纯化水管线酸洗钝化方案

1、附件20卫生级管路酸洗钝化方案Sanitary Pipe Chemical Pickled & Passivation Procedure起草/审核签名日期起草人审核/批准TABLE OF CONTENTS1 编制方案的依据 Basis of scheme compilation 32 工作范围 Working scope 33 清洗工艺 Cleaning process 34 清洗过程 Cleaning process 55 废液处理 Waste liquor treatment 96 甲方提供的条件 Condition supplied by theowner 97 临时配管 Te

2、mporary tubing 108 检验与验收 Test and accept 1.09 安全1.1.1 编制方案的依据 Basis of scheme compilation1.1 管道活洗的必要性 Necessity of piping cleaning纯化水不锈钢管道在使用前，要进行脱脂、酸洗、钝化和消蠹处理，管道 才能达到生产使用的技术要求。Before used stainless steel piping for purified water should be degreased, pickled, passivity and disinfected. Only in this

3、 way can piping meet technical needs of production and usage.1.2 脱脂工程施工及验收规范HG20202-2000Construction and Acceptance Criteria of Industrial Piping1.3 工业设备化学活洗质量标准HG/T2387-2007Quality Criteria of Chemical Cleaning for Industrial Equipment1.4 VWS提供的图纸Drawings supplied by VWS1.5管线的材质为全部为316L,如有其它材质，活洗前必

4、须说明。Material of pipeline is all 316L. Give a description of the material before cleaning if other materials are used.2 工作范围 Working scope主要为卫生级不锈钢SS316L管道Mainly for sanitary SS316L pipe.2.1从纯水制造机到纯水TANK®口前级的循环管道；Pipes from Orion to water tank and pipes of water tank returning to the front tank.

5、2.2纯水循环管道；PW loop distribution Pipes.3 清洗工艺 Cleaning process3.1采用我公司多年成熟的不锈钢管道活洗工艺。Adopt cleaning process for stainless steel pipe which we are good at.3.2 管道的活洗工艺为：Piping cleaning process is as follows:临时配管建立循环回路form circulation水冲洗water flush脱脂degrease水冲洗 rinse by water酸洗 pickling,钝化 passivation水冲洗

6、 rinse by water系统恢复 system reset3.3设备、管线系统内不宜活洗的部件：Components in the equipment and piping that are not suitable to be cleaned活洗系统中的仪表类（一次仪表、二次仪表及仪表传感器）和 UV杀菌灯、 热交换器（板式及管壳式）对活洗液敏感的部件应临时拆除。Other components, such as 1 st loop instrument, 2 nd loop instrument and other transmitter, UV, HX （including pla

7、te type and tube/shell） that are not in conformity with material and are sensitive to cleaning agent, such as flow meter, conductivity meter, level meter, wiring, tank, etc should be dismantled temporarily.3.4管线系统内不参与活洗的短管等拆除的部件采用浸泡活洗，活洗完成后经 检验合格后用塑料保鲜膜包扎，等管线系统活洗完成后再安装复位。All components did not invol

8、ved on the pipeline to be soaked and cleaned. After cleaned and tested, it must be packed with plastic film. Installed and positioned after pipe clean finished.3.5 活洗流程 Cleaning process3.5.1. 所有需要活洗的管道用临时管道连接形成活洗循环系统，采用循环活 洗，活洗时建立一个循环回路.All piping that need cleaning should be connected by temporary

9、piping to form circulation system. Circulating cleaning is used and one loop was formed when proceeding with cleaning.3.5.2.活洗流程图4 清洗过程 Cleaning process所有活洗系统的过程是一样的。 All cleaning system have the same process.4.1 人工处理 Manual handling4.1.1. 管线在活洗前要做全面检查，设备材质和方案中所列要一致。Pipelines should be inspected in

10、the overall perspective before cleaning and make sure that equipment material is in conformity with that listed in the scheme.4.1.2. 不参与活洗的被隔离的仪表阀门等要在活洗前检查确认Isolated instruments and valves that are not cleaned should be checked before cleaning 。4.1.3. 测试样品必须包含两个新焊的，未活洗的焊缝。一个安装在将要 活洗的管路中，另外一个放在化学活洗罐内

11、;.4.2水冲洗：水冲洗及试压的目的在除去管线内表面积灰、泥沙、 脱落的金届 氧化物及其它疏松污垢，并在模拟活洗状态下对临时活洗回路进行泄漏检 查。Rinse with water. Rinse and pressure test aim to remove ashes, mud and shed metallic oxide and other loose dirt on the surface of pipelines and proceed with leak test on temporary cleaning loop under the circumstances of clean

12、ing stimulation.用纯化水(氯离子小于0.1ppM)进行冲洗，冲洗时控制进出水平衡。冲洗 的同时检查活洗循环系统是否有泄漏等情况发生，如果有，在活洗剂添加 前要处理好。Rinse with purified water (chlorine ion is less than 0.1ppM). In rinse process control the balance between incoming and outgoing water and check if circulating system leaks. If so, do it well before adding cle

13、aning agent.4.3脱脂：脱脂处理的目的系统内表面在制作、安装、过程中产生的油脂，使 酸洗液能完全，彻底地和系统内表面接触，从而使活洗彻底，车屯化膜完整；Degrease. It aims to degrease the oil produced in the fabrication, installation of inner surface of system to make pickling agent get in full contact with inner surface system. Therefore cleaning can be finished fully

14、and passivation membrane is in complete situation.4.3.1. 操作步骤，系统加入纯化水(氯离子小丁0.1ppM)至预定液位，开始循环，并加入碱洗药剂。Procedure. Inject purified water (chlorine ion is less than 0.1ppM) into the system and begin the circulation. And add alkaline cleaning medicament for stainless steel and degreasing finishes.4.3.2.

15、工艺条件：Process温度 temperature常温 normal temperature循环时间 circulating time2 小时 hours循环时间可根据天气、管道复杂情况适当延长或缩短。Circulating time can be lengthened or shortened according to the weather and piping.4.3.3. 脱脂药剂：Degreasing medicament）丁与名称NoName1氢氧化钠直到其浓度为2%-3%4.3.4. 测试项目：Items to be testedPH1 次/半小时 once/half hour

16、脱脂液PH要求维持在12以上，当PH小丁 12时应添加氢氧化钠。PH of Degreasing agent to be kept as above 12 and sufficient degreasing agent to be added.PH测试使用PH试纸PH checked with PH test paper4.4水力冲洗：水力冲洗的目的是除去脱脂后脱落的污物，并将系统表面残留的脱脂液冲洗十净。Water rinse to get rid of shed ordure and flush remaining degreasing agent on system surface cl

17、ean.4.4.1. 操作步骤，排尽系统内脱脂液，用大量水冲洗。Operation procedure. Drain degreasing solution in the system and flush the system with enough water.4.4.2. 测试项目，用视觉观察冲洗水至透明无微粒，测定 PH小于9。Items to be tested. Check flush water to be transparent with no particulate visually and make sure PH value less than 9.PH2 次/半小时 tw

18、ice/ half hourPH测试使用PH试纸，当PH小于等于9时水冲洗完成。PH checked with PH test paper and water flush finished when PH <9.4.5酸洗：酸洗的目的是利用酸洗液将金届表面的铁锈氧化物等污垢进行化学 和电化学反应，生成可溶性物质，并利用酸洗液的冲刷作用除去污垢。Pickling. Pickling aims to make dirt like rusted oxide on the surface of metal proceed with chemical and electromechanical r

19、eaction to produce dissoluble material and get rid of dirt with pickling solution.4.5.1. 操作步骤，排净系统水冲洗残液后，随即系统加水至一定液位循环， 加入不锈钢专用酸洗剂，随后补充水至控制液位。活洗过程中定期排 污排空。Operation procedure. After remaining rinse solution is drained away, inject a certain amount of water into the system to a certain level for circ

20、ulation. Add special pickling medicament for stainless steel into it. Then inject a certain water to control level. Blow down the waste periodically during cleaning.4.5.2. 工艺条件：Process situation常温 normal temperature活洗温度cleaning temperature循环时间 circulating time2小时hours4.5.3.酸洗钝化药剂:）丁与名称NoName1柠檬酸，保证浓

21、度在10%15%4.5.4. 测试项目：Items to be testpH 值 PH value1 次/半小时 twice/half hour酸洗液PH要求小丁等丁 1,当PH大丁 1时应添加柠檬酸，保证浓度在10%15%。Picked chemical PH less than 1 and picked chemical to be added incasePH is higher than 1.PH测试使用PH试纸PH checked with PH test paper4.6水冲洗：车屯化完成后的水冲洗是为了把残留的*屯化液除去。Water rinse. Water rinse aft

22、er finishing passivation is to get rid of remaining passivation solution.4.6.1. 钝化结束后，排尽钝化液洗液，用纯化水(氯离子小丁0.1ppM)进行冲洗，除去残留的钝化液，当PH直接近中性Ph>6,电导率差小丁 0.5 g/cm,即可结束。After finishing passivation, drain away solution for passivation and flush with purified water (chlorine icon is less than 0.1ppM) to remo

23、ve remaining passivation solution. When PH is close to the neutralization (pH>6), difference of conductivity less than 1 饵/cm passivation finishes.4.6.2. 工艺条件 Process condition活洗温度 cleaning temperature 常温 normal temperature4.6.3. 测试项目：Items to be testedPH2 次/半小时 twice/half hour2 次/半小时 twice/half

24、hour电导率 conductivityPH测试使用PH试纸PH test by PH test paper.使用电导率仪测定电导率Cond tested by cond. Meter.4.7系统恢复，活洗完成后将系统恢复原样。System reset. Get the system back after finishing cleaning.4.8如果系统长时间不投入使用，建议用氮气封存。If the system is not put into use for a long time, nitrogen is suggested for sealing.5 废液处理 Waste liquo

25、r treatment5.1各活洗过程中的冲洗水，未添加活洗剂，可以直接排放。Flush water without cleaning additive during cleaning can be discharged directly.5.2酸洗液的废液，车屯化液的废液，用槽罐车把废水运输到废水处理厂处理排 放。Waste liquor of pickling solution and greasing solution should be delivering with tank car to waste water treating plant for handling and dis

26、charging.6 甲方提供的条件 Condition supplied by the owner甲方负责提供如下公用设施：The following utilities are provided by the owner.6.1 水：全程采用纯化水，纯化水要求氯离子小于0.1ppM,使用ORION屯化水.Purified water is used through the system and purified water should include less than 0.1ppM chlorine icon. Orion will provide the purified water

27、 for chemical pickled and passivation.6.2 电源(活洗时使用纯化水泵)。Power supply. Purified water pump is used when cleaning.6.3 干燥无油的压缩空气或氮气，0.5-1 MPa。Dry compressed air or nitrogen with no oil of 0.5-1 MPa.7 临时配管 Temporary tubing7.1临时配管是指将活洗系统中管道连接起来，形成活洗循环回路，活洗完成 后需要拆除的管道和设施。Temporary tubing is the piping and

28、 facility that need be dismantled after cleaning Connect piping in the cleaning system to form circulating loop.7.2临时配管用软塑料管。Temporary tubing adopts soft plastic tube.8 检验与验收Test and accept8.1钝化表面目测，钝化膜完整，颜色一致。Check the surface of passivation visually to make sure that passivation film is complete and has the same color.8.2在回路的最后一个焊缝采用铁袱化钾溶液显蓝测定，变色时间大丁 30秒 钟。On