南京土壤检测中心-CNAS.doc

ISO/IEC 17025 认可证书 CNAS-PD20/09-B/1中国合格评定国家认可委员会认 可 证 书 附 件（注册号：CNAS L2464）名称: 中国科学院南京土壤研究所土壤与环境分析测试中心 地址：江苏省南京市北京东路71号签发日期：2010年12月10日 有效期至：2013年12月09日更新日期：2012年04月09日附件1 认可的授权签字人及领域序号姓 名授权签字领域备 注1章钢娅土壤、空气、植物与食品、水、肥料的检测项目2曹亚澄土壤、空气、植物与食品、水、肥料的检测项目CHINA NATIONAL ACCREDITATION SERVICE FOR CONFORMITY ASSESSMENTAPPENDIX OF ACCREDITATION CERTIFICATE(Registration No. CNAS L2464) NAME:Soil and Environment Analysis Center of Nanjing Institute of Soil Science, Chinese Academy of Sciences ADDRESS:No.71, Beijing East Road, Nanjing, Jiangsu, ChinaDate of Issue:2010-12-10 Date of Expiry:2013-12-09 Date of Update：2012-04-09APPENDIX 1 ACCREDITED SIGNATORIES AND SCOPEName Authorized Scope of SignatureNote1Zhang GangyaAll approved projects2Cao YachengAll approved projects 中国合格评定国家认可委员会认 可 证 书 附 件（注册号：CNAS L2464）名称: 中国科学院南京土壤研究所土壤与环境分析测试中心 地址：江苏省南京市北京东路71号认可依据：ISO/IEC 17025:2005以及CNAS特定认可要求签发日期：2010年12月10日 有效期至：2013年12月09日更新日期：2012年04月09日附件2 认可的检测能力范围序号检测对象项目/参数领域代码检测标准（方法）名称及编号（含年号）限制范围说明序号名称1土壤1pH0238LY/T 1239-1999 森林土壤pH值的测定2有机质0238LY/T 1237-1999 森林土壤有机质的测定及碳氮比的计算3水分0238LY/T1213-1999森林土壤含水量的测定4全氮0238NY/T 53-1987土壤全氮测定法(半微量凯氏法)1土壤5全磷0238LY/T 1232-1999森林土壤全磷的测定6有效磷0238LY/T 1233-1999森林土壤有效磷的测定7全钾0238LY/T 1234-1999森林土壤全钾的测定8速效钾0238LY/T 1236-1999森林土壤速效钾的测定9水溶性 盐分0238LY/T 1251-1999森林土壤水溶性盐分分析10有效铜0238LY/T 1260-1999森林土壤有效铜的测定11有效锌0238LY/T 1261-1999森林土壤有效锌的测定12有效铁0238LY/T 1262-1999森林土壤有效铁的测定13六六六、 滴滴涕0238GB/T 14550-2003土壤中六六六和滴滴涕测定的气相色谱法14碳稳定性同位素比值0238有机化合物的碳同位素质谱分析土壤农业化学分析方法中国农业科技出版社，1999年，564-570页15氮稳定性同位素比值0238氮同位素质谱分析土壤农业化学分析方法中国农业科技出版社，1999年，558-564页。16总铬0238HJ 4912009土壤 总铬的测定 火焰原子吸收分光光度法不用6.2.21土壤17铅, 镉0238GB/T 171411997土壤质量 铅、镉的测定 石墨炉原子吸收分光光度法18铜, 锌0238GB/T 171381997土壤质量 铜、锌的测定 火焰原子吸收分光光度法19总汞0238GB/T 22105.1-2008土壤质量 总汞、总砷、总铅的测定 原子荧光法 第1部分：土壤中总汞的测定20总砷0238GB/T 22105.2-2008土壤质量 总汞、总砷、总铅的测定 原子荧光法 第2部分：土壤中总砷的测定21电导率0238DIN ISO 11265-1997 土壤质量.特定电导率的测定22水解性氮0238LY/T 1229-1999 森林土壤水解性氮的测定23铵态氮、硝态氮、亚硝态氮0238ISO 14256-2-2005土壤质量-氯化钾萃取法测定潮湿土壤中的硝酸盐、亚硝酸盐和氨盐基的含量-第2部分: 以分段流程分析进行的自动测定方法24氯离子0238NY/T 1121.17-2006 土壤检测 第17部分：土壤氯离子含量的测定 仅用前处理方法24氯离子0238HJ/T 84-2001 水质 无机阴离子的测定 离子色谱法仅用测定方法1土壤25硫酸根离子0238NY/T 1121.18-2006 土壤检测 第18部分:土壤硫酸根离子含量的测定HJ/T84-2001 水质 无机阴离子的测定 离子色谱法26矿质全量0238偏硼酸锂熔融-ICP-AES法 土壤农业化学分析方法中国农业科技出版社，1999年，45-47页。27全钙、镁、钠0238NY/T 296-1995土壤全钙、镁、钠的测定28镍0238GB/T 17139-1997土壤质量 镍的测定 火焰原子吸收分光光度法29全硒0238NY/T 1104-2006 土壤中全硒的测定 原子荧光光度法30有机磷农药0238GB/T 14552-2003水和土壤质量 有机磷农药的测定 气相色谱法31石油烃0238GB/T 17378.5-2007 海洋监测规范 第5部分:沉积物分析2空气32空气中N2O氮、氧同位素比值0238GB/T 6041-2002质谱分析方法通则； 大气浓度下N2O、CH4和CO2中氮、碳和氧稳定同位素比值的质谱测定，土壤学报，2008,第45卷，第2期，249-258页。2空气33空气中CH4碳同位素比值0238GB/T 6041-2002质谱分析方法通则； 大气浓度下N2O、CH4和CO2中氮、碳和氧稳定同位素比值的质谱测定，土壤学报，2008,第45卷，第2期，249-258页。34气体中N2氮同位素比值023835空气中CO2碳、氧同位素比值023836气体中CH4含量0238GB/T 8984-2008气体中一氧化碳、二氧化碳和碳氢化合物的测定第1部分：气体中一氧化碳、二氧化碳和甲烷的测定气相色谱法37气体中CO2含量0238GB/T 18204.24-2000 气体中一氧化碳、二氧化碳和碳氢化合物的测定3植物与食品38六六六、 滴滴涕0227GB/T5009.19-2008食品中有机氯农药多组分残留量的测定39植物粗灰分的测定0244GB/T5009.4-2010食品中灰分的测定40全氮0227LY/T 1269-1999森林植物与森林枯枝落叶层全氮的测定3植物与食品41全磷0227LY/T 1271-1999 森林植物与森林枯枝落叶层全氮、磷、钾、钠、钙、镁的测定42全钾0227LY/T 1271-1999 森林植物与森林枯枝落叶层全氮、磷、钾、钠、钙、镁的测定43镉0227GB/T 5009.15-2003食品中镉的测定只做第一法44总汞0227GB/T 5009.17-2003食品中总汞及有机汞的测定只做第一法45铅0227GB/T5009.12-2010食品中铅的测定只做第一法46硒0227GB 5009.932010 食品安全国家标准食品中硒的测定只做第一法47碳稳定性同位素比值0244有机化合物的碳同位素质谱分析土壤农业化学分析方法中国农业科技出版社，1999年，564-570页48氮稳定性同位素比值0244氮同位素质谱分析土壤农业化学分析方法中国农业科技出版社，1999年，558-564页。4水49pH0238GB/T 6920-1986水质 pH值的测定 玻璃电极法50铜，锌， 铅，镉0238GB/T 7475-1987水质 铜，锌，铅，镉的测定 原子吸收分光光度法4水51铵0238ISO 11732-2005 水质 氨氮的测定.流动分析(CFA和FIA)和光谱测定法52硝酸盐氮0238ISO 13395-1996 水质用流动分析(CFA 和FIA)和光谱检测法测定水中亚硝酸盐氮和硝酸盐氮及二者的总量53电导率0238DZ/T0064.6-1993地下水质检测方法电导率的测定54全盐量0238HJ/T 51-1999水质 全盐量的测定 重量法55全钾0238EPA 200.7 水、固体、生物固体 痕量元素的测定 电感耦合等离子体原子发射光谱法56碳酸根、重碳酸根0238DZ/T0064.49-1993地下水质检测方法 滴定法测定碳酸根、重碳酸根和氢氧根57氯离子和 硫酸根0238HJ/T84-2001 水质 无机阴离子的测定 离子色谱法58磷酸盐0238ISO 10304-1-2007 水质-用离子色谱法测定溶解的阴离子-第1部分：溴化物、氯化物、氟化物、硝酸盐、亚硝酸盐、磷酸盐和硫酸盐的测定4水59铝0238EPA 200.7 水、固体、生物固体 痕量元素的测定 电感耦合等离子体原子发射光谱法60钙、镁0238EPA 200.7 水、固体、生物固体 痕量元素的测定 电感耦合等离子体原子发射光谱法61铁、锰0238EPA 200.7 水、固体、生物固体 痕量元素的测定 电感耦合等离子体原子发射光谱法62汞0238SL 327.2-2005 水质 汞的测定 原子荧光光度法63钠0238EPA 200.7 水、固体、生物固体 痕量元素的测定 电感耦合等离子体原子发射光谱法64镍0238EPA 200.7 水、固体、生物固体 痕量元素的测定 电感耦合等离子体原子发射光谱法65砷0238SL 327.1-2005 水质 砷的测定 原子荧光光度法66硒0238SL 327.3-2005 水质 硒的测定 原子荧光光度法4水67六六六、 滴滴涕0238GB/T 7492-1987水质 六六六、滴滴涕的测定 气相色谱法68有机磷农药0238GB/T 14552-2003 水、土中有机磷农药测定的气相色谱法69六价铬0238GB/T 7467-1987水质 六价铬的测定 二苯碳酰二肼分光光度法5肥料70总氮0232GB/T 17767.1-2008有机-无机复混肥料的测定方法 第一部分:总氮含量71总磷0232GB/T 17767.2-2010有机无机复混肥料中总磷含量的测定72总钾0232GB/T 17767.3-2010 有机-无机复混肥料中总钾含量的测定73汞、砷、镉、铅、铬0232NY 1110-2006 水溶肥料汞、砷、镉、铅、铬的限量及其含量测定No. CNAS L2464 第 28 页 共 28 页 The scope of the accreditation in Chinese remains the definitive version. CHINA NATIONAL ACCREDITATION SERVICE FOR CONFORMITY ASSESSMENTAPPENDIX OF ACCREDITATION CERTIFICATE(Registration No. CNAS L2464) NAME:Soil and Environment Analysis Center of Nanjing Institute of Soil Science, Chinese Academy of Sciences ADDRESS:No.71, Beijing East Road, Nanjing, Jiangsu, ChinaAccreditation Criteria:ISO/IEC 17025:2005 and relevant requirements of CNASDate of Issue:2010-12-10 Date of Expiry:2013-12-09 Date of Update：2012-04-09APPENDIX 2 ACCREDITED TESTINGTest ObjectItem/ParameterCode of Field Title, Code of Standard or Method Limitation NoteItem/ Parameter1Soil1pH0238LY/T1239-1999Determination of pH value in forest soil2OrganicMatter0238LY/T 1237-1999Determination of organic matter in forest soil and calculation carbon-nitrogen ratio3Water Content0238LY/T1213-1999Determination of forest soil water content1Soil4Total Nitrogen0238NY/T 53-1987Method for the determination of soil total nitrogen(Semi-micro Kjeldahl method)5TotalPhosphorus0238LY/T1232-1999Determination of total phosphorus in forest soil6AvailablePhosphorus0238LY/T1233-1999Determination of available phosphorus in forest soil7TotalPotassium0238LY/T1234-1999Determination of total potassium in forest soil8AvailablePotassium0238LY/T1236-1999Determination of available potassium in forest soil9Water soluble salts of soil0238LY/T 1251-1999Analysis methods of water soluble salts of forest soil10AvailableCopper0238LY/T 1260-1999Determination of available copper in forest soil11AvailableZinc0238LY/T 1261-1999Determination of available zinc in forest soil1Soil12AvailableIron0238LY/T 1262-1999Determination of available iron in forest soil13BHC, DDT0238GB/T 14550-2003Method of gas chromatographic for determination of BHC and DDT in soil14C isotope-ratio analysis0238C isotope-radio mass spectrum analysis in organic compounds China Agricultural Science &Technology Press, 1999. p. 564-57015N isotope-ratio analysis0238N isotope radio mass spectrum analysis China Agricultural Science &Technology Press, 1999. p.558-5641Soil16TotalChromium0238HJ 4912009Soil quality Determination of total chromium Flame atomic absorption spectrometryExcept for 6.2.217Lead,Cadmium0238GB/T 171411997Soil quality-Determination of lead,cadmium-Graphite furnace atomic absorption spectrophotometry18Copper, Zinc0238GB/T 171381997Soil quality-Determination of copper, zinc-Flame atomic absorption spectrophotometry19Mercury0238GB/T 22105.1-2008Soil quality-Analysis of total mercury, arsenic and lead contents-Atomic fluorescence spectrometry-Part1：Analysis of total mercury contents in soils1Soil20Total Arsenic0238GB/T 22105.2-2008Soil quality-analysis of total mercury, arsenic and lead contents-Atomic fluorescence spectrometry-Part2：Analysis of total arsenic contents in soils21Conductivity0238DIN ISO 11265-1997Soil quality-Determination of the specific electrical conductivity22HydrolyzableNitrogen0238LY/T 1229-1999Determination of hydrolyzable nitrogen in forest soil23Ammonia,Nitrate,Nitrite Nitrogen0238ISO 14256-2-2005Soil quality-Determination of nitrate, nitrite, and ammonium in field-moist soils by extraction with potassium chloride solution-Part2: Automated method with segmented flow analysis1Soil24Chloride0238NY/T 1121.172006Soil Testing Part 17: Method for determination of soil chloride ion contentAccredited only for treatment methodHJ/T 84-2001Water quality-Determination of inorganic anions-Ion chromatography methodAccredited only for determination method25Sulfate0238NY/T 1121.18-2006Soil Testing Part 18: Method for determination of soil sulfate contentHJ/T 84-2001Water quality-Determination of inorganic anions-Ion chromatography method26Mineral Total Elements0238Lithium metaborate fusion-ICP-AES method China Agricultural Science &Technology Press, 1999. p. 45-571Soil27Total calcium,magnesium,sodium0238NY/T 296-1995Determination of total calcium, magnesium, sodium in soil28Nickel0238GB/T17139-1997Soil quality-Determinationof nickel-Flame atomic absorption spectrophotometry29Total Selenium0238NY/T 1104-2006Determination of selenium in soils Atomic fluorescence spectrometry method30Organo-phosphorus pesticides0238GB/T 14552-2003Method of gas chromatographic for determination of organophosphorus pesticides in water and soil31Petroleum-hydrocarbon0238GB 17378.5-2007The specification for marine monitoring-Part 5: Sediment analysis2Air32N、O Isotopic composition to N2O in air0238GB/T 6041-2002 General rules for mass spectrometric analysis; Determination of nitrogen, carbon and oxygen stable isotope ratio in N2O, CH4 and CO2 at natural abundance levels by Mass Spectrometry，Acta pedologica sinca,Vol.45,No.2,Mar.,2008，pp249-25833C Isotopic composition to CH4 in air023834N Isotopic composition to N2 in air023835C、O Isotopic composition to CO2 in air023836CH4 content0238GB/T 8984-2008Determination of carbon monoxide, carbon dioxide and hydrocarbon in the gases-Gas chromatographic method2Air37CO2 content0238GB/T 18204.24-2000 Methods for determination of carbon dioxide in air of public place3Plant andFoods38BHC, DDT0227GB/T5009.19-2008Determination of organochlorine pesticide multiresidues in foods39Ash0244GB/T5009.4-2010Determination of ash in foods40Total nitrogen,phosphorus,potassium0227LY/T 1269-1999 Determination of total nitrogen in forest plant and forest floor41Total phosphorus0227LY/T 1271-1999Determination of total nitrogen, phosphorus, potassium, sodium, calcium, magnesium in forest plant and forest floor3Plant andFoods42Total potassium0227LY/T 1271-1999Determination of total nitrogen, phosphorus, potassium, sodium, calcium, magnesium in forest plant and forest floor43Cadmium0227GB/T5009.15-2003Determination of cadmium in foodsAccredited only for the first method44Total mercury0227GB/T 5009.17-2003Determination of total mercury and organic-mercury in foodsAccredited only for the first method45Lead0227GB/T5009.12-2010Determination of lead in foodsAccredited only for the first method46Selenium0227GB 5009.932010 National food safety standard Determination of selenium in foodsAccredited only forthe first method3Plant andFoods47C isotope-ratio analysis0244C isotope-radio mass spectrum analysis in organic compounds China Agricultural Science &Technology Press, 1999. p. 564-57048N isotope-ratio analysis0244N isotope radio mass spectrum analysis China Agricultural Science &Technology Press,1999 p. 558-56449pH0238GB/T6920-1986Water quality-Determination of pH value-Glass electrode method50Copper, Zinc, Lead,Cadmium0238GB/T 7475-1987Water quality-Determinationof copper, zinc, lead, cadmium-Atomic absorption spectrometry3Plant andFoods51Ammonium0238ISO 11732-2005 Water quality - Determination of ammonium nitrogen - Method by flow analysis (CFA and FIA) and spectrometric detection4Water52Nitrate0238ISO 13395-1996 Water quality - Determination of nitrite nitrogen and nitrate nitrogen and the sum of both by flow analysis (CFA and FIA) and spectrometric detection53Conductivity0238DZ/T0064.6-1993 Analysis method of ground water quality-Determination of electrical conductivity54Total salt0238HJ/T 51-1999Water quality-Determination of total salt-Gravimetric method4Water55Total potassium0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry56Carbonate,Bicarbonate0238DZ/T0064.49-1993Analysis method of ground water quality-Determination of carbonate, bicarbonate and hydroxyl-Titrimetric method57Chloride,Sulfate0238HJ/T 84-2001Water quality-Determination of inorganic anions-Ion chromatography method58Phosphate0238ISO 10304-1-2007Water quality-Determination of dissolved anions by liquid chromatography of ions-Part 1: Determination of bromide, chloride, fluoride, nitrate, nitrite phosphate and sulfate4Water59Aluminium0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry60Calcium,magnesium0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry61Iron,manganese0238EPA 200.7 Trace elements in water, solids, and biosolids by inductively coupled plasma-atomic emission spectrometry62Mercury0238SL 327.2-2005Water quality-determination of mercury-atomic fluore