.Theprobeshallbefreefromcontaminantsaffectingthereadings.
SeeAnnexCfortheprocedure.
5.3Samplingingasdetectortube
SeeAnnexDfortheprocedure.
4
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
1directionofflow
2crevice-freejoint
3suitablepressure-tightthreadconnection4tomembraneholder
BSISO8573−6:2003
Key
123abc
d
samplingprobeinthemainpipe
adjustableglandtoallowadjustmentofprobe
directionofairflow
mainpipediameter,D
minimumstraightlengthbeforeprobe,10×D
probeinsertionpointatminimumof3×D
internalprobediameter,d
sampling
Figure1—Equipmentset-upofprobeinsertionfor
Key
Probe
size
A
mm
B
mm
C
mm
1
7
9,6
200
2
10
12,6
200
3
17
19,6
400
Figure2—Stainlesssteelsamplingprobe
5
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
6Measurementmethods
TherecommendedprocedurefortheevaluationofthecontaminantconcentrationvaluesinalaboratoryisgiveninAnnexC.TheanalyticalequipmentproposedforusebyAnnexCisbasedonthedetectorprinciplesidentifiedinTable2.
Considerationshallbegiventothemeasurementsystemintegrityandthecalibrationrequirementsofthemeasurementequipment,whichshallbeusedinaccordancewiththeapplicableinstructionsandtothedegreeofgaseouscontaminationmeasured.
Forthemeasurementoftheconcentrationvalues,on-sitegasdetectortubesmaybeemployed.Thisoffersadirectreadingfromascaleviaachemicalreactionwithacolourchangeproportionaltotheactualcontaminantconcentrationintheactualcompressedairsampletaken.SeeAnnexD.
7Referenceconditions
Unlessotherwiseagreed,thereferenceconditionsforgaseouscontaminantconcentrationshallbeinaccordancewithTable3:
Table3—Referenceconditions
Airtemperature
20°C
Airpressure
0,1MPa(a)
[1bar(a)]
Relativewatervapourpressure
0
8Evaluationoftestresult
Theresultsofthemeasurementsaregivenasconcentrationvaluesofthecontaminantsasvolumefractionsorpercentagesbyvolume.SeeTable1.
9Uncertainty
NOTEAcalculationoftheprobableerroraccordingtothisclauseisnotalwaysnecessary.
Duetotheverynatureofphysicalmeasurementsitisimpossibletomeasureaphysicalquantitywithouterroror,infact,todeterminethetrueerrorofanyparticularmeasurement.However,iftheconditionsofthemeasurementaresufficientlywellknown,itispossibletoestimateorcalculateacharacteristicdeviationofthemeasuredvaluefromthetruevalue,suchthatitcanbeassertedwithacertaindegreeofconfidencethatthetrueerrorislessthanthesaiddeviation.Thevalueofsuchdeviation(normally95%confidencelimit)constitutesacriterionoftheaccuracyoftheparticularmeasurement.
Itisassumedthatallsystematicerrorsthatmayoccurinthemeasurementoftheindividualquantitiesmeasuredandofthecharacteristicsofthegascanbecompensatedforbycorrections.Afurtherassumptionisthattheconfidencelimitsinerrorsinreadingandintegrationerrorsmaybenegligibleifthenumberofreadingsissufficient:the(small)systematicerrorsthatcouldoccurarecoveredbytheinaccuracyofmeasurements.
Theinformationaboutassertingtheuncertaintyofmeasurementofindividualquantitiesmeasuredandon
confidencelimitsofthegaspropertiesareapproximations.Theseapproximationscanonlybeimprovedby
effortsofdisproportionateexpense(seeISO2602andISO2854).
6
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
10Testreport
10.1Statements
Statementsoftheconcentrationofgaseouscontaminantsinthecompressedairshallbemadeasvolumefractions(seeTable1).ThestatementshallbesufficientlydetailedtoallowthevaluestobeverifiedaccordingtotheproceduresofthispartofISO8573.
10.2Statementformat
Thereport/statementusedtodeclaretheconcentrationofgaseouscontaminantsinaccordancewiththispart
ofISO8573shallcontainthefollowinginformation:
a)adescriptionofthecompressedairsystemanditsworkingconditions,withsufficientdetailtoenablethe
applicabilityofthedeclaredconcentrationvaluetobedetermined;
b)adescriptionofthesamplingpointwherethesamplesweretaken;
c)adescriptionofthesamplingandanalyticalsystemthatwasused(particularlymaterialsused)anddetailsofitscalibrationrecordifapplicable;
d)thewords“DeclaredconcentrationofthecontaminantCO/CO2/SO2/HC/NO/NO2inaccordancewithISO8573-6”,followedby
—thefigurefortheactual,averagemeasuredvalueevaluatedaccordingtoClause8,
—theactualatmosphericconditions,and
—thedateofthesamplingandmeasurement;
e)astatementregardingtheapplicableuncertainty.
SeeAnnexAforanexamplereport.
7
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
AnnexA
(informative)
Compressedaircontaminantconcentrationreport—Example
SeeFigureA.1.
Statement
Inthecompressedairsystemat,consistingoffouraircompressors,after-coolersand
refrigeranttypedryers,withonecompressoronstand-by,twocompressorsworkingatfullloadandonecompressorloadedtoapprox.50%andworkingat0,7MPa(e)[=7bar(e)]networkpressure,measurementsontheconcentrationsCO,CO2,SO2,HCandNO2weremade.TheprobetoobtainthesampleswasinstalledwherethesupplypipeenterstheB-shop.
Samplesweretakenregularlyathourlyintervalsduringa48hperiod.
Eachsampleconsistedofthreeplasticgascollectionbags,manufacturedby
Atmosphericconditionsduringsamplingandmeasurementwereasfollows:
Startingdate:
19,5。C
0,1015MPa
49%relativehumidity
Finishingdate:
22。C
0,1016MPa
42%relativehumidity
NOTEAverageof48samplesforeverythreemeasurements.
Theanalysiswasmadeinlaboratory,withtheanalyticalequipmentmanufacturedby
Thecalibrationoftheanalyticalequipmentwasvalidatedon
Beforeandaftereachmeasurement,theanalysersettingwascontrolledbyspanandzerogases.
ThedeclaredconcentrationsinaccordancewithISO8573-6areasfollows:
Carbonmonoxide(CO)
(12±4)ml/m3orppmV
usedfullscalerange
(0to25)ml/m3orppmV
Carbondioxide(CO2)
(349±8)ml/m3orppmV
usedfullscalerange
(0to1000)ml/m3orppmV
Sulphurdioxide(SO2)
<3ml/m3orppmV
usedfullscalerange
(0to10)ml/m3orppmV
Hydro-carbons(HC)
(2±1)ml/m3C1orppmVC1
usedfullscalerange
(0to10)ml/m3C1orppmVC1
Nitrogenoxides(NOx)
<3ml/m3orppmV
usedfullscalerange
(0to10)ml/m3orppmV
Reportpreparedby,
(Signature)(Location,date)
FigureA.1—Examplereport
8
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
AnnexB
(informative)
Measurementandsamplingproceduresonsiteandanalysisinlaboratory
B.1Gassamplingbag
Thegassamplingbagsshallbegas-tight.
Thematerialofwhichthebagsaremanufacturedshallbeinert.
Thegassamplingbagsshallhavefittingsforinflatinganddischargeofsampletoagaschromatograph.
EXAMPLESamplingthroughamembraneusingagas-tightsyringe.
Thegassamplingbagsshallbeidentifiedwithtemperature-specificationsforthesakeofthetemperatureofthegassampledfromthesystem(compatibilitywithtemperatureforbagandsample).
Ifsulphurcompoundsinthecompressedairareexpectedtobefound,gassamplingbagswithblacklayersandfittingsofpolytetrafluoroethylene(PTFE)shouldbeused.
Undernocircumstanceshallstainlesssteelbeusedinsamplingvesselswhensulfurcompoundsarepresent.
B.2Samplingonsite
ThesampleshallbetakeninaccordancewithClause6.
B.3Analysinginlaboratory
Theanalysisofthegassampleshallbecarriedoutinaccordancewiththerecommendationsmadebyappropriateorganizations.
9
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
AnnexC
(informative)
Analyticalandon-linesamplingsystems
C.1Determinationofgaseouscontaminants
Thisannexpresentstheanalyticalsystemforgaseouscontaminants.Othersystemsoranalysersprovedtohavegivenequivalentresultsmaybeused.SeeFigureC.1foraschematicdiagramofthecompressedairanalysissystemandTableC.1forthesymbolsusedintheschematic.
Key
4
5
vent
zerogas
1air
2fuel
3spangas
FigureC.1—CompressedairanalysissystemforCO,CO2,SO2,NOx(analysisbyHCLDandheated
sampleline)andHC(analysisbyHFIDandheatedsampleline)
10
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
TableC.1—KeytosymbolsusedinFigureC.1
Symbol
Description
Symbol
Description
A
bagwithsample
R1,R2
pressureregulatorsforairandfuel
B
bathtocoolandcondensewaterfromsamplea
R3,R4,R5
pressureregulatortocontrolsampleflow
C
converterfortheNO2toNOconversion
SL
samplelinec
CAS
compressedairsample
SO2
NDIRanalyserforsulphurdioxide
CO
NDIRanalyserforcarbonmonoxide
SP
samplepointpressurecontrolandflowmonitoringfromthecompressedairpipe
CO2
NDIRanalyserforcarbondioxide
T1
thermometerofsamplestreamenteringHFIDanalyser
FL1,FL2,FL3
flowmetertomeasuresampleby-passflow
T2
thermometerofsamplestreamenteringHCLDanalyser
FL4,FL5,FL6,
FL7
flowmeterformeasuringflowthrough
analysers
T3
thermometerofNO2toNOconverter
G1,G2,G3
pressuregaugeformeasuringpressureinsamplelinestoanalysers
T4
thermometerofbathtemperature
HC
HFID
V1
valvefortakingsampleandclosingofsampleprobeline
HCLD
HCLDanalyserforoxidesofnitrogen
V10,V11
needlevalvestoregulateflowstotheanalysers
HFID
HFIDanalyserforhydrocarbons
V2,V3,V4,V5,V6
valvestodirectsample,zerogasorcalibratinggasstreamstotheanalysers
HSL1,HSL2
heatedsamplinglinesmadeinstainlesssteelorPTFEb
V7,V8
three-wayvalvetoby-passNO2toNOconverter
NO
heatedchemiluminescentdetector(HCLD)
V9
needlevalvetobalanceflowthroughNO2toNOconverterandby-pass
P
pump
V12,V13,V14
needlevalvestoproviderestrictionto
exhaustingairfrompressurereducingvalves
a
b
c
Thebathshallbemaintainedatatemperatureof0。to+4。Cbyiceorrefrigeration.
Thetemperatureshallbekeptbetween95。Cand200。C.
ThelineshallbemadeinPTFEorinstainlesssteel.Itmaybeheatedorunheated.
C.2Measurementofsamples
Aftercontrolofthesettingoftheanalysers,recordedonastripchartrecorderorwithanequivalentdataacquisitionsystem,thebagwiththesampleisconnectedtotheanalyticalsystematthethree-wayvalvewhilstroomairorsyntheticairispumpedthroughthesystem.Thenthevalveisswitchedtothepositionwherethesampleispumpedthroughthesystemsothattheanalysersshowthereadingofthecontaminantconcentration.Thereadingmustbestableforatleast3mininorderforaconcentrationvaluerepresentativeofthatsampletobeproduced.Thereadingisrecordedduringthewholetime.Theactualconcentrationvaluescanbeproducedmanuallyviainterpretationoftherecordorviaanelectronicdataevaluationdevicewhichidentifiesautomaticallyastableresponseoftheanalysersforaperiodof3minandthenprintstheconcentrationvalues.
11
LicensedCopy:LondonSouthBankUniversity,LondonSouthBankUniversity,FriDec2217:26:08GMT+00:002006,UncontrolledCopy,(c)BSI
BSISO8573−6:2003
AnnexD
(informative)
Equipmentforon-sitemeasurement—Samplingandmeasurementprocedures—Samplingingasdetectortube
D.1Samplingequipment
Thesampleistakenfromthecompressedairline.Themeasuredconcentrationcanberecognizedastheprogressofthecolourchangefrontalareawithreferencetothescaleontheglasstube.Thesamplingmeasurementshouldberepeatedtoarriveatanacceptableconfidencelevel.
FigureD.1showsaschematicdiagramofapossiblearrangementusingthedetectortubetechnologyasananalyticalsystem.
Key
1compressedairsystem(samplingpoint)
2pressureregulator
3needledosagevalve
4flowmeter
5detectortube
6pressuregauge
FigureD.1—Examplearrangementusinggasdetectortubemethod
D.2Measurementequipment
Theprocedureformeasuringtheconcentrationvaluesofgasesthatcouldbecontaminatingacompressedairsupplyisdescribedhere.Themethod,whichiswidelyused,iscommonlyidentifiedasdetectortubes.
Detectortubesareavailablefornearlyallrelevantgaseouscontaminantsand,insomecases,formorethanonecontaminant.SeeEN1231.
Theprincipleofthesedetectortubesisaspecificchemicalreactionofthecomponenttobemeasuredwithachangeofcolour.Thereisadefinedamountofreagentequi
温馨提示
- 1. 本站所有资源如无特殊说明,都需要本地电脑安装OFFICE2007和PDF阅读器。图纸软件为CAD,CAXA,PROE,UG,SolidWorks等.压缩文件请下载最新的WinRAR软件解压。
- 2. 本站的文档不包含任何第三方提供的附件图纸等,如果需要附件,请联系上传者。文件的所有权益归上传用户所有。
- 3. 本站RAR压缩包中若带图纸,网页内容里面会有图纸预览,若没有图纸预览就没有图纸。
- 4. 未经权益所有人同意不得将文件中的内容挪作商业或盈利用途。
- 5. 人人文库网仅提供信息存储空间,仅对用户上传内容的表现方式做保护处理,对用户上传分享的文档内容本身不做任何修改或编辑,并不能对任何下载内容负责。
- 6. 下载文件中如有侵权或不适当内容,请与我们联系,我们立即纠正。
- 7. 本站不保证下载资源的准确性、安全性和完整性, 同时也不承担用户因使用这些下载资源对自己和他人造成任何形式的伤害或损失。
最新文档
- 款服装批发购销合同
- 加盟合同解除的合法性分析
- 广告制品买卖合同
- 企业劳动合同补充协议的解读
- 农肥销售协议模板
- 餐馆垃圾清运处理协议
- 区域代理合同书范例
- 人工承包合同协议范本格式格式格式
- 不再沉迷打牌的誓言
- 企业在职业健康与环境保护方面的最佳实践案例考核试卷
- 2024秋期河南开放大学本科《法律社会学》一平台无纸化考试(作业练习1至3+我要考试)试题及答案
- 生猪屠宰兽医卫生人员考试题库答案(414道)
- 花木绿化养护考核评分表
- 塑胶件外观检验标准
- 肾上腺皮质激素类药ppt课件.ppt
- 制造中心年度工作计划供应链中心年度工作计划(2020年)
- 刮泥机出厂检测调试报告
- 工业管道基础知识PPT课件
- 运动处方知识点
- 英语口语绕口令Englishtonguetwisters
- 《八字新大陆》教材内部辅导讲义
评论
0/150
提交评论